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75 results about "Ammonium chlorate" patented technology
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Ammonium chlorate is an inorganic compound with the formula NH₄ClO₃. It is obtained by neutralizing chloric acid with either ammonia or ammonium carbonate, or by precipitating barium, strontium or calcium chlorates with ammonium carbonate or ammonium sulfate, producing the respective carbonate or sulfate precipitate and an ammonium chlorate solution. Ammonium chlorate crystallizes in small needles, readily soluble in water.
Room-temperature-cured-type clean solid propellant
The invention provides a room-temperature-cured-type clean solid propellant. The room-temperature-cured-type clean solid propellant is prepared from, by mass, 55%-70% of chlorine-free oxidizing agents, 5%-20% of metal fuels, 5%-15% of plasticizers, 5%-10% of amine-terminated polyether adhesives, 0.5%-1.0% of isocyanate curing agents and 0.01%-3% of function auxiliaries. According to the room-temperature-cured-type clean solid propellant, the detect that in the prior art, due to the fact that an oxidizing agent ammonium perchlorate is used in a compound solid propellant, a large amount of HCl gas is contained in a combustion product, and atomospheric pollution is serious is overcome; the amine-terminated polyether adhesives with the high reaction activity are introduced into a compound solid propellant system, and a cross-linking and curing reaction of terminal amino groups and the isocyanate curing agents is utilized, so that room-temperature curing of the amine-terminated polyether propellant is achieved; no HCl gas exists in the combustion product by adding the chlorine-free oxidizing agents.
Owner:HUBEI INST OF AEROSPACE CHEMOTECHNOLOGY
Double-effect perforating bullet containing active material layer, and active material
PendingCN107130946ASimple structureCompact structureFluid removalExplosivesAl powderManufacturing technology
The invention discloses a double-effect perforating bullet containing an active material layer, and an active material. The double-effect perforating bullet comprises a common perforating bullet and the active material layer, wherein the common perforating bullet comprises a cartridge shape cover, a cartridge case and a high explosive layer; the active material layer is arranged between the cartridge case and the high explosive layer; the active material is prepared from the following materials: aluminum powder, nickel powder, magnesium powder, potassium perchlorate, ammonium perchlorate, potassium nitrate, ferric oxide, copper oxide, polytetrafluoroethylene, fluorine rubber, and the like. The double-effect perforating bullet is reasonable in structural design and safe and reliable in manufacturing technology, and has double effects of perforating and removing a perforation compaction band and fracture forming in a pore path.
Owner:NORTH SCHLUMBERGER OILFIELD TECH XIAN
Preparation method of fluorine polymer/metal composite energy-containing material
ActiveCN109956844ASimple operation processEasy to prepare in batchesExplosive working-up apparatusAmmonium perchlorate explosive compositionsDetonationDecomposition
The invention discloses a preparation method of a fluorine polymer / metal composite energy-containing material. According to the preparation method, ammonium perchlorate is doped in a fluorine polymermetal energy-containing system through solution crystallization method so as to obtain a novel composite energy-containing material. According to the preparation method, ammonium perchlorate decomposition is adopted to generated a gas product for enhancing the system pressure output and combustion reaction performance, at the same time, the gas obtained through ammonium perchlorate decomposition and reaction product carbon from a fluorine polymer metal system are subjected to oxidation reaction, energy and pressure release is accelerated, so that the fluorine polymer metal energy-containing system energy and combustion reaction characteristics are improved obviously. The preparation method is capable of improving the energy and pressure output of the fluorine polymer metal energy-containing system, and combustion reaction rate is converted from slow combustion to detonation and blast. Doping is adopted to form the novel energy-containing system, and it is possible for the novel energy-containing system to be used in fields such as solid propellant, metallized explosive, and gas generators.
