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34results about How to "Small residual current" patented technology

Production method and application of nano-platinum doped/enzyme modified carbon paste electrode

The invention discloses a production method and an application of a nano-platinum doped / enzyme modified carbon paste electrode. The method is characterized in that a carbon paste electrode is doped with nano-platinum ions, and comprises the following steps: mixing carbon nanotubes with graphite powder with 1-ethyl-3-methylimidazole tetrafluoroborate as an adhesive to prepare a carbon paste electrode, and modifying the carbon paste electrode with methyltransgerase to obtain the nano-platinum doped / enzyme modified carbon paste electrode. Compared with common carbon paste electrodes, the nano-platinum doped / enzyme modified carbon paste electrode has 1-2 times rising conductivity, wide electrochemical window, simple production method, low cost, easy updating of the surface, and small residual current; the electrode can be used to rapidly detect SAM in a sample, so a detection method using the electrode has the advantages of high sensitivity, good selectivity, short response time and less interference, is better than other detection methods, and is a simple, rapid and easy SAM determination method; and an immobilized methyltransgerase electrode sensor made in the invention has the advantages of low cost, simple production process, good specificity and automatic onsite determination realization potential.
Owner:UNIV OF JINAN

Preparation method of quantum dot/enzyme compounded carbon paste electrode for detecting SAM (S-Adenosylmethionine)

The invention discloses a preparation method of a quantum dot/enzyme compounded carbon paste electrode for detecting SAM (S-Adenosylmethionine). The preparation method is characterized by comprising the following steps of doping water-soluble CdZnTe quantum dots and transmethylase in a carbon paste electrode; by taking 1-ethyl-3--methylimidazolium hexafluorophosphate as an adhesive, mixing a carbon nano-tube with graphite powder to prepare the carbon electrode, so as to obtain the quantum dot/enzyme compounded carbon paste electrode; compared with an ordinary carbon paste electrode, the quantum dot/enzyme compounded carbon paste electrode has the advantages of conducting property improved by 1 to 2 times, wide electrochemical window, simple preparation method, low cost, easy update for surface, low residual current and the like; the eelctrode can be used for quickly detecting the SAM in a sample; the method has the characteristics of high sensitivity, good selectivity, short response time and low interference, is superior to other detection methods, and is a determination method with simpleness, quickness, convenience and feasibility for the SAM. A fixed methyltransferase electrode sensor prepared by the preparation method disclosed by the invention is low in cost, simple in preparation process and good in specificity, and has the possibility of realizing automated field determination.
Owner:UNIV OF JINAN

Preparation method of titanium nitride/carbon nano tube composite paste electrode sensor

The invention discloses a preparation method of a titanium nitride / carbon nano tube composite paste electrode sensor. The preparation method is characterized by comprising the steps of: processing a carbon nano tube by using sulphuric acid and periodate potassium, so that a pre-processed carbon nano tube is obtained; preparing a composite adhesive by adopting 1-butyl-1-methyl pyrrole trifluoromethylsulfonate and cellulose; and then, adding the following components into an agate mortar in percentage by weight: 36-42% of nano titanium nitride, 28-32% of the pre-processed carbon nano tube, 12-16%of the composite adhesive, and 15-18% of liquid paraffin, uniformly grinding to form a carbon paste, putting the carbon paste into a glass tube, wherein the glass tube is connected to a conducting wire; the inside diameter of the glass tube is phi5 mm; and thus, the titanium nitride / carbon nano tube composite paste electrode sensor is prepared. Compared with the ordinary carbon paste electrode, the electrical conductivity of the carbon paste electrode prepared in the invention is increased by 6-8 times; the carbon paste electrode prepared in the invention has the advantages of being wide in electrochemical window, simple in preparation method, low in cost, easy to update the surface, low in residual current, high in paracetamol detection sensivity, good in selectivity and the like.
Owner:UNIV OF JINAN

Production method of molecularly imprinted composite paste electrode sensor for detecting ribavirin

