Patents
Literature
Hiro is an intelligent assistant for R&D personnel, combined with Patent DNA, to facilitate innovative research.
Hiro

186results about How to "Improve elution" patented technology

Drug eluting ocular implant

Disclosed herein are drug delivery devices and methods for the treatment of ocular disorders requiring targeted and controlled administration of a drug to an interior portion of the eye for reduction or prevention of symptoms of the disorder. The devices are capable of controlled release of one or more drugs and may also include structures which allows for treatment of increased intraocular pressure by permitting aqueous humor to flow out of the anterior chamber of the eye through the device.
Owner:DOSE MEDICAL CORP

Method for extracting and purifying cannabidiol from China-hemp

The invention belongs to the technical field of extraction and purification of plant ingredients and particularly relates to a method for extracting and purifying cannabidiol from China-hemp. In the method, an ingredient of cannabidiol is extracted from floral leaves in a mature period of the China-hemp according to a supercritical CO2 extraction technique, a cannabidiol extract is further purified by macroporous adsorbent resin and a rapid purification system, a cannabidiol content of an obtained product is 98% or higher, and the cannabidiol product does not contain a psychotoxic ingredient tetrahydrocannabinol. According to the method, a chemical organic solvent is not used in an extraction process, so that the method is environment-friendly and is low in toxicity and high in efficiency; the loss of cannabidiol in an adsorption elution process is reduced in a purification process, so that the impurity ingredients such as tetrahydrocannabinol and the like are effectively removed, and the use of an organic regent is decreased, so that the purification cost is lowered, and the environmental pollution is reduced. The product is high in yield and purity, and the requirement for development of a value-added product of the China-hemp, in particular to the market requirement of the active ingredient of the cannabidiol product in the China-hemp, can be met, and especially, the cannabidiol product has the great application advantage in the pharmaceutical field.
Owner:DAQING BRANCH OF HEILONGJIANG ACAD OF SCI

Efficient acidic oil sludge decomposing agent, and preparation method and application thereof

The invention discloses an efficient acidic oil sludge decomposing agent, comprising the following component materials in percentages by weight: 1-15% of oxidant, 1-10% of coprecipitator, 5-30% of flocculating agent, 1-10% of surfactant, 0.5-10% of emulsion breaker, 1-10% of acidity regulator and 50-90% of water. The invention further discloses a preparation method of the efficient acidic oil sludge decomposing agent. The preparation method comprises the following steps of: 1, preparing sodium carboxymethylcellulose hydrosol; 2, dissolving all kinds of component materials; and 3, adding the sodium carboxymethylcellulose hydrosol prepared in the first step into the solution obtained in the second step so as to obtain the efficient acidic oil sludge decomposing agent. The invention further discloses application of the efficient acidic oil sludge decomposing agent. The efficient acidic oil sludge decomposing agent disclosed by the invention has the advantages of simple preparation process, low cost and easy industrialization; by means of chemical reaction, surface activation action, flocculation and salting-out emulsion breaking actions, the viscosity of the oil sludge is reduced, the oil phase, the water phase and the sludge phase are effectively separated, and the efficient acidic oil sludge decomposing agent can be used for recovering the crude oil from the oil sludge and quickly treating the petroleum pollution soil.
Owner:重庆融极环保工程有限公司

Multielement ex-situ remediation equipment and method used for organo-chlorine pesticide contaminated soil

The invention discloses multielement ex-situ remediation equipment and method used for organo-chlorine pesticide contaminated soil, belongs to the technical field of materializing remediation equipment for contaminated sites. The equipment comprises a stirring device, an eluent injecting device, an eluent recovery device, an ultrasonic generator and a heater. The equipment has extremely strong remediation broad-spectrum performance for organo-chlorine pesticide site soil with different characteristics such as organo-chlorine pesticide substance types, soil contamination incidents, soil contamination concentration, soil organic matter content, soil texture and the like, and a removal rate by single or repeated continuous elution is higher (larger than or equal to 85%); the equipment can form a good matching technology with a patent eluent (ZL201010547630.2), and is developed specially aiming at solving actual contamination situation of organo-chlorine pesticide sites in our country; and during a process of manufacturing the equipment, on the basis of synergistic effects generated by multielement strengthening components such as stirring, ultrasonic, heating and the like, the parameter condition design is optimized, the distribution is scientific and reasonable, and the optimal integration of multielement strengthening components is reflected.
Owner:INST OF SOIL SCI CHINESE ACAD OF SCI

