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94 results about "Solid oxygen" patented technology

Solid oxygen forms at normal atmospheric pressure at a temperature below 54.36 K (−218.79 °C, −361.82 °F). Solid oxygen O₂, like liquid oxygen, is a clear substance with a light sky-blue color caused by absorption in the red part of the visible light spectrum.

Method for directly preparing titanium and titanium alloy by titanium-containing waste residue

InactiveCN101457372ASpeed up recoveryNo electrolysisLiquid copperElectrochemistry
The invention relates to a method for directly preparing titanium and titanium alloy from titaniferous waste residues, and belongs to the technical field of electrochemical metallurgy. The method is characterized in that the titaniferous waste residues are made into an electrolysis electrode, and the electrolysis is performed in a crucible of an electrolytic cell by a solid oxygen permeable membrane in a specific molten salt electrolyte. The method comprises the following process steps: the titaniferous residues is processed by ball milling, then pressed and formed in a mould at 3-6MP, dried in the air, and then sinteredat the temperature of 1000-1100 DEG C for 2h to be made into an electrolysis cathode; molten salt is separated from an anode by an oxygen permeable membrane tube which only conducts oxyanion, the anode is liquid copper or copper alloy with saturated carbon powder, calcium chloride is taken as the molten salt electrolyte, the cathode and the anode are vertically arranged, the electrolytic temperature is 1000-1100 DEG C, the electrolytic voltage is 3.0-3.5V, the electrolysis time is 2-6h, and the cathodic products obtained by the electrolysis are metallic titanium and the titanium alloy. The method has the advantages of simple process, high electrolysis speed and high current efficiency.
Owner:SHANGHAI UNIV

Double-smelting dephosphorization process for high-phosphorus molten iron

The invention discloses a double-smelting dephosphorization process for high-phosphorus molten iron. The double-smelting dephosphorization process comprises a pre-dephosphorization process and a converter smelting process. The pre-dephosphorization process comprises the steps that pre-dephosphorization is performed by the adoption of a pre-dephosphorization furnace; a desiliconization slagging material is added to the high-phosphorus molten iron, and oxygen injection is performed for desiliconization slagging; the desiliconization slagging material is put into the furnace after desiliconization slagging, a solid oxygen agent is put into the furnace after dephosphorization slagging, meanwhile dephosphorization agent injection is performed, and inert gas bottom-blowing is performed so that mixing can be strengthened; and the pre-dephosphorized molten iron passes iron-slag separation equipment and then enters the converter smelting process. The dephosphorization process has the beneficialeffects of being stable, low in temperature, large in treatment capacity and the like, and the problem about high-phosphorus ultrahigh-phosphorus molten iron dephosphorization is solved thoroughly. The double-smelting dephosphorization process is suitable for high-phosphorus molten iron and ultrahigh-phosphorus molten iron, and the dephosphorization rate of pre-dephosphorization can reach 64-71%.According to the process, the molten iron pre-dephosphorization furnace and converter double-smelting are adopted, the high-phosphorus ultrahigh-phosphorus molten iron smelting operation can be achieved, the converter steelmaking load is lowered greatly, steelmaking is more efficient, and the smoothness and stability of the production procedures are guaranteed.
Owner:唐钢国际工程技术有限公司

Method for directly preparing titanium alloy by titanium concentrate powder

The invention relates to a method for directly preparing titanium alloy by titanium concentrate powder, and belongs to the technical field of the preparation process for metal titanium alloys. The method mainly comprises the following steps: taking Gossampinus titanium concentrate powder as a raw material to obtain a fine material of titanium concentrate through ball milling and screening; then performing tabletting and sintering; winding round tablets on a molybdenum rod by using a fine molybdenum wire to prepare a cathode, or sintering the ore concentrate powder to form circular sheets, putting the circular sheets into a small stainless steel crucible directly, immersing the integral small stainless steel crucible into molten salt in an electrolytic cell, leading the small stainless steel crucible out by using the molybdenum wire as the cathode; taking copper solution of saturated carbon dust in a solid oxygen-permeable membrane tube as an anode; taking a corundum crucible as a reaction vessel, and taking CaCl2 as a molten salt electrolyte; taking high-purity argon as protective gas; performing electrolysis at a temperature of 1,100 DEG C under the constant voltage of between 3.5 and 4.0 V for 2 to 6 hours, taking the electrolyzed cathode out, and washing and drying the electrolyzed cathode to prepare the titanium alloy. The method has the characteristics of short flow, high efficiency, no pollution, low cost and the like.
Owner:SHANGHAI UNIV

Oxygen chemical sensor for high-temperature and high-pressure hydrothermal system and preparation method of oxygen chemical sensor