Owner:INST OF CHEM MATERIAL CHINA ACADEMY OF ENG PHYSICS
Gas generating agent composition, method for preparing same, application of gas generation agent composition and gas generator
InactiveCN107698415AKeep shapeForm-retaining agents do not work wellPedestrian/occupant safety arrangementNon-explosive/non-thermic compositionsStrontium titanateCopper nitrate
The invention relates to a gas generating agent composition, a method for preparing the same and a gas generator with the gas generation agent composition. The gas generating agent composition comprises, by weight, 40%-60% of guanidine nitrate, 25%-40% of alkali copper nitrate, 1%-20% of strontium nitrate, 1%-10% of ammonium perchlorate, 5.5%-10% of strontium titanate and 0.6%-10% of talc powder.The gas generating agent composition, the method and the gas generator have the advantages that the strontium titanate and the talc powder are jointly used as shape keeping agents, synergistic effectscan be realized by the strontium titanate and the talc powder, accordingly, pre-combustion shapes of tablets can be effectively kept after the tablets are combusted, and gas bags can be prevented from being burnt due to melting and splashing of the combusted tablets; the strontium nitrate is used as an auxiliary oxidizing agent, the usage amount of the alkali copper nitrate is reduced, and accordingly molten copper residues can be reduced; the ammonium perchlorate is used as an ignition performance regulator, accordingly, the low-temperature ignition performance of the gas generating agent composition can be obviously improved, the combustion speeds can be increased, and the gas generating agent composition mainly can be used for gas generators for supplementary restraint systems of automobiles.
Owner:HUBEI HANGPENG CHEM POWER TECH
Method for extracting and gathering total alkaloids of hypecoum leptocarpum
ActiveCN105168376AHigh column efficiencyHigh mechanical strengthPlant ingredientsPolystyreneSilica gel
The invention relates to a method for extracting and gathering total alkaloids of hypecoum leptocarpum. The method comprises the following steps: (1) extraction, crushing a medicinal material hypecoum leptocarpum, then leaching the hypecoum leptocarpum with ethanol with the volume concentration of 10%-69% to obtain an extract solution, and recovering ethanol from the extract solution through vacuum reduced pressure until a liquid extract is formed, so as to obtain a hypecoum leptocarpum extract; (2) gathering of alkaloids, dissolving the hypecoum leptocarpum extract, carrying out treatment with a strong cation exchange material silica SCX column of silica gel matrix, sequentially eluting the hypecoum leptocarpum extract with pure methanol and an ammonium perchlorate-methanol solution, and collecting a salt elution part; and (3) desalting treatment, carrying out desalting on the salt elution part with a polystyrene-based reverse resin column, eluting with water until colorless, eluting with pure methanol, collecting a pure methanol eluent, and recovering methanol from the pure methanol eluent, so as to obtain the total alkaloids of the hypecoum leptocarpum. The method is simple in technology, low in cost and high in efficiency.
Owner:CHINA ACAD OF SCI NORTHWEST HIGHLAND BIOLOGY INST
Chlorine-containing gas generant compositions including a copper-containing chlorine scavenger
InactiveUS20050016646A1Non-explosive/non-thermic compositionsAmmonium perchlorate explosive compositionsScavengerCopper nitrate
A chlorine-containing gas generant composition and a related method for generating an inflation gas for use in an inflatable restraint system are provided. The chlorine-containing gas generant composition includes a nitrogen-containing fuel such as guanidine nitrate, ammonium perchlorate oxidizer, and a chlorine scavenger present in an amount effective to result in a gaseous effluent that is substantially free of hydrogen chloride when the gas generant is combusted, wherein at least about 98 weight percent of the chlorine scavenger is a copper-containing compound such as a copper nitrate complex, basic copper nitrate, cupric oxide or a combination thereof.
Owner:AUTOLIV ASP INC
Ammonium perchlorate embedded carbon/metallic oxide composite catalyst, and preparation method thereof
ActiveCN106391080AFull catalytic effectGood catalyticCatalyst activation/preparationAmmonium perchlorateOxide composite
The invention discloses an ammonium perchlorate embedded carbon / metallic oxide composite catalyst, and a preparation method thereof. According to the ammonium perchlorate embedded carbon / metallic oxide composite catalyst, three-dimensional ordered macroporous-mesoporous carbon is taken as a carrier material, and at the same time, the ammonium perchlorate embedded carbon / metallic oxide composite catalyst is obtained via loading of nano metallic oxide particles and ammonium perchlorate. The ammonium perchlorate embedded carbon / metallic oxide composite catalyst possesses excellent catalytic effect on thermal decomposition of ammonium perchlorate, and is capable of reducing high temperature thermal decomposition temperature of ammonium perchlorate greatly, and increasing apparent heat release greatly.