Hemp softening oil, preparation method and use thereof

InactiveCN101230541AEasy to useNo special requirements for water qualityVegetal fibresFiberBiodiesel
The invention provides a soft hemp oil agent. The soft hemp oil agent has the components as follows: biodiesel of 2 to 20 percent, moisture absorption humectant of 0.5 to 3 percent, emulsifier of 1 to 10 percent, and water which is the rest. The soft hemp oil agent is prepared according to the steps as follows: the biodiesel and the emulsifier are added to a reaction kettle for stirring according to the proportion first; the water is gradually added after the solution is well-proportioned; the stirring is continued still the solution disperses evenly; then the moisture absorption humectant is added; the water is added to a set quatity after being stirred. The soft hemp oil agent provided by the invention is used for immersing flexible hemp after the degumming of hemp stem-fibre, oil mechanical injection soft hemp before health preserving, or soft hemp health preserving before opening. Bastose processed by adopting the soft hemp oil agent provided by the invention has the smooth, soft, and hygroscopic as well as moist effect, the penetration process is accelerated at the same time, the cost is lowered, and the invention is beneficial for environmental protection.
Owner:THE QUARTERMASTER EQUIPMENT RESEARCH INSTITUTE OF THE GENERAL LOGISITIC DEPARTME +1

A device and method for extracting micro-plastic in settlings

A device and method for extracting micro-plastic in settlings are provided. The device includes a filter drum, a liquid storage tank, a motor, a pedestal, a screen sieve and a transmission shaft. The filter drum is mounted in the liquid storage tank. The upper port of the filter drum is provided with the screen sieve. The liquid storage tank and the motor are mounted on the pedestal. The bottom of the liquid storage tank is provided with a drainage hole communicated with the filter drum. The motor is connected to one end of the transmission shaft through a rotating shaft, and the other end of the transmission shaft passes through the drainage hole and is connected to the bottom of the filter drum. The device and the method are advantageous in that (1) dispersion effects of muddy settlings and elution effects of a sample are obviously improved; (2) the recovery rate of the sample is increased, (3) the extraction efficiency is greatly increased, (4) extraction time is shortened and (5) labor is saved.
Owner:HOHAI UNIV

Method for extracting tea polyphenol from glede tea

The invention relates to a method for extracting tea polyphenol from glede tea, comprising the following process flows: glede tea is dried and crushed, and is screened by a 60-mesh sieve, refluxed and extracted by 80% ethanol, and pH is adjusted to be 2; then glede tea is treated by high-speed centrifugation, supernatant fluid treatment, polyamide absorption, elution, concentration, refrigeration and drying in vacuum, so as to obtain pure tea polyphenol. 80% ethanol is used to crudely extract the tea polyphenol of glede tea, and extraction rate is relatively higher than hot-water extraction rate; the pH of crude extract is adjusted to be 2, and pigment, caffeine and large-molecule substance are separated in advance by high-speed centrifugation; de-ionized water is used to adjust the concentration of the supernatant fluid to ensure low ethanol content in the supernatant fluid, which is convenient for follow-up 80% ethanol to elute tea polyphenol; polyamide has strong adsorbability to tea polyphenol, and has low cost and easy regeneration; the elution rate of 80% ethanol which is used as main eluent can reach 97.2%, and ethanol has no pollution and is safe and easy to recover. The method has simple technical process and high tea polyphenol extraction rate, and EGCG content in the pure product is higher than that in common green tea. The method has the advantages of low production cost and low energy consumption.
Owner:HEFEI UNIV OF TECH

