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577 results about "Glycerite" patented technology

A traditional glycerite is a fluid extract of an herb or other medicinal substance made using glycerin as the majority of the fluid extraction medium.

Purification of glycerin

A process for purifying glycerin recovered as a byproduct of biodiesel production comprises heating a glycerin effluent stream containing a low molecular weight alcohol, water and fatty acid esters of the low molecular weight alcohol to cause transesterification of the fatty acid esters to glycerides and additional low molecular weight alcohol. The reaction mixture is sparged with nitrogen to help remove water and low molecular weight alcohol, which drives the transesterification reaction towards glyceride formation. A wash water stream may also be added to the recovered glycerin stream from biodiesel production. Either before or following the transesterification reaction, an oil layer can be separated from the recovered glycerin stream by reducing the pH of the stream to below 7. Following separation of the oil layer and transesterification the glycerin stream is flash distilled to separate glycerin from water, salts, and glycerides.
Owner:SUNOCO INC (R&M)

Process for preparing n-propanol by hydrogenating glycerol

The invention provides a method for preparing normal propyl alcohol by glycerol hydrogenation, wherein glycerite or biodiesel byproduct glycerol which is diluted by glycerol or solvent reacting with hydrogen or gaseous mixture containing hydrogen to generatenormal propyl alcohol, which provides a new way for synthesizing normal propyl alcohol. The present invention can enhance activity of glycerol hydrogenation and selectively generates normal propyl alcohol, also can make normal propyl alcohol united generating with 1,2-propanediol, ethandiol, methylic alcohol and ethyl hydrate, thus its product process program is very flexible. The present invention is characterized in that its technological condition is geniality, raw material is cheap and can be obtained easily and the cost of manufacture is low, which belongs to environment friendly green chemical industry technique.
Owner:SHANGHAI HUAYI NEW MATERIAL

Electronic cigarette smoke solution with herbal tea flavor

ActiveCN104770863ARich taste qualityAppropriate physiological sensationTobacco treatmentFlavorAlcohol
The invention relates to an electronic cigarette smoke solution with the herbal tea flavor. The electronic cigarette smoke solution comprises, by weight, 35-70 parts of propylene glycol, 10-45 parts of edible glycerinum, 0.5-10 parts of a tobacco extract, 0.005-5 parts of a flavoring agent, 0.5-15 parts of a herbal tea flavor agent, 0-5 parts of edible alcohol and 0-10 parts of water. The electronic cigarette smoke solution with the herbal tea flavor contains a herbal tea flavor agent capable of clearing heat of the whistle, the appropriate strength and the full-bodied cigarette fragrance can be provided, the herbal tea flavor is added, a certain health care effect of clearing heat to reduce fire is achieved, and the shortcomings on taste of an electronic cigarette are overcome.
Owner:CHINA TOBACCO GUIZHOU IND

Strength enhancers and method of achieving strength enhancement in an electronic vapor device

InactiveUS20170172204A1Increasing harshnessDesirable balanceTobacco treatmentTobacco devicesGrapefruit oilCayenne pepper
A pre-vaporization formulation pre-vaporization formulation for an e-vaping device, the pre-vaporization formulation including a vapor former including a combination of propylene glycol and glycerol, and an additive including at least one of capsicum, allyl isothiocyanate, piperine, isoeugenol, carvacrol, thymol, menthol, monomenthyl succinate, N-(2-hydroxyethyl)-2,3-dimethyl-2-isopropyl butanamide, horseradish oil, garlic extract, onion oil, black pepper, cayenne pepper, ginger oil, thyme oil, cinnamon bark oil, turmeric, fenugreek, cardamom, rosemary extract, grapefruit oil and andrographis extract.
Owner:AKRIA CLIENT SERVICES LLC

