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33results about How to "Strong retardation" patented technology

High-temperature-resistant and large-temperature-difference-resistant cement grout for well cementation in oil field

ActiveCN105694832AExcellent dehydration performanceGood adaptabilityDrilling compositionSolid phasesSilica fume
The invention relates to high-temperature-resistant and large-temperature-difference-resistant cement grout for well cementation in an oil field. The cement grout is prepared from components of raw materials in parts by weight as follows: 600 parts of G-grade oil well cement, 30-36 parts of an HS101L fluid loss agent, 8-20 parts of an HS201L retarder, 1.8 parts of an HS-301S dispersant, 150 parts of quartz sand, 30 parts of silica fume, 1.8 parts of an HS-XF1S suspension stabilizer, 280-300 parts of water and 1 part of bis(2-ethylhexyl) sulfosuccinate sodium salt, wherein the grain size of the quartz sand is 80-120 meshes, the grain size of the silica fume is 300-400 meshes, and the content of silicon dioxide is 90% or higher. Liquid-phase raw materials are added to a grout mixing container and mixed uniformly; solid-phase substances are added to a solid-phase container and stirred uniformly, the solid-phase mixture is added to the grout mixing container, finally, a defoaming agent is added, and the mixture is stirred uniformly. The cement grout can be used under the condition of 50-180 DEG C, has prominent large-temperature-difference-resistant performance and can effectively avoid a super-retarding phenomenon caused by large temperature difference.
Owner:CHINA PETROCHEMICAL CORP +2

Macroporous concrete containing low grade recycled aggregates and preparation method of concrete

The invention discloses macroporous concrete containing low grade recycled aggregates. The macroporous concrete containing low grade recycled aggregates is prepared from the following raw materials: cement, water, low grade recycled aggregates, modified starch and a sugar retarder, wherein the grain size of the low grade recycled aggregates is 5-16mm, and the bulk density is 700-900kg / m<3>. The macroporous concrete containing low grade recycled aggregates is further prepared from additional water, the use level of which is calculated according to the follow formula: delta W=mgr*wgr, wherein delta W is the use level of the additional water of the macroporous concrete containing low grade recycled aggregates; mgr is the use level of the low grade recycled aggregates and wgr is 1h water absorption of the low grade recycled aggregates. According to the invention, the grade recycled aggregates are applied to preparation of the macroporous concrete, so that the mixture state satisfies the using demand under the condition that an additive in an extra amount is not added by virtue of adjusting the raw materials and matching with the sugar retarder and modified starch.
Owner:北京东方建宇混凝土科学技术研究院有限公司

Temperature response type amphoteric polymer retarder and preparation method thereof

The invention relates to an oil well cement retarder in the field of oil gas well exploration and development and a preparation method of the oil well cement retarder. The amphoteric polymer retarder is prepared from, by mass, 10-20% of dimethyldiallylammonium chloride (DMDAAC), 20-30% of 2-acrylamide-2-methyl propane sulfonic acid (AMPS), 30-50% maleic anhydride (MA) and 10-30% of acrylic amide (AM). Due to lateral groups in an amphoteric polymer structure, a self-response type response can be made for the temperature of surroundings, and the temperature adaptability is high. The delayed coagulation of cement paste within the whole temperature region with 70 DEG C and 140 DEG C as the upper and lower end temperatures of a cementing well section is achieved, the thickening time of the cement paste and the retarder added amount are in the good linear relation, the right-angled thickening effect is obvious, the temperature and the added amount sensitivity are low, and the cement paste comprehensive performance can meet the requirement for well cementation construction; in addition, the retarder is simple in synthesis technology, low in cost, high in operability and capable of achieving large-scale production and application.
Owner:SOUTHWEST PETROLEUM UNIV

Method for preparing food browning inhibitor from cedar pine needles

The invention discloses a method for preparing a food browning inhibitor from cedar pine needles. The method is characterized by comprising the following steps: smashing dried cedar pine needles, adding normal hexane according to the material-to-liquid ratio of 1g: (10-20mL), vibrating at room temperature for 12-24h and filtering to separate a normal hexane extracting liquid; recovering the degreased pine needles, adding 50-70wt% methanol as an extracting agent according to the material-to-liquid ratio of 1g: (10-30mL), vibrating at room temperature for 24-48h, separating a supernatant, concentrating and drying the supernatant to obtain a methanol extract with the yield of 15-22%; suspending the methanol extract into 20-30mL of 50wt% methanol, carrying out chromatography by using a macroporous adsorption resin DiaionHP-20 chromatographic column, carrying out gradient elution at the flow speed of 3-5mL / min by using water and methanol with the concentrations being respectively 0wt%, 15wt%, 30wt%, 40wt%, 60wt% and 100wt%, collecting the 40wt% methanol eluant, concentrating and drying to obtain the food browning inhibitor, separating and purifying by using a high performance liquid chromatography; and obtaining the effective component, i.e., 2R, 3R-dihydromyricetin of the food browning inhibitor.
Owner:SICHUAN UNIV