The invention discloses an oxygen chemical sensor for a high-temperature and high-pressure hydrothermal system and a preparation method of the oxygen chemical sensor. The oxygen chemical sensor comprises a base, circular platform-shaped high-temperature-resistant insulating conical pads, a solid oxygen buffer agent, high-temperature-resistant insulating conical sleeves, circular platform-shaped solid electrolyte ceramic, circular platform-shaped high-temperature-resistant insulating ceramic, spongy inert metal layers, inert metal sheets and electrode leads. The oxygen chemical sensor, namely an oxygen sensor based on an electrochemical cell, is formed by combining all the components into a conical self-tightening mechanism, and can be utilized for in-situ direct measurement of the oxygen fugacity or the oxygen activity in the high-temperature (250 to 700 DEG C) and high-pressure (normal pressure to 100 MPa) hydrothermal system, so as to solve the problems that various conventional oxygen chemical sensors for a high-pressure hydrothermal system are low in operating temperature and operating pressure (the operating temperature and the operating pressure can hardly exceed 400 DEG C and 40 MPa simultaneously), low in response speed, and low in reliability when being applied to a complex concentrated water fluid sample.
Owner:INST OF GEOCHEM CHINESE ACADEMY OF SCI

Solid hydrogen peroxide preparation technology

ActiveCN103351961AOvercome underutilizationOvercoming the problem of liquid waste dischargeNon-surface-active detergent compositionsBleaching apparatusBleachSodium sulfate
The invention relates to the technical field of preparation of solid oxygen-bearing bleaching agent, in particular to a solid hydrogen peroxide preparation technology. The preparation technology comprises the step of kneading sodium sulfate, hydrogen peroxide and salt in a kneader at a certain proportion to obtain the finished product. According to the invention, the ordinary 30% hydrogen peroxide can serve as a basic material, the problems that the preparation cost is higher, the mother liquor is not fully utilized and waste liquid is discharged in the prior art are solved, the yield of hydrogen peroxide in the obtained finished product is more than 80 percent, the process period is shorter, the cost is lower, no three-waste emission exists, and the solid hydrogen peroxide preparation technology is suitable for large-scale popularization and application.
Owner:CHANGZHOU XIAOGUO INFORMATION SERVICES

High-capacity all solid oxygen generator

ActiveCN104176709ASolve the problem of generating harmful impurity gasesGuaranteed oxygen contentOxygen preparationEngineeringSTI Outpatient
The invention discloses a high-capacity all solid oxygen generator which comprises a cylindrical shell and an upper cover, wherein the upper cover is installed on the cylindrical shell and is provided with an ignition starting assembly which is connected with an oxygen generating medicine block by virtue of a lead, the oxygen generating medicine block is arranged inside the cylindrical shell, and a filter assembly is arranged between the ignition starting assembly and the oxygen generating medicine block. The oxygen generating medicine block is prepared from the following components in parts by weight: 3 parts of ignition block, 23 parts of first oxygen generating medicine block, 25 parts of second oxygen generating medicine block, 25 parts of third oxygen generating medicine block and 25 parts of fourth oxygen generating medicine block. The generator disclosed by the invention has the beneficial effects that the problem that harmful impure gases are generated by high-temperature side reactions is solved, and the generator can provide sufficient and pure oxygen for personnel in a tight space in an emergency.
Owner:三亚光远新型材料有限公司

Preparation method of oxygen slow release preparation for repairing of contaminated site

InactiveCN104560051AExcellent oxygen release performanceOxygen release rate controlled releaseTreatment using aerobic processesOther chemical processesAlkaline earth metalPhosphate
The invention provides a preparation method of an oxygen slow release preparation for the repairing of a contaminated site, and belongs to the field of environmental protection technology. The adopted process comprises the following steps: firstly, mixing alkaline earth hyperoxide with dihydric phosphate and inorganic ammonium salt uniformly to obtain mixed solid particles; secondly, the mixed solid particles are coated with a long-chain tertiary amine ionic surface active agent and dried to obtain solid oxygen slow release preparation particles, so as to achieve the purpose that oxygen can be slowly released from the oxygen slow release preparation in soil and underground water; thirdly, the coated solid oxygen slow release preparation particles and permeable materials can be mixed uniformly, so that the permeability of an oxygen release material can be improved. With the adoption of the preparation method of the oxygen slow release preparation for repairing of the contaminated site, the prepared oxygen slow release preparation is especially suitable for in-situ pollution repairing of oil pollutants like benzenes, methyl tert-butyl ether and petroleum hydrocarbon; the oxygen slow release preparation can slowly release reactive oxygen, at the same time, load and slowly release nutrient substances needed by organisms, no pollution is caused to the environment, and the biological degradability is achieved.
Owner:ESD CHINA LTD

Method for preparing AB5 type hydrogen-storage alloy directly from metal oxide mixture