Alcohol-free printing fountain solution and preparation method thereof

The invention discloses an alcohol-free printing fountain solution and a preparation method of the alcohol-free printing fountain solution. The alcohol-free printing fountain solution comprises, by weight, 10-15% of propylene glycol monomethyl ether, 2-4% of ethylene glycol, 4-8% of a citric acid, 0.5-1.5% of sodium hydroxide, 15-25% of glycerinum, 0.1-0.3% of sodium carboxymethyl cellulose, 0.05-0.1% of lauroyl diethanol amine, 0.4-0.6% of liquid tea saponin, 0.3-0.6% of dodecyl dimethyl benzyl ammonium chloride, 0.5-1% of dodecyl glucoside, 0.05-0.1% of 2-ethyl hexanol and 50-55% of water. The alcohol-free printing fountain solution does not contain isopropyl alcohol and is low in toxicity, safe, environmentally friendly, good in printing effect and low in cost, thereby having huge economic benefit and social benefit.
Owner:安徽唯宝印刷科技有限公司

Method for preparing 1,2-dihydroxypropane by glycerine hydrogenation

The invention provides a method for preparing 1, 2- methyl glycol through glycerin hydrogenation. The glycerin, diluted glycerin or side product coarse glycerin of biodiesel mixes with hydrogen gas or hydrogen gas- containing gas, and reacts under catalyst action to produce 1, 2- methyl glycol. The conversion rate is high.
Owner:SHANGHAI HUAYI NEW MATERIAL

Refining process of biodiesel byproduct crude glycerol

The present invention provides a refining process of biodiesel byproduct crude glycerol, and relates to the technical field of chemical product production. The refining process includes diluting, desalting, removing impurity, distilling, decoloring and deflavouring. The high-quality refined glycerine is produced by employing the technologies of sodium oxalate complexing impurity removal and active carbon decoloring and deflavouring. The refining process is simple, high in glycerin yield, high in finished refined glycerin purity, and good in product quality.
Owner:江苏洁美生物能源有限公司

Catalysts for production of biodiesel fuel and glycerol

InactiveUS20090119979A1Inexpensive and commercially availableSimplifies evacuationFatty acid esterificationNitrogen-metal/silicon/boron binary compoundsTrans esterificationBiodiesel
A method of producing biodiesel through the trans-esterification of a triglyceride, comprising mixing a triglyceride, an alcohol, and a catalyst to form a mixture, where said catalyst is non-metal quaternary ammonium hydroxide or non-metal quaternary phosphonium hydroxide, removing volatile components from said mixture, and allowing the remaining mixture to separate into a biodiesel-rich layer and a glycerol-rich layer.
Owner:IMPERIAL PETROLUEM

Method for preparing chitosan complex film using glycerin and stearic acid as plasticizer

The invention discloses a preparation method for chitosan composite membrane, which aims at providing a preparation method for the composite membrane with great toughness and less water and air permeability. The invention comprises the following steps that: the chitosan is dissolved by dilute acetum; the feed liquid ratio of the chitosan and the dilute acetum is 1:40 to 100 (weight / volume), and the chitosan is added with plasticiser, and then water-bath heating is implemented so as to make the chitosan dissolve completely, after that, the room temperature is lowered, so that the membrane solution is obtained; the plasticiser is a combination of the glycerin which accounts for 0.2 percent to 1.0 percent of the acetum in volume percent and the stearic acid which accounts for 0.3 percent to 0.8 percent of the acetum in mass percent. The prepared membrane solution is filtered for removing impurity, and is deaerated for half an hour, and then the membrane solution is poured into a clean glass plate, and is dried to form a membrane at the constant temperature of 40 to 80 DEG C; after the membrane is formed, and then stripping is implemented for generating the chitosan composite membrane. The invention adopts the glycerol and the stearic acid as the plasticiser, the composite membrane is prepared through the use selection, and the composite membrane not only has certain toughness and can keep a lower water and air permeability.
Owner:TIANJIN UNIV OF COMMERCE

Method for using molecular distillation to extract nervonic acid from acer truncatum buge oil