Eluting agent capable of synchronously removing polychlorinated biphenyl and heavy metal in soil, preparation method and application thereof

The invention belongs to the soil pollution restoration field, and discloses an eluting agent capable of synchronously removing polychlorinated biphenyl and heavy metal in soil, a preparation method and an application thereof. The eluting agent capable of synchronously removing polychlorinated biphenyl and heavy metal in soil is prepared by mixing a citric acid solution and a tween 80 solution. The method for restoring polychlorinated biphenyl and heavy metal-polluted soil comprises the following steps: taking the polychlorinated biphenyl and heavy metal-polluted soil, adding the eluting agent capable of synchronously removing polychlorinated biphenyl and heavy metal in soil, mixing and oscillating, and leaching to complete the restoration for polychlorinated biphenyl and heavy metal-polluted soil. The eluting agent has the advantages of wide raw material source, low cost, the raw materials are biodegradable substances, and environment risk after leaching and restoring can be reduced. The soil restoration effect by employing the eluting agent capable of synchronously removing polychlorinated biphenyl and heavy metal in soil is good, and elution rate is high.
Owner:SOUTH CHINA UNIV OF TECH

Purification method of echinocandins antifungal drug anidulafungin

The invention discloses a purification method of echinocandins antifungal drug anidulafungi. The method comprises the following steps of: (1) preparing a dry sample: adding organic solvent in a crude product of the anidulafungin to dissolve the crude product, adding silica gel after the crude product of the anidulafungin is adequately dissolved, and uniformly mixing and drying the mixture to obtain the anidulafungin dry sample; (2) pressurizing and eluting: uniformly filling the anidulafungin dry samples in the top end of a chromatographic column with silica gel, pressurizing and eluting the chromatographic column with the anidulafungin dry samples by adding elution solvent, utilizing a high-effective liquid phase chromatography to monitor, and collecting the elution solution with the anidulafungin content being greater than 98 percent; and (3) concentrating: concentrating the elution solution with the anidulafungin content being greater than 98 percent until dryness to obtain a pure product with the anidulafungin content being greater than 98 percent. By adopting the column chromatography, simplicity in operation is realized, and the equipment cost is low; the organic solvent with low toxicity and low boiling point is adopted as the elution solution, so that the subsequent recycling treatment is simple, and the environmental pressure can be greatly reduced; and the purification separation time is short, the purification effect is good, the purification yield is high, and the purification method is applicable to industrialized mass production.
Owner:NCPC NEW DRUG RES & DEV

Method for extracting and separating cannabidiol

The invention relates to a method for extracting and separating cannabidiol. The method comprises the following steps of 1) pulverization, wherein dried industrial cannabis flowers and leaves are pulverized into granules by using a grinding disperser; 2) extraction, wherein ethyl alcohol, petroleum ether or solvent naphtha is taken as a single solvent or a mixed solvent to perform reflux extraction on the materials; 3) enrichment, wherein an industrial hemp fluid extract obtained by extraction and concentration is subjected to macroporous resin chromatography, and an eluate is collected in stages to obtain a cannabidiol enrichment; 4) separation, wherein the cannabidiol enrichment is subjected to silica gel column chromatography, and an eluate is collected in stages, concentrated, dried and crystallized to obtain the cannabidiol. The product has the advantages that the purity is higher, the extraction is convenient and fast, and the purification cost is lower.
Owner:栾云鹏