Owner:INST OF CHEM MATERIAL CHINA ACADEMY OF ENG PHYSICS
Chemical energy-increasing high-efficiency discharge aiding agent and preparation method and use method thereof
InactiveCN108048068AGood interfacial tensionImprove flowback energyDrilling compositionMass ratioSurface-active agents
The invention discloses a chemical energy-increasing high-efficiency discharge aiding agent and a preparation method and a use method thereof and belongs to the field of oil exploitation. The chemicalenergy-increasing high-efficiency discharge aiding agent is prepared from a cationic surface active agent, a fluorocarbon surface active agent and an energy producing chemical agent, wherein a mass ratio of the cationic surface active agent to the fluorocarbon surface active agent to the energy producing chemical agent is (6 to 8) to (1 to 1.6) to 1; the energy producing chemical agent is a mixture of compound A and compound B; the compound A is ammonium bioxalate, ammonium oxalate, ammonium chlorate, hydrogen peroxide or ammonium chloride; the compound B is potassium nitrite. The discharge aiding agent can generate a lot of gas to improve flowback energy of a fracturing and gel breaking solution, promote high-efficiency flowback of the fracturing and gel breaking solution, reduce fracturing solution adhesion damage and is suitable for being applied to a compact oil reservoir oil well fracturing and production increasing technology to promote the flowback of fracturing and gel breaking solution. The preparation method comprises the steps: taking the cationic surface active agent, the fluorocarbon surface active agent and the energy producing chemical agent; mixing; fully and evenly stirring to prepare the chemical energy-increasing high-efficiency discharge aiding agent. The method is simple, and the utilized raw materials are easy to obtain.
Owner:PETROCHINA CO LTD
Cleaning type low-pressure low-temperature burning solid fuel
InactiveCN101265426AGood flame visibilityStrong wind resistanceSolid fuelsWaste based fuelHydroxyl-terminated polybutadieneNuclear engineering
The invention relates to a clean type solid fuel which is burnt in low temperature and low pressure. The fuel comprises the components of hydroxyl-terminated polybutadiene, ammonium perchlorate, ammonium nitrate, toluene diisocynate, nitro cotton, plasticizer, equalizer and potassic nitrate, and odor regulator and / or flame color regulator can also be added. The fuel has the advantages of strong combustion blaze, good blaze visibility, less burnt residue, clean burning, high burning heat value, smokelessness, innocuity, high wind resistance and high security; the fuel can be continuously and stably burnt particularly under the environmental condition of 0.02 MPa and minus 40 DEG C, and can not be put out in strong wind, heavy rain and heavy snow when being matched with a special burner; the solid fuel with good and reliable performance is provided for delivering a torch at the peaks of summits (including the Everest), and can be limitlessly used on the terrene; the fuel is particularly suitable for the field operation in extremely cold areas, and the portable and reliable solid fuel with high heat value is provided for wild lives, wild mountaineering, expeditions, heating, field training and signal setting off.
Owner:XIAN NORTH HUIAN CHEM IND CO LTD
Nearly spherical core-shell structure composite energetic material and preparation method thereof
ActiveCN110655432AHigh bulk densityDense grainMicroballoon preparationAmmonium perchlorate explosive compositionsEthyl acetateSolvent
The invention discloses a nearly spherical core-shell structure composite energetic material and a preparation method thereof. Recrystallization is carried out by a solvent-non-solvent method, and dihydroxylammonium 5,5'-bistetrazole-1,1'-diolate is sheared by a colloid mill to obtain nearly spherical dihydroxylammonium 5,5'-bistetrazole-1,1'-diolate particles; ammonium perchlorate is dissolved inwater, the dihydroxylammonium 5,5'-bistetrazole-1,1'-diolate particles are added into an ethanol / ethyl acetate mixed solvent and stirred, an ammonium perchlorate aqueous solution is dripped into dihydroxylammonium 5,5'-bistetrazole-1,1'-diolate suspension, and the ammonium perchlorate is saturated and separated out to obtain the core-shell structure composite energetic material with the ammoniumperchlorate tightly coating the dihydroxylammonium 5,5'-bistetrazole-1,1'-diolate. The composite energetic material prepared by the method provided by the invention has the advantages of high bulk density, low sensitivity and high explosion heat, and can effectively improve the explosion heat of the dihydroxylammonium 5,5'-bistetrazole-1,1'-diolate and improve the oxygen balance of the dihydroxylammonium 5,5'-bistetrazole-1,1'-diolate.
