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1095results about How to "Efficient preparation method" patented technology

Method for preparing polymer porous nanofiber through mixed phase separation

The invention discloses a method for preparing polymer porous nanofiber through mixed phase separation. The diameter of the prepared polymer porous nanofiber is between 300nm and 900nm, and the aperture is 1 to 120nm. The preparation method for the polymer porous nanofiber comprises the following steps of: mixing a polymer, an additive and a solvent according to certain proportion; heating and stirring the mixture until the mixture is completely dissolved and forms transparent solution; performing electrostatic spinning on the solution; depositing primarily generated fibers in ice-water bath or the water bath with the temperature of 0 to 20 DEG C, wherein thermally induced phase separation and nonsolvent induced phase separation are caused; and extracting residual solvent and additive through post treatment to obtain the polymer porous nanofiber. The preparation method is simple and highly effective and is convenient to perform; and polymer porous nanofibers with different diameters and porosities can be prepared by adjusting the conditions of electrostatic spinning. The method has enormous application prospect in aspects, such as high-tech composite materials, water treatment, catalyst carriers, electrode materials and the like.
Owner:ZHEJIANG UNIV

Anode material for lithium-ion battery and preparation method of anode material

The invention discloses an anode material for a lithium-ion battery and a preparation method of the anode material. The material is structurally characterized by adopting a core-shell structure and comprises an active and stable core formed by uniformly dispersing submicron-grade multi-scale tungsten carbide particles in an amorphous silicon substrate and a highly-conductive shell coated with a thin-layer graphene sheet formed by stripping. The preparation method is a two-step ball-milling method, during ball milling in the first step, the tungsten carbide particles can fully play a milling assisting role to efficiently refine original coarse silicon; during ball milling in the second step, the graphene sheet formed by stripping ordinary graphite can stabilize the structure and improve the electrical conductivity. Therefore, the prepared anode material for the lithium-ion battery has the advantages of stable structure, good cycle performance, excellent rate performance and the like.
Owner:SOUTH CHINA UNIV OF TECH

Aluminum silicon carbide composite material with laser welding layer and preparing method of aluminum silicon carbide composite material

The invention discloses an aluminum silicon carbide composite material with a laser welding layer and a preparing method of the aluminum silicon carbide composite material. The composite material is composed of the laser welding layer and an aluminum silicon carbide layer, the laser welding layer is composed of pure aluminum or aluminum alloy comprising silicon and aluminum, the volume fraction of the silicon in the aluminum alloy is a, the volume fraction of the aluminum in the aluminum alloy is b, the a is greater than 0 and less than or equal to 30%, and the b is greater than or equal to 30% and less than 100%. The aluminum silicon carbide layer is composed of silicon carbide and pure aluminum or aluminum alloy, and the volume fraction of the silicon carbide ranges from 30% to 70%. The preparing method comprises the steps that silicon carbide pelleting powder is prepared firstly, then silicon carbide preformed parts are prepared, and the aluminum silicon carbide composite material with the laser welding layer is prepared in the vacuum pressure impregnation method finally. The aluminum silicon carbide composite material is good in weldability and gas tightness, high in heat conductivity, low in coefficient of thermal expansion, simple in preparing method, efficient and low in cost.
Owner:NAT UNIV OF DEFENSE TECH

Completely-methanated catalyst as well as preparation method and application thereof