Pretreatment method for detecting nitrofuran metabolites in aquatic product

The invention discloses a pretreatment method for detecting nitrofuran metabolites in an aquatic product. The method comprises the following steps of: weighing a sample to be detected, dissolving, derivating, extracting, and performing chromatographic separation. A constant temperature oscillator, a reduced pressure rotary evaporator, a silica gel chromatographic column and a high speed refrigerated centrifuge are used in the method. A sample solution prepared by the method can be directly detected by liquid chromatography-tandem mass spectrometry. Compared with the conventional national standard method, the pretreatment method has the advantages of low cost, high repeatability and the like, is simply and effectively operated, is high in operability, is expected to be popularized and applied to environmental protection industry, commodity inspection, entry-exit inspection and quarantine and the like on a large scale, and is obvious in economic and social benefits.
Owner:FUJIAN CCIC FAIRREACH FOOD SAFETY TESTING

Lectin-macromolecule carrier coupling compound for separating glycosylated exosome in clinical sample

The present invention relates to a lectin-macromolecule carrier coupling compound for separating a glycosylated exosome in a clinical sample. The lectin-macromolecule carrier coupling compound comprises a macromolecule carrier; and lectin coupled to the outer side of the macromolecular carrier. The lectin-macromolecular carrier coupling compound provided by the invention can be used for simply, conveniently, rapidly and accurately separating the glycosylated exosomes in the clinical sample; the compound is simple in operation, high in separation efficiency and good in repeatability, and the separated exosome is complete in form and free of breakage or fragmentation and can be directly used for glycosylated exosome liquid detection or directly used for immunological related detection or directly used for gene detection and analysis by extracting related nucleic acid in the exosome.
Owner:北京尧景基因技术有限公司

Catheter

The invention relates to rigid surgical devices formed from rigid ceramics such as zirconium dioxide. In particular, the invention relates to a neurosurgical catheter formed from extruded zirconium dioxide. The invention also relates to an advancement means for advancing or retracting such a device along an axis of insertion into a patient.
Owner:RENISHAW (IRELAND) LTD

Method for recovering anion exchange resin polluted by organic matters and recovery medicine

The invention relates to a method for recovering anion exchange resin polluted by organic matters and a recovery medicine, and aims to solve the problems that an elution effect is poor in the conventional recovery method and the conventional recovery medicine cannot increase the number of strong alkali groups when the anion exchange resin is severely polluted by the organic matters or macromolecular linear organic matters are tightly wound in the anion exchange resin. The method for recovering the anion exchange resin polluted by the organic matters comprises the following steps of: 1, transforming the anion resin; 2, flushing; 3, removing the organic matters from the anion resin to recover the anion resin; 4, flushing; and 5, regenerating. The recovery medicine used in the method for recovering the anion exchange resin polluted by the organic matters consists of NaCl, NaOH, an organic aid and water. The method is suitable for recovering the anion resin polluted by the organic matters and removing the organic matters from cation resin.
Owner:HARBIN INST OF TECH

Method for determining content of saffron in medicinal composition

ActiveCN103529140AEnhanced elution capacityReduce distractionsComponent separationDrugCarthamus
The invention discloses a method for determining the content of saffron in a medicinal composition, and aims to solve the problem that the content of saffron in a complex medicinal composition is difficult to determine. According to the method, methanol-acetonitrile-0.05mol / L ammonium acetate in a volume ratio of (30-45):5:(50-65) is adopted as a mobile phase, and a high performance liquid chromatography is adopted for determination; the mobile phase is a multi-solvent system, the mobile phase system is kept to be stable by adopting buffer salt, and the elution power is reinforced. The method provided by the invention is stable in determination result and good in linearity, the correlation coefficient, the resolution and the number of theoretical plates can meet the requirement of measurement standard, and a good detection result can be obtained on the saffron in a medicinal composition with a complex prescription.
Owner:JINHE TIBETAN MEDICINE

Method for separating component from direct-coal-liquefaction full distillate oil by utilizing solid-phase extraction method