Owner:XIAN MODERN CHEM RES INST
Preparation method and application of ammonium perchlorate thermal decomposition catalytic material
PendingCN112125348ALarge specific surface areaRapid responseNanotechnologyCobalt compoundsPolyethylene glycolPhysical chemistry
The invention discloses a preparation method of an ammonium perchlorate thermal decomposition catalytic material and application of the ammonium perchlorate thermal decomposition catalytic material incatalyzing thermal decomposition of ammonium perchlorate. The preparation method comprises the following steps of: dissolving Co(NO3)2.6H2O, Cu(NO3)2.6H2O and urea in polyethylene glycol to form a transparent pink solution, transferring the solution into a stainless steel reaction kettle containing a polytetrafluoroethylene liner, reacting at 160-220 DEG C for 10-24 hours, and preparing the nanoflower-like structure CuCo2O4 catalytic material for thermal decomposition of ammonium perchlorate by a solvothermal method. By optimizing the process route and reducing the cost, the invention provides a simple and practical method for preparing the bimetallic CuCo2O4 nano material, and the bimetallic CuCo2O4 nano material has important scientific value and development prospect in the field.
Owner:SHANGHAI INST OF TECH
Gas generating agent composition as well as preparation method and application thereof
ActiveCN111675589AAvoid burnsImprove low temperature ignition performancePedestrian/occupant safety arrangementAmmonium perchlorate explosive compositionsSlagAutomobile safety
The invention relates to a gas generating agent composition, a preparation method and a gas generator containing the gas generating agent composition. The gas generating agent composition comprises the following components in percentage by mass: 40-60% of guanidine nitrate, 25%-60% of basic copper nitrate, 1%-20% of strontium nitrate, 1%-10% of ammonium perchlorate, 1%-10% of a slag-forming agent,and 0.6%-10% of a release agent / lubricant. The gas generating agent composition uses a slag-forming agent as a form-retaining agent. A tablet can well keep the form after combustion and is preventedfrom melting and splashing to burn an air bag after combustion, strontium nitrate and ammonium perchlorate are adopted as auxiliary oxidants, the use amount of basic cupric nitrate is reduced, moltencopper residues are reduced, and the gas generating agent composition is mainly used for an automobile safety airbag gas generator.
Owner:HUBEI HANGPENG CHEM POWER TECH
Remote-controlled aircraft for hail mitigation and precipitation and hail mitigation and precipitation method
PendingCN107318546AImprove securityLoose airspace controlPiston type power plantsJet type power plantsJet engineSilver iodide
The invention discloses a remote-controlled aircraft for hail mitigation and precipitation and a hail mitigation and precipitation method. The remote-controlled aircraft is adopted to scatter silver iodide in a cloud layer, the safety is better, airspace control is relatively loose, and the adaptability is strong. The silver iodide is dissolved in an acetone-alcohol solution, the use of ammonium chlorate is avoided, pollution is decreased, and the remote-controlled aircraft has better environmental protection property. In addition, explosive materials are avoided, the aircraft is safer, and inventory management, transportation management and operation management are loose to control. Wings are foldable and are convenient to store, transport and operate, and the cost is reduced. The acetone-alcohol solution containing the silver iodide is burned at the tail portion of a jet engine, corrosion of the jet engine is avoided, and the service life is prolonged.
Owner:BEIJING INSTITUTE OF TECHNOLOGYGY
Ammonium perchlorate wastewater processing method
ActiveCN111115842AGood removal effectThorough treatmentWater contaminantsWaste based fuelVolatile fatty acidsElectron donor
The invention discloses an ammonium perchlorate wastewater processing method, and the method comprises the following steps: obtaining an intermediate product hydrogen and volatile fatty acid through akitchen waste anaerobic digestion hydrogen and acid production stage; providing an electron donor and a carbon source for the process of reducing ammonium perchlorate by perchlorate reducing bacteriaby utilizing the intermediate product hydrogen and volatile fatty acid; reducing ammonium perchlor`ate into chloride ions by adopting a three-stage degradation combined process of hydrogen autotrophic reduction, organic acid heterotrophic reduction and iron / sulfur autotrophic reduction to reduce the concentration of the ammonium perchlorate wastewater and complete the processing of the ammonium perchlorate wastewater . According to the method, the removal effect of the ammonium perchlorate wastewater can be remarkably improved, meanwhile, generated biogas is used as clean energy for life andproduction, and the economic rationality and the process operability are remarkably improved.