ActiveCN103071507AImprove activity and high temperature hydrothermal stabilityHigh activityGaseous fuelsCatalyst activation/preparationActive componentNatural gas
The invention provides a completely-methanated catalyst as well as a preparation method and an application thereof. The preparation method comprises the following steps of: respectively mixing precursors of an active component, a first auxiliary agent and a second auxiliary agent and dissolving into water to prepare a solution I; adding a precipitating agent into water to be dissolved to respectively prepare a solution II and a solution II'; adding a precursor of a carrier into the water to be dissolved to prepare a solution III or a solution III'; adding the solution I into the solution II to carry out precipitation to obtain a precipitating system I; adding the solution II' into the solution III to carry out the precipitation to obtain a precipitating system II or adding an acidic solution into the solution III' to peptize to obtain the precipitating system II; and then mixing the precipitating system I with the precipitating system II. According to the completely-methanated catalyst as well as the preparation method and the application thereof, the catalyst is prepared by applying a sub-step reverse precipitating method; and the catalyst has the characteristics of high activity and high safety and is suitable for being applied to a high-temperature or low-temperature completely-methanated reaction process for synthesizing natural gas by coal gasification through methanation.
Owner:DATANG INT CHEM TECH RESINST

Preparation method of nemadectin

The invention discloses a preparation method of nemadectin. According to the invention, a fermentation broth used for producing nemadectin is directly dried by spraying, such that solid powder is obtained; the solid powder is extracted by using an organic solvent, the extract is filtered, and nemadectin in the extract is absorbed by using macroporous resin; nemadectin absorbed by macroporous resin is then eluted; and the eluent is extracted, concentrated, and dried, such that a nemadectin pure product is obtained. According to the invention, a direct spray-drying method is adopted upon the fermentation broth, and the obtained dried solid fermentation bacterium powder is transportation-tolerant, and is easy to store. With the method provided by the invention, the producing of nemadectin degradation product is reduced, the bacterium powder is easy to extract, and the consumption of the extraction solvent is low. The technology is simple, the cost is low, and the method is easy to operate. With the method, the prepared nemadectin has a high HPLC purity of above 90%.
Owner:CHONGQING DAXIN PHARMA +2

Carbon nano tube reinforced polyaniline nano-fiber and preparing method thereof

InactiveCN102558554AConductivity controllableOvercome the technical problem of not being able to conduct electricity under alkaline conditionsFiberPolymer science
The invention discloses carbon nano tube reinforced polyaniline nano-fiber and a preparing method thereof. The preparing method includes steps of: adding aniline monomers and carbon nano tubes into dilute acid for ultrasound treatment to obtain carbon nano tube and aniline monomer blend solution; dissolving initiators into ethanol to form initiator solution and dissolving oxidants in dilute acid to form oxidant solution; and adding the initiator solution into the carbon nano tube and aniline monomer blend solution, then adding the oxidant solution, severely swinging for a moment, performing centrifugation, washing, redispersion and the like after standing reaction is complete so as to finally obtain the carbon nano tube reinforced polyaniline nano-fiber. The preparing method is simple, efficient and high in controllability. The carbon nano tubes can be uniformly dispersed on a polyaniline matrix. The mean diameter of the obtained carbon nano tube reinforced polyaniline nano-fiber is 30-60 nm, the length is 1-2 mu m, and electric conductivity is 10(-8)-10(2) S/cm, and the carbon nano tube reinforced polyaniline nano-fiber can be used in the application fields such as sensors, actuating devices, ultra-capacitors, electrochromatic windows, functional coatings and ultrafiltration membranes.
Owner:UNIV OF SHANGHAI FOR SCI & TECH

Bioactive bacterial cellulose-zein composite film and preparation method thereof

The invention discloses a bioactive bacterial cellulose-zein composite film and a preparation method thereof. The method comprises the following steps: preparing and purifying a bacterial cellulose film; uniformly stirring the purified bacterial cellulose in distilled water, shearing by using a high-speed shearing machine, and homogenizing by high pressure microfluidization to obtain a nano-fiber dispersion liquid; dissolving zein and water-insoluble bioactive substances in an ethanol-water solution to obtain an alcoholic solution; dissolving sodium caseinate in water, stirring and adding the solution into the alcoholic solution to obtain a mixed solution; removing the ethanol, and centrifuging to obtain bioactive molecule enriched zein nanoparticles; mixing the nano-fiber dispersion liquid and the bioactive molecule enriched zein nanopartiles, uniformly stirring, and carrying out ultrasonic treatment; and sucking and filtering in vacuum, and quickly forming a film; and drying. The composite film material has the advantages of excellent mechanical performance, biocompatibility and biodegradability, and has managed bioactivities of bacteria resistance, oxidation resistance and the like.
Owner:SOUTH CHINA UNIV OF TECH