The invention provides a method for separating a component from direct-coal-liquefaction full distillate oil by utilizing a solid-phase extraction method. The method comprises the steps of: S1, sampling and absorbing the direct-coal-liquefaction full distillate oil to be separated to a separation column which is formed by a fixed phase; S2, washing at a washing speed of 20-50 ml / min by adopting a saturated hydrocarbon eluting agent having a weight ratio of (10-50):1 to the full distillate oil and collecting a first eluent, wherein the saturated hydrocarbon eluting agent is one or more selected from a group which is composed of n-hexane, n-pentane and petroleum ether; and S3, volatilizing the saturated hydrocarbon eluting agent in the first eluent to obtain a saturated hydrocarbon component. Aiming at the special chemical composition of the direct-coal-liquefaction full distillate oil, the saturated hydrocarbon eluting agent having an excellent elution effect on saturated hydrocarbon is selected in the method; and as the saturated hydrocarbon is separated under the condition of controlling an agent-to-oil ratio and the washing speed, an ideal separation effect of the saturated hydrocarbon and aromatic hydrocarbon in the full distillate oil having high-content aromatic hydrocarbon is achieved.
Owner:CHNA ENERGY INVESTMENT CORP LTD +2

Mixed eluant for synchronously removing polychlorinated biphenyl and heavy metals in soil and its preparation method and use

The invention belongs to the technical field of polluted soil restoration and discloses a mixed eluant for synchronously removing polychlorinated biphenyl and heavy metals in soil and its preparation method and use. The mixed eluant is prepared by dissolution of active ingredients of saponin and Tween 80 in water. The mixed eluant is used for restoration of soil polluted by polychlorinated biphenyl and heavy metals. In use, the soil polluted by polychlorinated biphenyl and heavy metals is taken, and the polluted soil is mixed with the eluant and is eluted so that restoration of soil polluted by polychlorinated biphenyl and heavy metals is realized. The mixed eluant has a wide raw material source, has a low price, is environmentally friendly, has good elution effects and high elution efficiency and has a multi-ingredient polluted soil elution rate of 80% or more.
Owner:SOUTH CHINA UNIV OF TECH +1

Method for simultaneously detecting multiple types of persistent organic pollutants in water body

The invention discloses a method for simultaneously detecting multiple types of persistent organic pollutants in a water body. The persistent organic pollutants comprise polychlorinated biphenyl, polybrominated diphenyl ethers and polycyclic aromatic hydrocarbon. The method comprises the following steps: (1) sample pre-treatment is conducted, specifically, a to-be-detected water sample is taken to be filtered, standard substitutions and internal standard substances of the persistent organic pollutants are added to be evenly mixed, and a pretreated water sample is obtained; (2) solid-phase extraction is conducted, specifically, the pretreated water sample is guided into a solid-phase extraction column to be subjected to solid-phase extraction, and the solid-phase extraction column is driedand eluted through eluents, namely n-hexane and acetone; (3) purification is conducted, specifically, dried eluate is purified through a Florisil column; (4) gas chromatography-mass spectrometry combined detection is conducted; and (5) the content of the persistent organic pollutants is calculated. By selecting the appropriate eluents and adopting a triple quadrupole gas chromatography-mass spectrometry combined instrument, the polychlorinated biphenyl, the poly brominated diphenyl ethers and the polycyclic aromatic hydrocarbon are simultaneously detected, the detection limits are all low, and the method has great significance in the field of persistent organic pollutant detection.
Owner:SHENZHEN ACAD OF ENVIRONMENTAL SCI

Method for circularly repairing organic polluted soil by cyclodextrin eluting solution

The invention discloses a method for circularly repairing organic polluted soil by a cyclodextrin eluting solution and belongs to the technical field of repairing of polluted soil. The method comprises the following steps: eluting the organic polluted soil by the cyclodextrin eluting solution and performing centrifugal separation to obtain liquid supernatant; irradiating the liquid supernatant by ultraviolet lights; and with the liquid supernatant as an eluting solution, repairing the organic polluted soil circularly. According to the method disclosed by the invention, organic pollutants in the eluting solution can be efficiently decomposed; meanwhile, the cyclodextrin eluting solution can be protected from being decomposed; the eluting solution and the organic pollutants can be separated without a special separation device or a special separation technology along the complete degradation of organic polluted substances so as to realize regeneration and recycling of cyclodextrin. The regenerated eluting solution still has a good effect of eluting the organic polluted soil. Furthermore, the method has the advantages of no secondary pollution, simplicity and feasibility in operation, simple equipment and the like.
Owner:WUHAN UNIV