The invention relates to a method for using molecular distillation to extract nervonic acid from acer truncatum buge oil, which obtains the acer truncatum buge oil with acer truncatum buge seeds as raw materials by extracting and pressing; absolute ethyl alcohol or methanol and the acer truncatum buge oil are mixed, then the catalyst is added for reaction, unreacted ethyl alcohol or methanol is removed, glycerine is separated, and fatty acid ester of the acer truncatum buge oil is obtained by rinsing; five-grade molecular distillation is carried out to the fatty acid ester of the acer truncatum buge oil under the condition of different vacuum degrees and temperature so as to obtain the fatty acid ester with the content of nervonic acid ester of more than 80 wt percent; the fatty acid ester is saponated, acid is added to adjust pH value to be 2 to 3, rinsing is carried out so as to lead the fatty acid ester to be neutral, petroleum ether is used for extracting the fatty acid, the petroleum ether is then removed and the product with the content of nervonic acid of more than 80 wt percent is obtained. The invention has the advantages of low operating temperature, simple technique and high content of nervonic acid.
Owner:SHANXI INST OF COAL CHEM CHINESE ACAD OF SCI

Normal atmosphere degreasing crude glycerine pretreatment method for separating wood fiber biomass components

The invention relates to a normal pressure degreased crude glycerin pre-treatment method for realizing the separation of components of wood fiber biomass. The method comprises the following steps: the wood fiber biomass and the degreased crude glycerin are evenly mixed; under atmospheric pressure or micro-pressure, by auto-catalysis of the glycerin or addition of catalyst, the mixture is heated up and cooked; after cooking, the mixture is cooled down and the components of the mixture are fully dissolved; after filtering and washing, glycerin cellulose with good enzymolysis property is obtained; the filtrate is regulated to be weak acid, condensed, deposited in ethanol, and filtered for the second time to obtain semi-cellulose components; and the secondary filtrate is reclaimed by the ethanol, regulated to be strong acid, deposited and centrifuged to obtain the glycerin lignose component. The method has the advantages of not only facilitating economic utilization of low-grade crude glycerin, but also solving the potential danger of organic solvent such as low-boiling point ethanol in the magnification process of the pulping process, such as high pressure operation and easy burning and explosion of volatile gases.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI

Liquor-fragrance E-cigarette nicotine liquid

InactiveCN104489905AImprove the defects that cannot meet the needs of consumersMeet needsTobacco treatmentFlavorLiquid smoke
The invention relates to liquor-fragrance E-cigarette nicotine liquid. The liquor-fragrance E-cigarette nicotine liquid is made by mixing, by weight, 1 to 30% of tobacco extract, 0.5 to 10% of tobacco flavor, 0.5 to 15% of Chinese liquor, 0.5 to 10% of taste fragrance conditioner, 1 to 15% of deionized water, 1 to 25% of edible glycerin and the balance of propylene glycol. The defect that the existing E-cigarette is unable to meet the needs of consumers for taste and fragrance is overcome; the liquor-fragrance E-cigarette nicotine liquid has fragrant aroma, has the tobacco fragrance and the liquor fragrance, has fine and soft taste, has lingering liquor charm and tobacco fragrance, feels good and can substantially meet the needs of consumers.
Owner:CHINA TOBACCO GUIZHOU IND

Sea-buckthorn perilla seed oil soft capsule having function of assisting blood-fat reduction and preparation method thereof

The invention relates to a preparation method of a health-care product having a function of assisting blood-fat reduction, in particular to a preparation method of a sea-buckthorn perilla seed oil soft capsule having a function of assisting the blood-fat reduction. The sea-buckthorn perilla seed oil soft capsule consists of a capsule casing and contents and is characterized in that the capsule casing consists of, by weight, edible gelatine 40%-45%, glycerol 18%-25% and pure water 35%-40%, and the contents include, by weight, sea-buckthorn seed oil 30%-50% and perilla seed oil 50%-70%. In addition, the preparation method comprises the steps of firstly adopting a supercritical CO2 fluid extraction technology to respectively extract the sea-buckthorn seed oil and the perilla seed oil, evenly mixing the sea-buckthorn seed oil and the perilla seed oil according to formula amount and manufacturing a mixture into soft capsules in a dropping-pill mode, wherein the sea-buckthorn perilla seed oil soft capsule does not contain solvents and other impurities and contains abundant unsaturated fatty acid, vitamin E and various nutritional health-care ingredients. A health-care food functional experiment and a toxicology safety evaluation test prove that the sea-buckthorn perilla seed oil soft capsule has the function of assisting the blood-fat reduction and is suitable for long-term taking of people with high blood fat.
Owner:甘肃省轻工研究院有限责任公司

