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105 results about "Superparamagnetic iron oxide nanoparticles" patented technology

Method for preparing magnetic oxide iron and magnetic oxide iron desulfurizer prepared thereby

ActiveCN101585557AGuaranteed temperatureGuaranteed firing temperatureIron oxides/hydroxidesFerrous saltsSulfur
The invention relates to a method for preparing magnetic oxide iron Fe21.333O32, which comprises the following steps: (a) mixing solid soluble ferrous salt and solid hydroxid according to a molar ratio of iron to hydroxyl being between 1:2 and 1:3; (b) completing reaction of a mixed material prepared in step (a) by kneading, and controlling the temperature of the material not to exceed 70 DEG C in the kneading process; (c) drying a reaction product obtained in step (b) in air; (d) washing and filtering a material obtained in step (c); (e) naturally drying or baking a solid obtained in step (d); and (f) roasting a product obtained in step (e) at a temperature of between 150 and 500 DEG C. The invention further discloses a magnetic oxide iron Fe21.333O32 desulfurizer prepared by the preparation method. Tests show that the desulfurizer has high sulfur capacity reaching 62.0 percent.
Owner:BEIJING SJ ENVIRONMENTAL PROTECTION & NEW MATERIAL CO LTD

Preparation method of magnetic biochar loaded photosynthetic bacteria material and sewage treatment method

The invention relates to the technical field of sewage treatment, and in particular to preparation method of magnetic biochar loaded photosynthetic bacteria material and a sewage treatment method. The preparation method comprises the steps of: preparing a magnetic nano iron oxide material by a chemical coprecipitation method, conducting activation and expansion culture on photosynthetic bacteria, loading the nano iron oxide particles on the surface of biological carbon material through a self-assembly method to form a magnetic biochar; and loading the photosynthetic bacteria on the surface of the magnetic biochar through a co-incubation method, so as to obtain the magnetic biochar loaded photosynthetic bacteria material. The magnetic biochar loaded photosynthetic bacteria material is co-incubated with sewage for a period of time, so as to realize degradation of COD, ammonia nitrogen and phosphate radical in the sewage. The invention employs the electrostatic binding of high specific surface of the nano magnetic iron oxide and the bacteria with charge on the surface to achieve immobilization of strains, and magnetic iron oxide material has activation on strain enzyme, thereby enhancing the degradation of COD, ammonia nitrogen and phosphate radical by microbes.
Owner:JIANGSU ACADEMY OF AGRICULTURAL SCIENCES

D-glucosamine-modified iron oxide nanoparticles and preparation method of lyophilized powder thereof

The invention relates to d-glucosamine-modified iron oxide nanoparticles used as a tracer for magnetic resonance, a preparation method of lyophilized powder thereof and use thereof. The d-glucosamine-modified iron oxide nanoparticles comprise superparamagnetic iron oxide nanoparticles, wherein the surfaces of the superparamagnetic iron oxide nanoparticles are modified by a substance having carboxyls; the carboxyls react with the aminos of the d-glucosamine to form amido bonds; and thus a structure that the surfaces of the superparamagnetic iron oxide nanoparticles are modified by the d-glucosamine is formed. The invention provides a novel tumor-targeted MRI contrast agent which has high selectivity of tumors for the tumor targeted magnetic resonance diagnostic tests and clinic tumor diagnosis. By preserving the d-glucosamine-modified superparamagnetic iron oxide nanoparticles in form of the lyophilized powder, the unstable problem of the d-glucosamine-modified superparamagnetic iron oxide nanoparticles is solved. The d-glucosamine-modified iron oxide nanoparticles are sterile, anhemolytic and free from vascular stimulation and can meet the requirements of tests of cells, animals and the like.
Owner:ZHENJIANG NO 1 PEOPLES HOSPITAL +1

Novel mesoporous silicon sphere co-loaded medicine nano-complex and preparation method thereof

The invention discloses a novel mesoporous silicon sphere co-loaded medicine nano-complex and a preparation method thereof. The novel mesoporous silicon sphere co-loaded medicine nano-complex is Ce6@MMSN / DOX / Ko143@PAsp-b-PEG-FA; the preparation method comprises the following steps: selecting TEOS (Tetraethyl Orthosilicate) as a silicon source, CTAB (Cetyltrimethyl Ammonium Bromide) as a template agent and n-hexane as a pore expanding agent and synthesizing mesoporous silicon dioxide nanoparticles with a double-pore-channel core-shell structure; carrying out amination modification on the mesoporous silicon dioxide nanoparticles; synthesizing Fe3O4 nanoparticles by adopting an LSS (Liquid-Solid-Solution) phase transfer method and ligand exchange reaction; modifying and embedding superparamagnetic iron oxide nanoparticles on the surface of aminated MSN through nucleophilic substitution, so as to construct magnetic mesoporous silicon dioxide nanoparticles; taking DCC (Dicyclollexyl Carbodiimide) as a condensation agent and covalently binding a photosensitizer Ce6 through amidation; meanwhile, loading a BCRP (Breast Cancer Resistance Protein) inhibitor Ko143; then crossly linking a copolymer FA-PEG-b-PAsp; finally, loading an anti-tumor medicine DOX.
Owner:SECOND AFFILIATED HOSPITAL SECOND MILITARY MEDICAL UNIV

