The invention relates to a preparation method for a doped
float zone silicon crystal. The method comprises that: (1) cone
grinding,
corrosion, cleaning and
drying are performed on a polysilicon material; (2) the polysilicon material is fixed in a cavity of a magnetron
sputtering apparatus, a
phosphorus-
silicon-doped target is arranged, vacuumizing is performed to achieve 5*10<-3> Pa,
argon gas is introduced to achieve the pressure in the cavity of 1 Pa, a
high voltage of 500 Kv is applied between the two electrodes,
argon ions produced through
ionization continuously bombard the target, the
phosphorus atoms and the
silicon atoms in the target obtain energy, sputter, and deposit on the surface of the polysilicon to form a layer of a uniform and compact
phosphorus / silicon film, the
sputtering is performed for 30-90 min and then is stopped, the
sputtering chamber is opened to rotate the polysilicon 180 DEG, the steps are repeated, and the sputtering is continuously performed for the same time; and (3) the polysilicon material is taken out and placed into a
float zone silicon
crystal furnace, the
seed crystal and the polysilicon are centered, steps of vacuumizing,
argon gas introduction, preheating,
fusion splicing,
narrow neck shrinking and
crystal diameter achieving are sequentially performed until the equal
diameter is maintained, and the ending step is performed. The preparation method has characteristics of low-cost, high production efficiency and no
toxicity and harm, wherein the uniformities of the radial resistivity and the axial resistivity are good.