Polyvinyl chloride synthetic leather for luggage and manufacturing method thereof

The invention discloses polyvinyl chloride synthetic leather for a luggage. The leather comprises a surface layer, a foaming layer, a bonding layer and fluffing cloth. The surface layer is slurry prepared from the following raw materials in parts by weight: 40-50 parts of SG-3 PVC (Polyvinyl Chloride) resin, 70-80 parts of SG-5 PVC resin, 30-35 parts of glycerol triacetate, 10-15 parts of epoxidized soybean oil, 20-25 parts of glycerol triglycerate, 5-6 parts of PVC color cream, 1-2 parts of bimercapto iso-octyl acetate di-n-octyl tin, 5-10 pats of zinc oxide and 5-10 parts of modified attapulgite. Through improvement of formula and process provided by the invention, the flexibility of the synthetic leather is enhanced, and the synthetic leather has a natural and comfortable handfeel similar to that of natural leather. The synthetic leather is not easy to damage or tear within 3-5 years, and suitable for use in lug gages.
Owner:HEFEI ANSHAN COATING FABRICS

Artificial zero-thans fatty acid cream

The invention discloses artificial zero-thans fatty acid cream which is simple in production process, good in taste, good in fermentation and resistant to storage and a preparing method thereof. The preparing method includes the following steps that oil phase is prepared; after natural coconut oil, palm stearin, shea butter and pomegranate seed oil are evenly mixed, double glycerate, lecithin and vitamin E are added to the mixture, the mixture is heated till the grease is totally melt, and the mixture is evenly mixed for use; water phase is prepared, wherein milk powder and salt are added to deionized water to be fully stirred, and the mixture is made to be totally dissolved to be the even water phase for use; the oil phase and the water phase are added to an emulsification tank to be emulsified according to the weight ratio of 8:2, meanwhile ascorbic acid palm ester is added to the mixture, stirring is conducted while the ascorbic acid palm ester is added, the emulsifying temperature ranges from 62 DEG C to 65 DEG C, and the time ranges from 30 min to 33 min; the emulsified lactescence is placed into a shock cooling kneading machine, cooling is conducted while kneading is conducted, the kneaded lactescence is cooled and formed, and artificial cream products are obtained.
Owner:COCONUT RES INST OF CHINESE ACAD OF TROPICAL AGRI SCI

Anhydrous antiperspirant and deodorant compositions containing solid vitamin B3 particulates and glycerin

InactiveUS7033579B1High visible residueReduces visible residueCosmetic preparationsToilet preparationsParticulatesDeodorant
Disclosed are anhydrous antiperspirant and deodorant compositions that comprise from about 0.1% to about 30% by weight of an antiperspirant or deodorant active; from about 0.01% to about 20% by weight of a solid, water-soluble Vitamin B3 material; from about 0.1% to about 40% by weight of a suspending agent; from about 0.1% to about 2.0% by weight of glycerin; and from about 10% to about 99% by weight of an anhydrous carrier liquid other than and in addition to the glycerin. The anhydrous compositions have lower visible residue on the applied areas of the skin even though they also contain relatively high residue solids in the form of solid, water-soluble, Vitamin B3 materials. The compositions also provide for a dry, silky feeling during or after application.
Owner:THE PROCTER & GAMBLE COMPANY

Phenol-formaldehyde resin by colophony modified with alkyl phenol being mixed and its preparation method