Detection method for dezocine related substances

The invention provides a detection method for dezocine related substances. Octadecyl silane bonded silica gel is adopted as a chromatographic column of a filling agent, and an acetonitrile-triethylamine solution is adopted as a mobile phase, wherein the acetonitrile-triethylamine solution is obtained by taking 1000 ml of water, adding 5 ml of triethylamine and 2 ml of a tetrabutyl ammonium hydroxide water solution, and adjusting pH to 3.2 through diluted phosphoric acid (1-5), and the ratio of acetonitrile to triethylamine is 200:800; the flow rate is 0.6 ml per min, and the detection wavelength is 281 nanometers. According to the detection method for dezocine related substances, the concentration of buffer salts is increased, elution is enhanced, an ion-pairing agent is added, the peak shape is improved, and the problems that due to the fact that the number of theoretical plates of an original method is small and a main peak cannot be rapidly eluted, the peak width is large and trailing is serious are solved.
Owner:JINAN LIMIN PHARMA

Eluent for a pesticide-DDT in black soil and eluting method of eluent

InactiveCN104550221AGood elution removal effectEasy to useContaminated soil reclamationInorganic saltsSolvent
The invention discloses an eluent for a pesticide-DDT in black soil and an eluting method of the eluent. The eluent disclosed by the invention is composed of a non-ionic surfactant, an anionic surfactant, inorganic salt, an organic additive and a solvent. The specific composition of the eluent is as follows: the mass ratio of the non-ionic surfactant-twain 60 to the anionic surfactant-sodium dodecyl sulfate in the eluent is (1-3) to 1, the total concentration of the two is 3000-4000mg / L, the concentration of the inorganic salt-K2SiO3 or K2CO3 in the eluant is 1.0g / L, the concentration of the organic additive-n-propanol or n-butyl alcohol in the eluent is 1.0-2.0mol / L, and the solvent is water.
Owner:NORTHEAST FORESTRY UNIVERSITY

Cigarette filter with smoke odor selection function

The invention relates to a cigarette filter with a smoke odor selection function. The cigarette filter consists of a cavity-containing mouth stick and a perfuming thread / rod-containing mouth stick, which are mutually connected, wherein the cavity-containing mouth stick is formed by forming a cavity in a filter stick, and the perfuming thread / rod-containing mouth stick is formed by adding at least two perfuming thread / rods into another filter stick; a layer of hard forming paper wraps the part of the perfuming thread / rod-containing mouth stick, so that the perfuming thread / rod-containing mouth stick and the cavity-containing mouth stick are controlled to be connected during rotation so as not to be separated from each other. By the adoption of the cigarette filter, a consumer can enable the cavity to be aligned with the perfuming threads / rods through rotating the perfuming thread / rod-containing mouth stick, so that the elution function of smoke to specific odor ingredients is improved, and the content of some odor ingredient in smoke is increased to achieve the smoke odor selection purpose. Meanwhile, owing to the unique appearance, various filters with different appearances can be formed by combination, the recognition degree of the filters and the product differentiation are improved.
Owner:CHINA TOBACCO YUNNAN IND

