34results about How to "Ease of widespread commercial application" patented technology

The invention discloses a microcapsule self-repairing anticorrosive coating and a preparation method thereof. The coating is composed of silicon dioxide microcapsules containing corrosion inhibitor inside in silicon-based emulsion. The method is as follows: firstly, a tetraethyl orthosilicate cyclohexane solution and the corrosion inhibitor are mixed, and the pH value is adjusted by acid, then themixture is stirred and allowed to react, and then the reaction solution is filtered; subsequently, a sodium dodecyl benzene sulfonate aqueous solution is added to the obtained organic-inorganic hybrid emulsion and stirred, the obtained water-in-oil core material emulsion is subjected to solid-liquid separation, washing and drying in turn to obtain silicon dioxide microcapsule encapsulated with corrosion inhibitor, the metal platinum catalyst is added in silicone oil and stirred to obtain silicon-based emulsion, the silicon dioxide microcapsule encapsulated with corrosion inhibitor and the a metal platinum catalyst are mixed and maleic anhydride monododecyl ester is added, the mixture is subjected to stirring and reacting to obtain the target product. It has good stability and fast repairing speed, so it is very easy to be widely used in the field of steel structure and concrete steel structure corrosion protection.

The invention discloses a silver nanowire and M-phase vanadium dioxide nanoparticle composite film and a preparation method thereof. The film is prepared from silver nanowire film with the film thickness of 80-120 nm and an M-phase vanadium dioxide nanoparticle film with the film thickness of 100-1000 nm, which are sequentially coated on a substrate, wherein the linear diameter of the silver nanowire for forming the silver nanowire film is 40-100 nm, and the wire length is 50-100 microns; the particle size of the M-phase vanadium dioxide nanoparticle for forming the M-phase vanadium dioxide nanoparticle film is 20-100 nm. The preparation method comprises the following steps: spin coating or blade coating the substrate with silver nanowire isopropanol solution with the concentration of 0.3-1.5 wt%, drying the substrate, spin coating or blade coating the substrate coated with the silver nanowire film with M-phase vanadium dioxide nanoparticle aqueous solution with the concentration of 2-5 wt% or ethanol solution, and at last preparing the target product. The silver nanowire and M-phase vanadium dioxide nanoparticle composite film is low in phase transformation voltage; the preparation method is convenient and low in cost; the composite film can be widely applied to the fields such as energy-saving windows, gas sensors, optoelectronic switches, thermistors, infrared remote sensing receivers and uncooled focal plane radiation detectors.

The invention discloses a gallium sulfide quantum dot material and a preparation method thereof. The material is gallium sulfide quantum dots, the chemical formula is Ga x S 3 , where 1≤x≤5, the chemical formula is Ga x S 3 The gallium sulfide quantum dots have a diameter of 1-8nm; the method is to mix four or mixed to obtain a mixed solution, and then the mixed solution is placed in an inert atmosphere and reacted at 220-300°C for 2-20min to obtain a reaction solution. After that, the molar ratio of the gallium source, solvent and precipitant in the reaction solution The ratio is 1:50-300:100-1400, adding solvent and precipitant successively to the reaction liquid cooled under an inert atmosphere to obtain a suspension, and then performing solid-liquid separation on the suspension to obtain a gallium sulfide quantum dot material . Its luminescence peak under the excitation of ultraviolet light is adjustable in the range of 420-505nm, and it is very easy to be widely commercialized and applied in the fields of light-emitting devices and ion detection.