InactiveCN1462759AImprove solubilityGood oil meltingSolubilityAlkylphenol
A rosin modified mixed alkylphenol-phenolic resin is prepared from reaction between p-tert-octylphenol, p-nonylphehnol, dodecylphenol and formaldehyde in alkaline condition, modifying by rosin, and esterifying by glycerin and then trihydroxymethyl propane. Its advantages are high soft point, good viscoelasticity, and excellent solubility in fatty hydrocarbon band oil. It can be used for high-speed print color ink.
Owner:山西省应用化学研究所

Method for refining crude glycerine being by-product of biodiesel

The invention relates to a method for refining crude glycerine being a by-product of biodiesel, which comprises the following steps: the crude glycerine produced during the production process of biodiesel is added into an acidification reactor, dilute acid is utilized to adjust the pH to be faintly acid, and acidizing is performed for 30-60 minutes at the temperature of 45-50 DEG C; upper-layer acid oil returns to a biodiesel preparation system and is used as the biodiesel production raw material, the lower-layer glycerine solution enters into a neutralized reactor, a dilute aqueous alkali is used for adjusting the pH to alkalescence, and standing is performed for layering; the produced sediment is discharged from the bottom of the reactor, and various impurities in the obtained dilute glycerite are removed via an ion exchange column to obtain a glycerinum dilute solution; the glycerinum dilute solution enters into a short-range pipeline evaporator, and thin layer efficient rapid continuous evaporation and concentration are performed to obtain high-purity glycerine. The method has the following benefits: through the combination of ion exchange and the pipeline thin layer evaporation technology, the flow is simple, the efficiency is high, and the costs for recycling and refining glycerine and preparing biodiesel are reduced.
Owner:QINGDAO JIENENG ENERGY SAVING ENVIRONMENTAL PROTECTION TECH

Technology for preparing biodiesel by food and beverage waste oil

The embodiment of the invention discloses a method for manufacturing biodiesel, which is characterized in that the method comprises the following steps: filtering food and beverage waste oil by an oil filter; then, heating the waste oil for dewatering; carrying out esterification reaction on the pretreated food and beverage waste oil and methanol or ethanol in the existence of catalysts of basic ionic liquid; carrying out distillation for recovering the rest methanol in the reaction; separating the basic ionic liquid catalysts and the glycerin phase in the reaction lower layer liquid to obtain coarse ester; washing obtained materials by hot water to neutral materials after the coarse ester is washed by saturated sodium chloride solution water; and finally, carrying out heating, stirring and dewatering to obtain finished products of biodiesel. The basic ionic liquid catalysts have the molecular formula as the accompanying drawing.
Owner:LOGISTICAL ENGINEERING UNIVERSITY OF PLA

PET (polyethylene glycol terephthalate) fiber/ceramic fiber composite sound absorbing cotton and preparation method of PET fiber/ceramic fiber composite sound absorbing cotton

The invention discloses PET (polyethylene glycol terephthalate) fiber / ceramic fiber composite sound absorbing cotton, which is prepared from the following ingredients in parts by weight: 70 to 80 parts of PET fibers, 40 to 50 parts of ceramic fibers, 10 to 15 parts of emulsifying agents OP-4, 5 to 10 parts of peregal O-15, 80 to 100 parts of PP (propene polymer), 30 to 40 parts of SBR (styrene butadiene rubber), 15 to 20 parts of nanometer bauxite, 10 to 15 parts of modified kieselguhr, 2 to 3 parts of stearic acid, 5 to 8 parts of glycerol triglycerin acid ester, 4 to 6 parts of triphenyl phosphate, 2 to 3 parts of microcrystalline wax, 1 to 2 parts of vinyl (beta-methoxyethoxy) trisilane, 2 to 3 parts of zinc stearate, 1 to 2 parts of lead sulfate tribasic, 0.5 to 1.5 parts of anti-aging agents ODA (octyl decyl adipate) and 1 to 2 parts of antioxidants 168. The sound absorbing cotton prepared by the invention has the advantages that the appearance evenness is good, the thickness is uniform, the hand feeling is soft, the product bonding degree is good, the tensile performance is high, the sound absorbing performance is excellent, the flame retardant effect is good, and the like.
Owner:芜湖跃飞新型吸音材料股份有限公司