An environment-friendly eluent for treating heavy metal polluted soil

An environment-friendly eluent for treating heavy-metal-polluted soil comprises tetrasodium iminodisuccinate, concentrated nitric acid and water, wherein the mass ratio of each component after preparation is as following: tetrasodium iminodisuccinate 0.18-5 per mill, concentrated nitric acid 0.024-0.6 per mill, and water 994.4-999.796 per mill. The preparation method is as following: 1. putting tetrasodium iminodisuccinate with mass ratio 0.18-5 per mill into a plastic barrel, and adding water with mass ratio 994.4-999.796 per mill into the plastic barrel, then stirring the resultant by a stirrer for 10 min to have the tetrasodium iminodisuccinate fully dissolved; 2. adding concentrated nitric acid with mass ratio 0.024-0.6 per mill into the plastic barrel, and then stirring the resultant by a stirrer for 10 min to obtain the environment-friendly eluent for treating heavy-metal-polluted soil. By the invention, the eluent can restore heavy-metal-polluted soil and can be biodegraded completely without causing a second pollution.
Owner:河北协同化学有限公司

Treatment method of cyanogen-containing tailing slurry

The invention belongs to pollutant treatment methods in the field of environmental protection and particularly relates to a treatment method of cyanogen-containing tailing slurry. The method comprisesthe steps of positive pressure filtration, water washing, blowing-off, filtrate treatment and the like, and an integrated treatment process is formed. The method provided by the invention has the advantages that the defects of low elution efficiency, large water consumption and the like existing in traditional stirring and elution processes can be overcome, cyanides and valuable metals in the cyanogen-containing tailing slurry can be eluted and treated, harmless treatment of the cyanogen-containing tailing slurry can be realized, recovery of cyanogen and valuable metal elements in the tailingslurry can be realized, full utilization of water resources can be realized, and the method has the characteristics of high elution efficiency, low water consumption, good elution effect and broad application prospect.
Owner:CHANGCHUN GOLD RES INST

Activation extraction separation method for fluorine and chloride ions in zinc sulfate solution

The invention relates to an activation extraction separation method for fluorine and chloride ions in a zinc sulfate solution, which comprises the following steps: acid adjustment activation: adding concentrated sulfuric acid into the zinc sulfate solution to adjust the pH value and temperature, and mixing and blending the solution with an activating agent to damage the fluorine-containing metal complexes in the solution and decompose the fluorine-containing metal complexes into free-state fluorine ions and convert into HF molecules; extraction separation: separating the fluorine and chloride ions in the activated zinc sulfate solution by use of an extraction agent to obtain an organic phase loaded with fluorine and chloride and a raffinate with low content of fluorine and chloride; raffinate purification: removing most of the extraction organic phase through multi-segment standing clarification and ultrasonic air flotation; performing deep adsorption by use of powdery active carbon to remove residual organic phase in the raffinate to obtain adsorption residue and qualified raffinate; and impurity washing and back extraction of the loaded organic phase. According to the method provided by the invention, the key reason hindering the extraction fluorine removal effect in the zinc sulfate solution as well as the crystallization and scaling in the back extraction process is found so that the different problems are simple and easy to impellent. The fluorine removal rate exceeds 60%, and the chlorine removal rate reaches about 90%. The liquid after impurity washing and the liquid after back extraction directly return to an alkali washing process of a zinc hydrometallurgy system to be comprehensively utilized.
Owner:GREENNOVO ENVIRONMENTAL TECH CO LTD

Method for adsorbing chromium and iron ions in industrial ferrochrome ore liquid through ion exchanging resin.

InactiveCN107828962ATo achieve the purpose of separating ferrochromium ionsImprove adsorption capacityProcess efficiency improvementLiquid wasteFerrochrome
The invention provides a method for adsorbing chromium and iron ions in industrial ferrochrome ore liquid through ion exchanging resin. 001x7 cation exchange resin is added into the industrial ferrochrome ore liquid, and constant temperature oscillation adsorption is performed at room temperature; centrifugal separation is performed after adsorption balance; and saturated resin uses an ammonium sulphate solution with the mass fraction being 5%-10% or water as eluant, constant temperature oscillation elution is performed at room temperature till balance is achieved, and the eluant is collected.An experiment shows that the method for adsorbing the chromium and iron ions in the industrial ferrochrome ore liquid through the ion exchanging resin can achieve high adsorption of the chromium andiron ions in the simulated industrial ferrochrome waste liquid, and a good elution effect is achieved. Thus, the method can be used for recycling of the chromium and iron ions in the industrial ferrochrome ore liquid.
Owner:LANZHOU CITY UNIV