The invention relates to a method for direct preparation of AB5 type hydrogen storage alloys through metal oxide mixture, belonging to the solid oxygen permeable membrane electrolysis method alloy preparation technology technical field. The method mainly utilizes the solid oxygen permeable membrane technology and an electrochemical method to directly prepare the AB5 type hydrogen storage alloys through the oxide mixture of target alloys. The metal oxide mixture which forms the elemental constituent of the hydrogen storage alloys is pressed into a wafer which is used as a cathode, and graphite is used as an anode; the metal oxide mixture wafer is arranged inside a solid oxygen permeable membrane pipe; the metal oxide mixture wafer and the graphite which are used as the cathode and the anode are arranged inside a graphite crucible electrolytic cell which is stored with copper liquid, and then electrolysis is performed after galvanization and heating; the electrolytic voltage is 0 to 4.5 volts and the electrolytic current is 0 to 6.0 amperes; finally the AB5 type hydrogen storage alloys are obtained. The compositions of raw materials used by the AB5 type hydrogen storage alloys are as follows: La2O3 of 18.1+-0.46 weight percent, CeO2 of 8.54+-0.28 weight percent, Pr2O3 of 0.73+-0.18 weight percent , Nd2O3 of 2.46+-0.18 weight percent, MnO2 of 6.42+-0.24 weight percent, Al2O3 of 1.77+-0.30 weight percent , Co2O3 of 11.17+- 0.22 weight percent and residual NiO.
Owner:SHANGHAI UNIV

Device and method for rapidly producing oxygen

The invention relates to a device and method for producing oxygen, in particular to a device and method for rapidly producing oxygen, aiming at the problems of the existing solid oxygen generator, such as complicated structure, too many used reagents and high cost, and the problem of an automatic oxygen generator that hydrogen peroxide is easily decomposed, hard to control and harmful to human bodies. The device for rapidly producing the oxygen comprises a container, an oxygen discharging pipe, a triggering pipe, a molecular sieve and oxygen producing reactants, wherein the oxygen producing reactants are put in the container; the molecular sieve is arranged at the opening of the container and forms a reacting cavity together with the container; the lower end of the triggering pipe is inserted into the oxygen producing reactants, and the upper end of the triggering pipe penetrates through the molecular sieve and is exposed out of the reacting cavity; the lower end of the oxygen discharging pipe penetrates through the molecular sieve to be inserted into the reacting cavity and is arranged above the oxygen producing reactants; and the oxygen producing reactants include sodium superoxide, white alum and silicon dioxide. The device and method are used for producing the oxygen.
Owner:HARBIN INST OF TECH

Oxygen candle grain and preparation method thereof

InactiveCN107867675AMake sure it doesn't burn outLow calorific valueOxygen preparationSodium chlorateCandle
The invention provides an oxygen candle grain and a preparation method thereof. The oxygen candle grain comprises an inflammable drug layer formed by an inflammable drug, a grain inner core formed byan inner core drug as well as a grain outer ring formed by an outer ring drug, wherein the inflammable drug layer is located at the top end of the oxygen candle grain; the grain outer ring is of a cylindrical structure; the grain inner core is arranged in the cylindrical structure of the grain outer ring; both the grain inner core and the grain outer ring are located below the inflammable drug layer. The inner core drug contains a small quantity of metal powder fuel; the outer ring drug comprises sodium chlorate and a catalyst in a proper proportion as main components and contains no metal fuel. By means of the design, the outer ring drug is catalytically decomposed by heat transmitted by the inner core drug, so that heat emission of the oxygen candle is reduced greatly. The oxygen candlegrain is applicable to various specifications of solid oxygen generators and applies to the fields of marine vessels, aerospace, mines, self-rescue from various disasters and the like. By means of oxygen candle grain, the heat production quantity of the oxygen candle is small, oxygen evolution is stable, and the overall structure of the oxygen candle is stable.
Owner:HUBEI INST OF AEROSPACE CHEMOTECHNOLOGY

Novel technology for producing medium/low carbon manganese iron by air three-times blowing method

InactiveCN103572057AGood production process controllabilityGood product quality controllabilityFurnace temperatureHigh carbon
The invention provides a novel technology for producing medium / low carbon manganese iron by an air three-times blowing method. The novel technology comprises the following steps: blowing primary air into a high carbon manganese iron flux, which is different from blowing oxygen by which high temperature evaporation manganese is generated and blowing components are damaged, and completely decarburizing through powerful dynamics stirring; blowing secondary air on a high carbon manganese iron flux liquid level so as to burn carbon monoxide generated by primary-air blowing for increasing heat, and adding more manganese ores so as to increase manganese oxide solid oxygen which facilitates decarburization and the recovery of manganese metal; blowing tertiary air and fuel gas into a furnace at the same time so as to provide external heat for increasing the furnace temperature, conditionally adding more manganese ores in an oxidation period and more reducing agent in a reduction period, conditionally adding a refinement period and meanwhile adding the manganese ores and the reducing agent so as to ensure the blowing technological operation and adjust product components for ensuring the quality.
Owner:王洪东
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