Two-dimensional perovskite single-crystal material and preparation method thereof

The invention relates to a two-dimensional perovskite single-crystal and a preparation method thereof. The chemical composition of the two-dimensional perovskite single-crystal material is A2PbBr4, wherein A is C4H9NH3+ or C3H7NH3+. Lead bromide and ammonium bromide with the ratio being 1:2 are adopted as raw materials, dimethylformamide is adopted as a solvent, chlorobenzene or a mixture of chlorobenzene and acetonitrile are adopted as an anti-solvent, and due to the anti-solvent mixing evaporation method, the large-size two-dimensional perovskite single-crystal is prepared under the room temperature atmosphere environment. The method is low in environment condition requirement, simple in process, applicable to preparing large-size crystal. The two-dimensional perovskite single-crystal has the good application prospect in the photoelectric field, and the efficient and simple preparation method has the great potential for single-crystal commercialization application.
Owner:WUHAN UNIV

Machining technology for high-precision outer conical surface thin wall sleeve

InactiveCN103495844AMeet the technical requirements of high-precision outer tapered thin-walled sleevesReduce distortionNumerical controlEngraving
The invention relates to the technical field of high-precision part machining process, in particular to a machining technology for a high-precision outer conical surface thin wall sleeve. The machining technology includes the following technology processes of workblank preparing, spheroidizing annealing, rough turning, thermal refining, semi-finish turning, finish turning, hole drilling, distressing, plane grinding, rough grinding, secondary distressing, plane grinding, spiral groove turning, plane lapping, accurate grinding, wire-electrode cutting, end face turning, serial number engraving, detecting, qualified product obtaining, press fitting, conical surface fit detecting, part matching and serial number printing, cleaning, lubricating oil coating and warehousing. A double-end vertical type numerical control grinder is adopted as a finishing machine, and through the machining methods of rough grinding and accurate grinding or rough grinding, semi-accurate grinding and accurate grinding, the technical requirements of the high-precision outer conical surface thin wall sleeve can be met; through the corresponding distressing heating processing technology, residual stress in the machining process is removed, deformation in the machining process can be reduced, the yield of products is improved, and finally the good manufacturing method of the high-precision outer conical surface thin wall sleeve is provided.
Owner:CRRC QISHUYAN CO LTD

Cu2O-TiO2/reduced graphene oxide ternary complex, and preparation method and applications thereof

The invention discloses a Cu2O-TiO2 / reduced graphene oxide (RGO) ternary complex, and a preparation method and applications thereof. The preparation method of the ternary complex comprises the following steps: preparing graphene oxide (GO) through a Hummers method, preparing a TiO2 / RGO binary complex through a hydrothermal method, and preparing the Cu2O-TiO2 / RGO ternary complex through precipitating and reducing processes. The preparation method has the advantages of simplicity, low cost and benefiting for the industrialized production; and the prepared ternary complex has a high catalysis activity in a visible region as a visible-light-induced photocatalyst, has a high catalysis efficiency, is especially suitable for degrading organic pollutants in a solution, and can be used for photo-decomposing water to produce hydrogen and degrading volatile organic pollutants in air as the visible-light-induced photocatalyst.
Owner:CENT SOUTH UNIV

Silicone composition

The present invention relates to silicone compositions which comprise at least one ketoximosilane-terminated polydiorganosiloxane and also at least one alkoxysilane. These compositions are neutrally crosslinking and combine a low odour with high adhesion and good storage stability.
Owner:SIKA TECH AG
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