Support for antibody purification, manufacturing method for same, and application for same

An object of the present invention is to provide a carrier on which Protein A has been immobilized, the Protein A having a specific amino acid sequence that permits the desorption of antibodies under mild pH conditions (specifically, pH4.0 to 5.5) in which many antibodies do not undergo acid modification; and a manufacturing method for the carrier. An immobilization carrier (excluding an immobilization carrier having a monolith structure) on which a protein is adsorbed by electrostatic interaction, the protein consisting of an amino acid sequence represented by the general formula: R1-R2-R3-R4-R5-R6, wherein the part represented by R1-R2-R3 is used for immobilization on the immobilization carrier, wherein: the sequence represents a sequence from the amino-terminal side towards the carboxyl-terminal side; the sequence of the R2 part is the sequence of a Protein A mutant as a protein to be immobilized or a sequence in which 1 to 3 units of the sequence thereof were linked together, the Protein A mutant having characteristics of strongly binding to an antibody under neutral conditions and dissociating with the antibody bound under neutral conditions under weakly acidic conditions of pH 4.0 to 5.5.
Owner:OSAKA SODA CO LTD

Large-volume enrichment liquid aerosol liquid sampler suitable for air microbe analysis

ActiveCN110387318AFully elutedReduce sampling efficiencyBiological material testing proceduresSingle stageDNA extraction
The invention discloses a large-volume enrichment liquid aerosol liquid sampler suitable for air microbe analysis. The large-volume enrichment liquid aerosol liquid sampler is mainly used for correlation analysis of air microbes, and can be in single-stage or multi-stage series with enrichment bottles; large-volume enrichment liquid can be filled in each enrichment bottle, the large-volume enrichment liquid aerosol liquid sampler is characterized in that the enrichment of more microbes is conducted, a gas jet column is arranged at the bottom of the sampler, an air inlet is connected with a flowmeter, aerosol firstly enters the first stage of single-stage or multi-stage enrichment bottles; if the multi-stage series enrichment bottles are arranged, the air microbes not eluting in the first stage enrichment bottle can enter the second stage enrichment bottle again or more-stage enrichment liquid after the second stage enrichment bottle is further fully eluted; and the last stage enrichment bottle of single-stage or multi-stage enrichment bottles is connected with a diaphragm vacuum pump, and the enrichment liquid of the enrichment microbes is collected from the outlets under the enrichment bottles. According to the aerosol liquid sampler, the long-term sampling without obvious microbe secondary proliferation can be realized; samples can guarantee the microbe activity and culturability, and can guarantee the high-quality DNA extraction; and the microbial concentration at sampling sites is not limited, adaptable sampling types are wide, simple and efficient, and the production cost is low.
Owner:NANKAI UNIV

Preparation method of all-organ acellular matrix of heart

The invention discloses a preparation method of all-organ acellular matrix of a heart. In the method, perfusion with 1% SDS solution and 1% Ttiton is performed, then PBS is used for flushing, liquid is exchanged for 4-5 times every day, and cleaning is totally performed for 72-128h. According to the method, a reasonable all-organ acellular system is designed, an existing heart all-organ acellular method is improved and optimized, and acellular treatment is performed according to different eluting sequences and time proportions by combining with SDS detergent and TritonX100, so that the eluting effect of the perfusate in the heart organ is improved, and a foundation is built for application of the method in elevation of late acellular matrix and reconstruction of tissue engineering. The all-organ acellular matrix of the heart prepared by the method can reserve original second-level and third-level vessel structures, supermicro conformation and extracellular matrix components of the heart under the condition of removing original resident cells of the original tissue.
Owner:INST OF BASIC MEDICAL SCI ACAD OF MILITARY MEDICAL SCI OF PLA
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products