The invention discloses a silicon dioxide nano porous membrane with gradient porosity and a preparation method of the silicon dioxide nano porous membrane. The nano porous membrane has the membrane thickness of 100-500 nm and consists of three or more layers of porous membranes with different spherical pore diameters, wherein the bottom pore diameter is 1-3 nm, the surface pore diameter is 5-8 nm,the pore edge space is 10-2 nm from bottom to top, and the porosity ranges from 30%-35% to 60%-70% from bottom to top. The method comprises the steps as follows: tetraethyl orthosilicate and ethanolare mixed, a mixed solution is obtained, a nitric acid aqueous solution is dropwise added to the mixed solution, silicon dioxide sol is obtained after stirring, cetyl trimethyl ammonium bromide is added, stirring is performed, mixed sol is obtained after aging, then, a substrate is sequentially placed in the mixed sol with gradually increased cetyl trimethyl ammonium bromide for pull coating 3 times or more, the obtained product is aired and annealed, and a target product is prepared. The silicon dioxide nano porous membrane has wear resistance and super-hydrophilic property and can be very easily and commercially applied to anti-fog, self-cleaning, wide spectrum anti-reflection fields and the like.

The invention discloses a magnesium hydroxide-calcium alginate composite fire retardant and a preparation method thereof. The fire retardant is prepared from magnesium hydroxide and calcium alginate with the molar ratio being (1 to 3) to 1. The method comprises the following steps of calcining dolomite mineral powder to obtain dolomite ash powder, then adding the dolomite ash powder into water forstirring to obtain a digestive juice, then dropwise adding a sodium alginate aqueous solution into the digestive juice under stirring, performing stirring and foaming to obtain a foamed gel, then performing dryness finalization treatment on the foamed gel to prepare a target product, wherein dryness finalization treatment is spray drying finalization, spinning drying finalization, coating dryingfinalization or die formation drying finalization. The magnesium hydroxide-calcium alginate composite fire retardant has a limit oxygen index of 40 percent, is not decomposed with heat still at high temperature of 250 DEG C and is very easy to be widely and commercially applied to the fields of degradable fire-retardant fabrics, fire-retardant coating layers for decoration, non-combustible children toys and the like.

The invention discloses a SiO with porous structure 2 Acid-base composite nano-coating and preparation method thereof. The coating is composed of a 150‑200nm thick multi-slit film on the substrate, in which the multi-slit film is composed of SiO2 distributed in a three-dimensional network 2 Nanoparticles interposed with SiO containing mesoporous 2 Nano chains are formed; the method is to drop the separately prepared ethyl tetrasilicate ethanol solution into the mixed aqueous solution drop by drop, then stir and age, and then add the obtained SiO 2 After adding nitric acid aqueous solution dropwise to the alkaline sol, add water, ethanol and ethyl tetrasilicate mixture to it in turn, after stirring to obtain an acid-base composite sol, then add polyethylene glycol 300 to it first and stir for aging Finally, the substrate is placed in the obtained sol for coating, dipped to pull the coating, and then dried, and then annealed the obtained substrate coated with a film to obtain the target product. It has good hydrophilicity, wear resistance and high light transmittance, and it is very easy to be widely commercialized and used in anti-fog, self-cleaning, wide-spectrum anti-reflection and other fields.

The invention discloses an outdoor SiO 2 Superhydrophilic nano coating and its preparation method. The coating is composed of a mesoporous acid film connected to a granular alkali film on a glass substrate; the method is to first drop the prepared ethyl tetrasilicate ethanol solution into the aqueous ammonia solution, and then stir and age the obtained alkali-catalyzed reaction precursor solution After, to the obtained aged SiO 2 Add nitric acid aqueous solution dropwise to the alkaline sol, then add water and a mixture of ethanol and ethyl tetrasilicate to it in turn, then, first stir the obtained acid-catalyzed reaction precursor solution containing alkali particle sol, and then wait for the obtained acid After the alkali composite sol is allowed to cool to room temperature, add a pore-forming agent to it and then age after stirring. Finally, the glass substrate is dipped in the obtained sol for coating to pull the coating and then dried, and then the obtained coating is Annealing the glass substrate to obtain the target product. It has high outdoor weather resistance, and it is very easy to be widely commercialized and applied in anti-fog, self-cleaning, wide-spectrum anti-reflection and other fields.