The invention relates to a production method of a molecularly imprinted composite paste electrode sensor for detecting ribavirin. The production method comprises the following steps: producing a nanodysprosium nitride / nano strontium titanate / graphene oxide composite paste electrode; preparing a ribavirin molecularly imprinted polymer: in an oxygen-free atmosphere, taking aconitic acid as a functional monomer, taking methylene bisacrylamide as a cross-linking agent, taking azobisisoheptonitrile as an initiator and taking ribavirin as a template to carry out a cross-linking polymerization reaction to prepare the ribavirin molecularly imprinted polymer; and producing a composite paste electrode sensor: dropwise adding a ribavirin molecularly imprinted polymer modification liquid into the nano dysprosium nitride / nano strontium titanate / graphene oxide composite paste electrode by adopting a dispensing method, volatilizing a solvent, and removing template molecules to obtain the composite paste electrode sensor. According to the method, a molecular imprinting technology, a layer-by-layer self-assembly method and a dispensing method are combined, and the produced molecular imprinting composite paste electrode sensor is good in response performance, good in selectivity and high in sensitivity.
Owner:INNER MONGOLIA UNIV OF SCI & TECH

PTC (Positive Temperature Coefficient) ceramic thermistor

The invention relates to a PTC ceramic thermistor, which is produced with barium carbonate as base material, the purity of the barium carbonate is 99.5 to 99.99 percent, the granularity of the barium carbonate is 0.1 to 2 microns, and the percentages of materials by weight are as follows: 57.53 percent of electron-level barium carbonate; 11.83 percent of electron-level strontium carbonate; 0.4321 percent of electron-level yttrium oxide; 0.4013 percent of electron-level silicon oxide; 30.41 percent of electron-level titanium oxide; and 0.417 percent of electron-level manganese oxide. The PTC ceramic thermistor has the characteristics of high voltage withstanding, low aftercurrent, low power, high reliability, long service life and the like, and is safe to use.
Owner:DONGGUAN YUCHI ELECTRONICS

Fast-response thermistor and application thereof

The invention discloses a fast-response thermistor and application thereof and relates to the technical field of PTC thermistors and application thereof. The fast-response thermistor is composed of polysiloxane, polycarbonate, epoxy resin, PVP, a carbon-based material, metal fibers, silicon dioxide, a fire retardant, an antioxidant, an anti-ultraviolet agent and lubricant. PVP is prepared into flaky xerogel, and a carbon skeleton penetrating through the whole thermistor is obtained after carbonization. The actuation time is effectively shortened, rapid response can be achieved, residual current is reduced, the safety of the thermistor is improved, excellent mechanical performance and corrosion resistance are achieved, and the application range is wide.
Owner:ANHUI NINGGUO TIANCHENG ELECTRICAL APPLIANCES

Thermistor medium material and preparation method thereof

The invention discloses thermistor medium material and a preparation method thereof. The thermistor medium material is prepared from the following raw materials in parts by weight: 80 to 85 parts of BaTiO3 (barium titanate), 10 to 20 parts of Sb2O3 (antimonous oxide), 5 to 12 parts of Co2O3 (cobalt sesquioxide), 1 to 9 parts of SrCO3 (strontium carbonate), 2 to 6 parts of MnO2 (manganese dioxide), 2 to 8 parts of Cr2O3 (chromium sesquioxide), 3 to 5 parts of SnO2 (stannic oxide), 2 to 10 parts of SiO2 (silicon dioxide), 2 to 10 parts of CeO2 (cerium dioxide), 2 to 8 parts of ZrO2 (zirconium oxide), and 3 to 10 parts of Y2O3 (yttrium oxide). The thermistor medium material has the advantages that the service life is prolonged, the cost is low, the preparation cost is simple, the material cost is greatly reduced, and the energy-saving and environment-friendly requirements are met.
Owner:ANHUI NINGGUO TIANCHENG ELECTRICAL APPLIANCES
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