Contrast medium used for glioma targeted magnetic resonance and fluorescence dual modality imaging, and preparation method thereof

The invention provides a contrast medium used for glioma targeted magnetic resonance and fluorescence dual modality imaging, and a preparation method thereof. The contrast medium is composed of an acrylamide monomer, an allyl monmer containing sulfhydryl or carboxyl or amidogen, superparamagnetic iron oxide nanoparticles, a fluorochrome and lactoferrin. The preparation method comprises following steps: the acrylamide monomer and the allyl monmer containing sulfhydryl or carboxyl or amidogen are subjected to polymerization reaction so as to obtain a copolymer nanogel; the superparamagnetic iron oxide nanoparticles are added in polymerization reaction process so as to obtain a superparamagnetic copolymer nanogel; the fluorochrome and lactoferrin and combined via covalent bonds so as to obtain fluorochrome labeled lactoferrin; and the superparamagnetic copolymer nanogel and fluorochrome labeled lactoferrin are combined via covalent bonds so as to obtain the contrast medium used for glioma targeted magnetic resonance and fluorescence dual modality imaging. The contrast medium possesses characteristics such as high specificity, selectivity and contrast effect, and low toxic and side effect; and is capable of realizing dual modality imaging.
Owner:HUAZHONG UNIV OF SCI & TECH

Method of preparing high purity iron oxide for soft magnet using titanium white by product ferrous sulphate

A process for preparing the high-purity iron oxide used as soft-magnetic material from the copperas, which is the by-product of Ti white powder, and ferrous sulfate includes such steps as removing impurities, two-step neutralizing, two-step oxidizing to obtain Fe3O4, filtering, baking and calcining. The technological parameters for said neutralizing and oxidizing steps are also disclosed.
Owner:广西冶金研究院有限公司

Sewage treatment microbial carrier and preparation method thereof

The invention discloses a sewage treatment microbial carrier, which consists of a magnetic carbon fiber bracket and a polypyrrole film layer, wherein microorganisms are fixed on the surface of the polypyrrole film layer; wherein the magnetic carbon fiber bracket is formed by weaving composite fiber bundles, and is obtained through pre-oxidation and carbonization treatment; the composite fiber is apolyacrylonitrile fiber doped with graphene, and magnetic iron oxide nanoparticles are uniformly distributed on the surface and inside the composite fiber. The iron oxide nanoparticles generated in situ have good photocatalytic activity, and can promote local graphitization of the carbon fibers and cooperate with graphene to improve the conductivity of the carbon fibers; the magnetic carbon fiberbracket is used as a working electrode; a polypyrrole film is electrochemically deposited on an iron oxide photocatalyst, so that microorganisms are effectively fixed and cannot be embedded, microorganism loading and proliferation are facilitated, the iron oxide photocatalyst and the microorganisms can be in full contact with pollutants in sewage, photocatalytic degradation and microorganism treatment are synchronously carried out, and the sewage treatment efficiency is greatly improved.
Owner:山东高速环保科技有限公司

High-sensitivity bimodal magnetic resonance contrast agent and preparation method thereof

The invention discloses a preparation method for a high-sensitivity bimodal magnetic resonance contrast agent. According to the preparation method, by means of a method for preparing ferric oleate andmanganese chloride through thermal decomposition, a high-boiling-point solvent is adopted as a reaction medium, oleic acid and oleylamine are used as stabilizers, and therefore manganese oxide embedded iron oxide nanoparticles with narrow particle size distribution and high degree of crystallinity are obtained. The invention particularly relates to a preparation method for modifying the manganeseoxide embedded iron oxide nanoparticles by utilizing the oleic acid/the oleamine, or a preparation method for the biocompatible and water-soluble manganese oxide embedded iron oxide nanoparticles. The preparation method for the high-sensitivity dual-mode magnetic resonance contrast agent has the advantages that the requirements of magnetic resonance imaging for the contrast agent and the characteristics of the Nanotechnology are combined, by means of regulation and control over chemical synthesis, manganese oxide with the T1 contrast capability and superparamagnetic iron oxide nanoparticles with the T2 contrast capability are combined so as to form the manganese oxide embedded iron oxide nanoparticles, and therefore the cooperatively-enhancing dual-mode magnetic resonance contrast effectcan be achieved between the two imaging modes, namely, the T1 imaging mode and the T2 imaging mode.
Owner:BEIJING TECHNOLOGY AND BUSINESS UNIVERSITY