Preparation method of starch sulfonate

The invention belongs to the technical fields of chemical industry and concrete construction materials. In order to solve the problems of high slump constant time loss and lower flowability in the concrete, the invention provides a preparation method of starch sulfonate. The preparation method comprises the following steps: dissolving dextrin prepared from starch or directly purchased dextrin in water, heating to react by using water as a dispersing agent and sodium bisulfite as a sulfonating agent, and regulating the pH value to 7 with sodium hydroxide to obtain a liquid which is the starch sulfonate. The invention uses the method for preparing starch sulfonate by using water as the medium and sodium bisulfite as the sulfonating agent for the first time, which is different from the preparation method by using dichloromethane or any other organic solvent as the medium in the prior art. The method has the advantages of simple technique, environment friendliness and no pollution emission, and is beneficial to industrial production. The product has favorable synergic dispersion properties for cement particles, solves the problems of poor slump retaining effect and poor workability in the existing retarder for concrete, use of toxic solvents in the preparation process, and difficulty in treating sulfonating agent byproduct chlorine ions. The invention provides a novel preparation method of starch sulfonate.
Owner:CHINA RAILWAY 12TH BUREAU GRP +1

Phosphorus slag based environmentally-friendly building material and preparation method thereof

The invention discloses a phosphorus slag based environmentally-friendly building material and a preparation method thereof. The phosphorus slag based environmentally-friendly building material comprises the following components in parts by mass: 14.61 to 44.08 parts of phosphorus slag powder, 1.11 to 18.72 parts of building waste residue powder, 1.11 to 6.24 parts of sialic sphere powder, 1.11 to3.12 parts of nanometer silex, 2.10 to 8.46 parts of an alkaline activator, 20.81 to 66.51 parts of sand, 11.08 to 16.53 parts of water and 0.22 to 1.17 parts of an efficient polycarboxylate superplasticizer. The phosphorus slag based environmentally-friendly building material is low in cost, simple in preparation technology and short in maintenance time.
Owner:中建西部建设贵州有限公司

Preparation method of high-temperature-resistant modified retarder

The invention relates to a preparation method of a high-temperature-resistant modified retarder, belonging to the technical field of sealing materials. According to the technical scheme, a silicon carbide whisker is utilized for modification, and a laminar matrix material is prepared through coating, so that on one hand, a polymer is endowed with the rigidity and thermal stability of an organic material, namely a laminar matrix substance, through the addition of the laminar matrix substance; on the other hand, the partial polymer is inserted among laminar inorganic material slice layers, the partial thermal decomposition effect is effectively shielded by the slice layer structures, and the micromolecule motion caused during the thermal decomposition is impeded, so that the polymer represents good heat stability. According to the retarder prepared by virtue of the scheme, polar groups are effectively released to the surface of cement particles to form an adsorption layer, and the adsorption layer is capable of preventing the contact between the cement and water so as to decrease the cement hydration speed and achieve a retarding effect, so that the heat stability of the material isimproved.
Owner:蒋留平

Preparation method of starch sulfate and application of starch sulfate as cement additive

The invention relates to a preparation method of starch sulfate and application of the starch sulfate as a cement additive. The invention relates to the technical field of fine chemical engineering and concrete admixtures. For the first time, the starch sulfate is prepared by taking sodium hydrogen sulfate or sulfuric acid or a composition aqueous solution of sodium hydrogen sulfate and sulfuric acid as a sulfonating agent by a semi-dry method, and synthesis raw materials comprise starch, the sulfonating agent and an inorganic alkali. The synthesis process comprises the following steps: preparing the sulfonating agent; mixing the sulfonating agent with the starch; heating and esterifying the mixture; and performing esterification product base neutralization. The method disclosed by the invention is different from a method for preparing the starch sulfate by taking concentrated sulfuric acid, chlorosulfonic acid, sulfur trioxide and the like as sulfonating agents in the prior art; the method has the advantages of simple preparation process, no emission of three wastes, low raw material cost, low equipment requirements and the like. The product prepared by the invention can be directly used as a super-retarding superplasticizer or retarder, and has the advantages of high water reducing rate, good retarding effect, strong cohesiveness, bleeding resistance, segregation resistance and the like; and if the starch sulfate is compounded with polycarboxylate superplasticizers and the like, an obvious synergistic effect can be generated.
Owner:殷鸽

