The invention relates to a preparation method of an
oxide porous material. According to the technical scheme, the method comprises the steps that an
oxide precursor salt is dissolved in
organic solvent according to the concentration
ranging from 5 mol / L to 10 mol / L, stirring is conducted, and a solution I is obtained; a binder is added into the solution I according to the
mass ratio of the
oxide precursor salt to the binder of 1 to 0.01-0.1, stirring is conducted, and a solution II is obtained; a template agent is added into the solution II according to the
mass ratio of the oxide precursor salt to the template agent of 1 to 0.1-0.35, stirring is conducted, and a solution III is obtained;
liquid nitrogen freezing treatment is conducted on the solution III,
drying is conducted in a vacuum freezing dryer, and a dried product is obtained; the product is put in a
tube furnace, the temperature rapidly rises to 300-800 DEG C at the speed of 4-5 DEG C / min in an
argon atmosphere or
air atmosphere, heat preservation is conducted for 4-12 h, natural cooling is conducted along with the furnace, the template agent is removed, and the oxide porous material is obtained. The preparation method of the oxide porous material is convenient to operate and suitable for industrial production, and the
hole size, the
porosity and the wall thickness of the product can be regulated in a larger range.