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657results about "Molybdenum oxides/hydroxides" patented technology

Method for producing metal oxide film, metal oxide film, element using the metal oxide film, substrate with metal oxide film, and device using the substrate with metal oxide film

Disclosed are: a metal oxide film, which is formed by a coating method that is one of the methods for producing a metal oxide film, and which has a good balance between excellent transparency and high electrical conductivity, while having excellent film strength; and a method for producing the metal oxide film. Specifically disclosed is a method for producing a metal oxide film, which comprises: a coating step wherein a coating film is formed on a substrate using a metal oxide film-forming coating liquid that contains various organic metal compounds; a drying step wherein the coating film is changed into a dry coating film; and a heating step wherein an inorganic film is formed from the dry coating film. The method for producing a metal oxide film is characterized in that in the heating step, the dry coating film, which is mainly composed of the various organic metal compounds, is heated to a temperature at which at least mineralization of organic metal compound components occurs or higher in an oxygen-containing atmosphere at a temperature not higher than the temperature that is lower by 10 DEG C than the dew point, so that the organic components in the dry coating film are removed by thermal decomposition or combustion, or by thermal decomposition and combustion, thereby forming a metal oxide fine particle layer which is densely filled with metal oxide fine particles that are mainly composed of various metal oxides.
Owner:SUMITOMO METAL MINING CO LTD

Method for preparing two-dimensional nanosheets by microwave-assisted liquid phase stripping of layered material

The invention discloses a method for preparing two-dimensional nanosheets by microwave-assisted liquid phase stripping of a layered material. The method comprises the following specific steps: 1) carrying out wet grinding of precursor powder of the layered material with a liquid medium in a mortar; 2) washing the wet-ground mixture with a same liquid medium and transferring into a microwave reaction tube; 3) placing the microwave reaction tube into a microwave reaction device, and carrying out microwave irradiation; 4) after microwave irradiation, washing and filtering the microwave mixture, and collecting a filter membrane; 5) carrying out ultrasonic dispersion of the obtained filter membrane in an organic solvent, and carrying out centrifugal separation, wherein a supernatant is a nanosheet dispersion liquid, and a precipitate is a separated unpeeled phase; and 6) filtering the obtained nanosheet dispersion liquid, collecting a filter membrane, and carrying out vacuum drying to obtain the nanosheet powder. The method is universal, fast and efficient in peeling various layered materials, and the prepared nanosheets are ultra-thin, large in size, small in peeling size reduction andhigh in chemical stability, and have broad application prospects in basic scientific researches, electronics, catalysis, energy, sensing and other hot fields.
Owner:SHANGHAI JIAO TONG UNIV

Method for synthesizing rod-like and echinoid molybdena-based nano-material

The invention relates to a quick and efficient non-template agent hydro-thermal synthesizing method. The system can synthesize an alpha-molybdenum trioxide nanometer rod and a high-density echinoid molybdenum oxide based nanometer materials. Molybdenum peroxide acid prepared from molybdenum trioxide and aqueous hydrogen peroxide solution is used as a precursor, is produced into scattered alpha-molybdenum trioxide nanometer rod by hydro-thermal synthesis at a temperature of between 80 and 180 DEG C, and is produced into the peroxide modified molybdenum oxide hydrate by hydro-thermal synthesis at a temperature of between 65 and 75 DEG C. The hydrate is a multiscale structure; a nanometer thin slice, a micron prism and a nanometer rod-shaped structure unit are divergently assembled into a micron-size high-density echinoid structure. The hydrate is roasted to obtain high-density echinoid alpha-molybdenum trioxide. Modulation of the synthesizing condition can realize fine adjustment for appearance of the nanometer rod, the micron-size echinoid structure and the structure unit thereof. The method uses raw materials with low cost, has the advantages of simple technical process, controllable conditions and the like, and can promote research and application of the molybdenum oxide in the fields of sensors, field transmission, electrode materials and so on.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI
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