Water-dispersible transparent astaxanthin emulsion and preparation method

The invention belongs to dosage form technology of functional additives, and particularly relates to a water-dispersible transparent astaxanthin emulsion and a preparation method. The astaxanthin emulsion comprises an oil phase, a water phase and an emulsifier, the oil phase is an astaxanthin solution and comprises astaxanthin and a solvent, mass-volume concentration of the astaxanthin solution is 1-30 mg / mL, the water phase is water or a mixture of glycerin and water, the solvent is edible oil, a volume ratio of the oil phase to the emulsifier is 1:3:3:1, and a volume ratio of the water phase to mixed liquid of the oil phase and the emulsifier is greater than or equal to 1:9. The preparation method includes: preparing the oil phase, preparing the water phase, and preparing the emulsion. The water-dispersible astaxanthin emulsion has high solubility and water dispersity, bioavailability of the water-dispersible astaxanthin emulsion is improved, and various physiological active functions of the water-dispersible astaxanthin emulsion are brought into effective play.
Owner:CHINA AGRI UNIV

Method for preparing micropore polymer electrolyte by using glyoxaline cation-intercalated montmorillonite

The invention provides a method for preparing high thermal stability microporous polymer electrolyte from imidazole cation intercalation montmorillonite. In the method, firstly, the imidazole cation intercalation montmorillonite is used to prepare high thermal stability montmorillonite; secondly, by the phase transition method, polyvinylidene fluoride, polyethylene glycol and the imidazole cation intercalation montmorillonite are added to the mixed solution of N,N-dimethylformamide and glycerin and violently stirred at a temperature of between 70 and 85 DEG C for 6 to 10 hours, the obtained evenly mixed solution is poured on a clean and preheated glass plate and vacuum dried at a temperature of between 100 and 130 DEG C for 30 t0 40 hours to obtain a polymer membrane with the thickness of between 100 and 300 micrometers; and finally the polymer membrane is soaked in electrolyte in a simple glass box for 24 to 72 hours to obtain the microporous polymer electrolyte. Tests show that the electrical conductivity of the microporous polymer electrolyte prepared by the method reaches 1.6 to 6.15mS / cm, and the residual mass of the dry membrane at a temperature of 400 DEG C(N2) is between 60 and 70 percent.
Owner:NORTHWEST NORMAL UNIVERSITY

Coenzyme Q10 composite soft capsule and preparation method thereof

The invention relates to a coenzyme Q10 composite soft capsule and a preparation method thereof, belonging to the technical field of health-care foods. The coenzyme Q10 composite soft capsule comprises a capsule shell and capsule content, wherein the capsule content comprises the following raw materials in proportions by weight: coenzyme Q10: zinc lactate: sodium selenite: vitamin E: corn oil =1:(0.8-1.6):(0.001-0.005):(1.5-3.5):(15-25); and the soft capsule shell comprises the following ingredients of gelatin, glycerol and pure water. The preparation method comprises the following steps of: preparing the capsule materials: heating the gelatin, the glycerol and the water in water bath to 50-95 DEG C for dissolving according to the proportions of (0.5-2):(0.2-0.8):(0.5-1.5) , and preserving the temperature at 45-80 DEG C; taking the zinc lactate and the sodium selenite according to the formula amount, evenly mixing in an equivalent progressive-increase way, then evenly mixing with the coenzyme Q10, and carrying out ultramicro crushing; putting the natural vitamin E and the corn oil in and stirring in 500-2000rpm to obtain mixed oil, adding fine mixed powder and evenly stirring; and preparing the coenzyme Q10 composite soft capsule by using an auto-rotating capsule rolling machine. the invention has the advantage of greatly increasing the stability of the coenzyme Q10.
Owner:BEIJING DAWN AEROSPACE BIO TECH
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