Owner:XI AN JIAOTONG UNIV
Flame tube for emergent warning motor vehicle and its formulation
InactiveCN1499452AImprove performanceStrong warningSmoke/fire/colored-gas signallingExplosivesStrontium carbonateEngineering
The flame tube is composed of burning stick, base and outer cover tube. One end of the burning stick is fixed on flat end of the base, and the outer cover tube put outside the burning stick is fitted to the base. Flammable kindling is installed on other end of the burning stick. Friction surface making the flammable kindling on fire is put the position on the outer cover tube for easy to use. Formula of powder is composed of granular ammonium chlorate, potassium chlorate, strontium nitrate and strontium carbonate. Advantages of the invention are that good performances: burning time more than 5 minutes, light intensity 160 candela up, period of validity 4 years; easy of use, high safety and high caution effect; applicable to other special uses besides traffic safety.
Owner:韩疏
Quaternary alkyl ammonium hypochlorite solution, method of producing the same, and method for processing semiconductor wafers
ActiveUS11390577B2Reduce yieldReduce cleaningAmino preparation from aminesDetergent mixture composition preparationHypochloriteReaction step
Owner:TOKUYAMA CORP
Device and method for degrading ammonium perchlorate wastewater by using hydrothermal-biological combined process
ActiveCN112441705AAvoid serious harmReduce pollution loadWater contaminantsTreatment with aerobic and anaerobic processesHigh concentrationSludge
The invention discloses a device and a method for degrading ammonium perchlorate wastewater by using a hydrothermal-biological combined process. The device comprises: a Fe(0) hydrothermal primary degradation unit, which is used for mixing Fe(0) and ammonium perchlorate wastewater, adjusting the pH value of a reaction system to an acidic condition, and performing primary reductive degradation of ammonium perchlorate; a hydrothermal solution cooling unit, which is used for cooling the ammonium perchlorate hydrothermal solution having been subjected to primary degradation; and a biological-process secondary degradation unit, which is used for carrying out secondary degradation on the cooled ammonium perchlorate hydrothermal solution by adopting a biological process, and discharging the ammonium perchlorate hydrothermal solution after the ammonium perchlorate hydrothermal solution reaches the standard, wherein a supernatant in the hydrolysis and fermentation stage of kitchen waste and landfill leachate is used as the source of an electron donor, a carbon source and trace elements, and inoculated sludge comes from the domestication stage of ammonium perchlorate reducing bacteria. According to the method, the removal effect of the high-concentration ammonium perchlorate wastewater can be remarkably improved, and meanwhile, the economic rationality and the process operability of the process of removing the ammonium perchlorate wastewater by the biological process are remarkably improved.
Owner:XI AN JIAOTONG UNIV
Quaternary alkyl ammonium hypochlorite solution, method of producing the same, and method for processing semiconductor wafers
ActiveUS20210155878A1Reduce yieldReduce cleaningCationic surface-active compoundsAmino preparation from aminesHypochloriteReaction step
Provided is a method of producing a quatenary alkyl ammonium hypochlorite solution with an excellent storage stability. Specifically, provided is a method of producing a quaternary alkyl ammonium hypochlorite solution, the method including: a preparation step in which a quaternary alkyl ammonium hydroxide solution is prepared and the concentration of amines in the quaternary alkyl ammonium hydroxide solution is set to 20 ppm by mass or less; and a reaction step in which the quaternary alkyl ammonium hydroxide solution is brought into contact with chlorine gas, wherein the concentration of carbon dioxide of a gas phase in the reaction step is 100 ppm by volume or less and the pH of a liquid phase in the reaction step is 10.5 or more.