A kind of preparation method of starch sulfonate

The invention belongs to the technical fields of chemical industry and concrete construction materials. In order to solve the problems of high slump constant time loss and lower flowability in the concrete, the invention provides a preparation method of starch sulfonate. The preparation method comprises the following steps: dissolving dextrin prepared from starch or directly purchased dextrin in water, heating to react by using water as a dispersing agent and sodium bisulfite as a sulfonating agent, and regulating the pH value to 7 with sodium hydroxide to obtain a liquid which is the starch sulfonate. The invention uses the method for preparing starch sulfonate by using water as the medium and sodium bisulfite as the sulfonating agent for the first time, which is different from the preparation method by using dichloromethane or any other organic solvent as the medium in the prior art. The method has the advantages of simple technique, environment friendliness and no pollution emission, and is beneficial to industrial production. The product has favorable synergic dispersion properties for cement particles, solves the problems of poor slump retaining effect and poor workability in the existing retarder for concrete, use of toxic solvents in the preparation process, and difficulty in treating sulfonating agent byproduct chlorine ions. The invention provides a novel preparation method of starch sulfonate.
Owner:CHINA RAILWAY 12TH BUREAU GRP +1

Method for preparing food browning inhibitor from cedar pine needles

The invention discloses a method for preparing a food browning inhibitor from cedar pine needles. The method is characterized by comprising the following steps: smashing dried cedar pine needles, adding normal hexane according to the material-to-liquid ratio of 1g: (10-20mL), vibrating at room temperature for 12-24h and filtering to separate a normal hexane extracting liquid; recovering the degreased pine needles, adding 50-70wt% methanol as an extracting agent according to the material-to-liquid ratio of 1g: (10-30mL), vibrating at room temperature for 24-48h, separating a supernatant, concentrating and drying the supernatant to obtain a methanol extract with the yield of 15-22%; suspending the methanol extract into 20-30mL of 50wt% methanol, carrying out chromatography by using a macroporous adsorption resin DiaionHP-20 chromatographic column, carrying out gradient elution at the flow speed of 3-5mL / min by using water and methanol with the concentrations being respectively 0wt%, 15wt%, 30wt%, 40wt%, 60wt% and 100wt%, collecting the 40wt% methanol eluant, concentrating and drying to obtain the food browning inhibitor, separating and purifying by using a high performance liquid chromatography; and obtaining the effective component, i.e., 2R, 3R-dihydromyricetin of the food browning inhibitor.
Owner:SICHUAN UNIV

Grouting Binder and Its Performance Parameter Testing Method

The invention discloses a grouting compound and a performance parameter detection method thereof. The grouting compound comprises the following components in parts by weight: 500-1500 parts of cement,500-3000 parts of aggregate, 10-150 parts of an admixture, 5-150 parts of rubber powder, 1-20 parts of a high-efficiency water-reducing agent, 1-10 parts of an anti-cracking capsule, 0.1-5 parts of adefoaming agent, 0.02-2 parts of a plastic expanding agent, 20-150 parts of a hardening expanding agent, 0.5-10 parts of an early strength agent, 0.5-5 parts of a slump retaining agent and 0.5-5 parts of fiber, wherein mixing water is 0.10-0.35 times of powder. Through a matching ratio, the grouting compound has very high early strength and superstrong coagulation retardation, has 90min fluiditybeing better than the discharge flow performance of the conventional grouting material, and can fully densify and infiltrate a concrete interface; in addition, because of good bonding performance, a circumferential construction joint constructed on a previous slab and an open end of the previous slab are repaired better to obtain overall bonding strength, so that mechanical properties of a liningare greatly improved; the defects that when the conventional grouting material is used for repairing, an original base surface is required to be chiseled and be brushed with an interface agent are overcome, and a concrete structure can be directly repaired.
Owner:北京鸿锐嘉科技发展有限公司
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