Developing apparatus and electrophotographic image-forming apparatus

A developing apparatus is provided which can suppress a fluctuation in image density in a discontinuous printing mode provided with a pause period. The developing apparatus includes a developer for developing an electrostatic latent image on a photosensitive drum, a developer bearing member for carrying and conveying the developer and a developer layer thickness-regulating unit placed close to the developer bearing member for regulating the amount of the developer carried and conveyed by the developer bearing member, the developer layer thickness-regulating unit being. As the developer, a negatively chargeable, one-component, magnetic toner is used having magnetic toner particles containing a binder resin and a magnetic iron oxide particle, and has a specific saturation magnetization, specific weight-average particle diameter and specific composition. The developer bearing member includes a surface layer containing a binder resin, a quaternary ammonium salt, graphitized particles, and conductive, spherical resin particles, and has a specific surface shape.
Owner:CANON KK

Magnetic black iron oxide

The invention relates to magnetic black iron oxide. A preparation process of the magnetic black iron oxide comprises the following steps of: (1), putting the mixture of ferric salt and ferrite into a container, adding a certain amount of water, and preparing a solution with the iron ion concentration of 1.0-2.0 mol / L; (2), adding ethanol and oleic acid into the container; (3), adjusting the pH of the solution in the container by using ammonia water till the pH is 1.0-1.4, and then, adjusting the pH by using liquid caustic soda till the pH is 7.4-8.1; (4), increasing the temperature of the container filled with a mixed solution after adjusting the pH; (5), filter-pressing, rinsing, drying and crushing at the beginning of increasing the temperature after reacting for 0.8-1.5 hours, and then obtaining the finished product. Because of adopting the technical scheme, the preparation process is lower in reaction temperature and shorter in process period; furthermore, the prepared finished product is higher in purity; the production energy consumption is reduced; the production cost is saved.
Owner:SHENGHUA GROUP DEQING HUAYUAN PIGMENT

siRNA conveying carrier and application thereof

The invention discloses a siRNA conveying carrier. The active ingredient of the conveying carrier is nanaparticles formed by coupling superparamagnetic iron oxide nanoparticles and polyethylene glycol-polyethyleneimine. In addition, the invention also discloses a eukaryotic cell transfection liquid which comprises a composite made from siRNA and the siRNA conveying carrier. The siRNA conveying carrier provided by the invention has the physical and chemical properties of small particle size and suitable surface potential, has good siRNA compounding ability, low cell toxicity and high transfection rate, is a safe and efficient nano carrier with siRNA conveying function and has broad application prospect in siRNA conveying and disease treatment based on RNA interference.
Owner:黄开红 +1

Positively chargeable developer

A positively chargeable developer is provided which is capable of providing stable image quality without causing any image defect even in long-term use. The developer includes at least positively chargeable toner particles each containing at least a binder resin and magnetic iron oxide, silica and an inorganic fine powder. A unconfined yield strength at a major consolidation stress of 5 kPa of the developer is in the range of 0.1 to 2.5 kPa, and a unconfined yield strength at a major consolidation stress of 20 kPa of the developer is in the range of 2.5 to 5.5 kPa.
Owner:CANON KK

Preparation method of magnetic chitosan modified silk fabric

The invention discloses a preparation method of a magnetic chitosan modified silk fabric. The preparation method comprises the following steps: dissolving chitosan in a beaker filled with distilled water, adding glacial acetic acid, putting the beaker in a magnetic stirrer, stirring until the chitosan is completely dissolved and the solution becomes transparent; adding ferric chloride into ethylene glycol, stirring until ferric chloride is completely dissolved and the solution becomes yellow and transparent, adding sodium acetate while stirring until the solution becomes thick and uniform brown yellow to obtain a ferric oxide solution; slowly adding the prepared chitosan solution into the magnetic nano iron oxide solution while stirring until the mixed solution slowly becomes transparent wine red to obtain a magnetic iron oxide chitosan hybrid solution; treating the silk fabric by using the solution on a constant-temperature oscillation dyeing machine, washing and drying to obtain thesilk fabric. The method is rapid and easy to operate, the surface roughness of the treated silk is increased, chitosan-coated magnetic iron oxide nano particles exist on the silk fabric, and adsorption of a natural dye namely anthocyanin is enhanced.
Owner:南通安广美术图案设计有限公司
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