The invention relates to a preparation method and application of a high-purity
rhenium standard sample for GD-MS
component analysis, and belongs to the field of rare
metal analysis. The method comprises the following steps: quantitatively adding corresponding simple substances or compounds of 30
impurity elements of Ag, Al, As, Ba, Be, Bi, Ca, Cd, Co, Cr, Cu, Fe, Ga, K, Mg, Mn, Mo, Na, Ni, Pb, Pt, Sb, Se, Si, Sn, Te, Ti, Tl, W and Zn into an
ammonium rhenate solution, mixing, reducing,
grinding, homogenizing, tabletting, shaping and
sintering to obtain the pure
rhenium standard sample. And carrying out uniformity test and
stability test on 30 elements in the sample, and carrying out accurate valuation. The high-purity
rhenium standard sample obtained through the method is regular in shape, uniform in component, good in stability, accurate in fixed value and convenient to store, and can be used for correction of high-purity rhenium
trace element measurement results and monitoring of instrument and equipment states.