Owner:TOKUYAMA CORP
Ammonium perchlorate wastewater treatment method and system
PendingCN112429918AReduce concentrationReduce economic costsWater contaminantsMultistage water/sewage treatmentSodium acetateElectron donor
The invention discloses an ammonium perchlorate wastewater treatment method and system, and the method comprises the following steps: hydrolyzing corncobs as a raw material to generate furfural, and recovering sodium acetate in the furfural wastewater neutralization process; using sodium acetate for providing an electron donor and a carbon source for the process of reducing ammonium perchlorate byperchlorate reducing bacteria; and using waste iron powder as a source of an electron donor, and conducting secondary reduction of ammonium perchlorate. Ammonium perchlorate is reduced into chlorideions by adopting an autotrophic reduction and heterotrophic reduction two-stage degradation combined process, so that the concentration of the ammonium perchlorate wastewater is reduced, and the treatment of the ammonium perchlorate wastewater is completed. According to the method, the treatment cost of the ammonium perchlorate wastewater can be remarkably reduced, the removal effect of the ammonium perchlorate wastewater is improved, and meanwhile resource recycling of the furfural wastewater is achieved.
Owner:XI AN JIAOTONG UNIV
Gas generating agent composition, gas generating agent, preparation method and application
PendingCN114044729APedestrian/occupant safety arrangementInorganic oxygen-halogen salt explosive compositionsCopper nitrateAutomobile safety
The embodiment of the invention provides a gas generating agent composition, a gas generating agent, a preparation method and application, and relates to the technical field of automobile safety air bags. The gas generating agent composition comprises guanidine nitrate serving as a fuel, basic copper nitrate serving as a main oxidizing agent, an auxiliary oxidizing agent and a slag forming agent; wherein the auxiliary oxidant is ammonium perchlorate. The slag forming agent is at least one zirconate, and the content of each component is as follows in percentage by mass: 40-60% of guanidine nitrate, 25%-50% of basic copper nitrate, 0.5%-7% of ammonium perchlorate, and 1%-10% of a slag forming agent; and the oxygen balance of the gas generating agent composition is 0 to -3%. According to the gas generating agent composition, the gas generating agent, the preparation method and the application, the content of toxic and harmful gas generated during combustion of the gas generating agent and the content of suspended solids in the air meet the limit requirements of USCAR on the content of the toxic and harmful gas and the content of the suspended solids in the air by adjusting the formula components and the proportion of the gas generating agent.
Owner:HUBEI HANGPENG CHEM POWER TECH
Modified hydroxyl-terminated polybutadiene as well as preparation method and application thereof
ActiveCN112574335AOptimized formulaSimple preparation processNon-explosive/non-thermic compositionsPressure gas generationPolymer scienceBoronic acid
The invention relates to modified hydroxyl-terminated polybutadiene as well as a preparation method and application thereof; the modified hydroxyl-terminated polybutadiene has the following structure:HTPB is used as a starting material for chemical modification of the modified hydroxyl-terminated polybutadiene to prepare modified HTPB containing hydroxyl, tertiary amine group and borate group orcyano group at the same time; then the modified product partially replaces HTPB and is added into the formula of the hydroxyl-terminated polybutadiene propellant, wherein the borate group or cyano group in the molecular structure has the function of interfacial bonding of the nitramine filler, the tertiary amine group has the function of interfacial bonding of the ammonium perchlorate and also hasa function of inhibiting decomposition of the ammonium perchlorate, and the hydroxyl group has the function of in cross-linking enhancement in the curing stage. Besides, the modified HTPB integratingthe functions of crosslinking enhancement, interface bonding, combustion speed adjustment and the like has excellent compatibility with a traditional HTPB adhesive, and after the modified HTPB and the traditional HTPB adhesive are mixed, the overall polarity of a propellant adhesive matrix can be improved, and the thermodynamic compatibility with other functional auxiliaries is enhanced.