The invention discloses a lead sulfide thin film with the wide absorption spectrum and a preparation method of the lead sulfide thin film. The thickness of the thin film is 500-540nm. The particle diameter of each lead sulfide crystal grain is 6-10nm. At the wave band of 450-220nm, the thin film consisting of the lead sulfide crystal grains the diameter of each of which 6-10nm displays an absorption peak. According to the invention, by use of the chemical vapour deposition method: firstly successively adding the sodium hydroxide solution, the thiourea solution and the triethanolamine solution into the lead acetate solution so as to obtain a mixed solution; then adding the deionized water into the mixed solution to obtain a reaction solution; arranging a substrate into the stirred reaction solution of the 70 DEG C-80 DEG C for at least 2h so as to obtain the substrate with the reagent on the surface; and cleaning and drying the substrate with the reagent on the surface to prepare the target product. According to the invention, the thin film has the quite wide wave band absorption characteristic, and is quite easily, widely and commercially applicable to field of photodetection, solar energy coating absorption layers and gas sensing detection.

The invention discloses a high-energy particle energy-reducing device and a preparation method thereof. The energy-reducing device is a graphite substrate covered with a dense boron nitride coating, and the thickness of the dense boron nitride coating is 5-800[mu]m; the preparation method adopts a vapor deposition method, and comprises the following steps: firstly, placing a graphite substrate into a vacuum chamber, then mixing an ammonia gas, a boron chloride gas and a nitrogen gas according to the volume ratio of the ammonia gas to the boron chloride gas to the nitrogen gas of (0.8-1.2):(0.8-1.2):(40-60) to obtain a mixed gas, then firstly raising the temperature in the vacuum chamber to 500-2000 DEG C, and finally introducing the mixed gas with a flow quantity of 10-100sccm into the vacuum chamber for 12-36h to obtain the target product. According to the high-energy particle energy-reducing device provided by the invention, the degassing rate is much lower than that of a graphite energy-reducing device, a high-energy particle beam has good penetrating performance on the high-energy particle energy-reducing device and the graphite energy-reducing device, and the high-energy particle energy-reducing device can be easily, widely and commercially applied to the fields of high-precision and high-energy particle beam energy reduction of a cyclotron.

The invention discloses a preparation method of porous graphene. The preparation method comprises the following steps: dissolving ammonium salt and glucose into deionized water according to a weight ratio of the ammonium salt to the glucose to the deionized water being (0.6 to 1.2) to (0.4 to 0.8) to 5, thus obtaining mixed liquor, then adding a 1.8 to 2.2g / L graphene oxide water solution into the mixed liquor according to a weight ratio of the graphene oxide water solution to the ammonium salt in the mixed liquor being 10 to (0.6 to 1.2), stirring, drying to form a paste shape at 30 to 50 DEG C, thus obtaining a pasty mixture, then putting the pasty mixture into a protective atmosphere, heating the pasty mixture to 900 to 1000 DEG C from room temperature through 2 to 4h, and preserving heat for 1 to 2h, thus preparing a target product, wherein the ammonium salt is ammonium chloride or ammonium carbonate or ammonium nitrate, and the protective atmosphere is an argon atmosphere or helium atmosphere or neon atmosphere. The target product prepared by the preparation method can be directly used, is higher in electrical conductivity, and is very easily and widely commercialized and applied to fields such as environmental governance and energy utilization.

The invention discloses a colorful solar cell and a preparation method thereof. The battery is an ordered silicon nanowire array with a PN junction formed on the surface on a silicon substrate, wherein the diameter of the silicon nanowire is 50-120nm, the period is 500-1500nm, and the surface is covered with a dielectric layer with a thickness of 1-200nm; method In order to make an ordered mask on the surface of the silicon substrate using the nanosphere template method or electron beam exposure method or nanoimprint technology, the ordered nanometers are etched on it using a wet process or a Bosch process of reactive ion etching. line array, and then use the diffusion process to do the boron element on the surface of the silicon substrate with the ordered silicon nanowire array on it, and then, the obtained ordered silicon nanowire array with the PN junction formed on the surface After the dielectric layer is made by chemical vapor deposition method, electron beam evaporation method, atomic layer deposition technology or spin coating method on the silicon substrate, electrodes are made on it to obtain the target product. It can be easily and widely commercially applied to photovoltaic power generation systems in cities.