Owner:HUNAN UNIV
Safe nail shooting tablet and preparation method thereof
ActiveCN113929546AConvenient pre-installation and construction workStrong thrustNon-explosive/non-thermic compositionsBulk chemical productionPtru catalystAdhesive
The invention relates to a safe nail shooting tablet and a preparation method thereof, and belongs to the technical field of building construction. The nail shooting tablet is prepared from, by weight, 15-35 parts of damp-proof ammonium perchlorate, 5-15 parts of a rapid catalyst, 25-45 parts of superfine reaction powder, 10-25 parts of an ultrahigh-standard energy multiplier and 10-45 parts of superfine double-base powder. All the raw materials are mixed to prepare a batch, then the batch and an adhesive are mixed, kneaded and subjected to compression molding, and finally the surface is coated with composite coating glue. Irregular ammonium perchlorate sold in the market is recrystallized in a tetrahydrofuran-acetone solvent, a crystal form is modified, then the ammonium perchlorate is coated with a composite coating adhesive, the composite coating adhesive is prepared from nitrocotton, Arabic gum and a volatile solvent, after coating, the solvent is volatilized, a coating layer containing the nitrocotton is formed on the surface layer, Arabic gum forms a film to play a role in separation, ammonium perchlorate and internal batch are prevented from absorbing moisture and caking, a certain amount of nitrocotton has an ignition effect, and normal ignition of the nail shooting tablet is guaranteed.
Owner:浏阳象形精品烟花出口制造有限公司
A device and method for degrading ammonium perchlorate wastewater by hydrothermal combined biological method
ActiveCN112441705BAvoid serious harmPromote reductionWater contaminantsTreatment with aerobic and anaerobic processesHigh concentrationElectron donor
Owner:XI AN JIAOTONG UNIV
Method for extracting and recovering ammonium perchlorate from solid propellant by adopting swelling method
InactiveCN112194547AGood recovery rateHigh Recovery Extraction RatePerchloratesAmmonium perchlorate explosive compositionsPerchloric acidEthyl acetate
The invention relates to a method for extracting and recovering ammonium perchlorate from a solid propellant by adopting a swelling method. The method comprises the following steps: by taking an ethylacetate aqueous solution as a swelling solvent, forming a mixture with an HTPB solid propellant through a swelling reaction; and filtering the mixture, and heating the filtrate until the filtrate isdried to obtain the ammonium perchlorate crystal. According to the invention, the raw materials are wide in source, low in price, low in volatility, small in harm to human bodies and good in compatibility with HTPB propellants, and the extraction rate of ammonium perchlorate reaches 93%-98%.
Owner:XIAN AEROSPACE CHEM PROPULTION PLANT
A continuous crystallization device and method for spheroidizing large-particle ammonium perchlorate
ActiveCN109126183BContinuous production processHigh yieldPerchloratesSolution crystallizationRocketVacuum pump
Owner:ZHONGBEI UNIV +1
A preparation method of loaded ammonium perchlorate/graphene oxide three-dimensional energetic material
ActiveCN108786883BImprove securityComponent distribution is evenPhysical/chemical process catalystsPerchloric acidAmmonium chlorate
Owner:ARMY ENG UNIV OF PLA
Production process for 400 micron ammonium perchlorate
ActiveCN109621479BStable supersaturationPerchloratesSolution crystallizationPhysical chemistryPerchloric acid
Owner:HUBEI DONGFANG CHEM IND
A kind of treatment method of ammonium perchlorate waste water
ActiveCN111115842BGood removal effectThorough treatmentWater contaminantsWaste based fuelVolatile fatty acidsElectron donor
Owner:XI AN JIAOTONG UNIV
A kind of solid propellant with nitrated hydroxyl-terminated polybutadiene as binder
Owner:HUBEI INST OF AEROSPACE CHEMOTECHNOLOGY
Preparation method of ammonium perchlorate standard samples with different water contents
ActiveCN112683841AEvenly distributedSpread evenlyMaterial analysis by optical meansMoisture distributionPhysical chemistry
The invention provides a preparation method of ammonium perchlorate standard samples with different water contents, and belongs to the technical field of standard sample preparation. According to the method, the relationship between the porosity and the moisture content of the ammonium perchlorate powder is fully considered, the ammonium perchlorate standard sample is prepared by adopting different modes according to different moisture contents, and the moisture with different contents can be uniformly distributed in pores of the ammonium perchlorate powder. Meanwhile, the influence of standing time on moisture diffusion is fully considered, uniform diffusion of moisture among pores of the ammonium perchlorate powder can be ensured by limiting the standing time in the preparation process of the ammonium perchlorate standard samples with different moisture contents, and the moisture distribution in the obtained ammonium perchlorate standard samples is uniform.
Owner:SOUTHWEAT UNIV OF SCI & TECH +1
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