The invention relates to an organic
silicon hydrolysate pyrolysis method and device of
solvent oil thermal drive circulation. Double spiral channels in a form of spiral-like
plate heat exchanger are coaxially arranged in the middle of a
pyrolysis device; the upper and lower ends of one spiral channel of the double spiral channels are not sealed, so that the spiral channel can serve as a pyrolysischannel, and the upper and lower ends of the other spiral channel are sealed to form a heat exchange medium channel;
solvent oil is distributed in an annular space between the column consisting of thepyrolysis channel and the double spiral channels and the
pyrolysis device; a mixture of organic
silicon hydrolysate and KOH solution is fed into the pyrolysis channel; the heat exchange medium of theheat exchange channel provides heat to the pyrolysis channel; the organic
silicon hydrolysate is mixed with
solvent oil in the pyrolysis channel, and experiences
vaporization while reacting; bubblesrise to drive the liquid in the pyrolysis channel to go up to the top of the pyrolysis channel; after gas-liquid separation, the solvent oil, the unreacted organic silicon hydrolysate and the KOH solution go down to the bottom of the pyrolysis device through the annular space, forming natural circulation. Without a stirring device, the heat and
mass transfer efficiency is high, and local overheating is avoided; the
production cycle of the device is prolonged, and the alkali consumption is reduced; moreover, the annulus yield as well as the quality of D4 and DMC is improved, and the operation is stable, safe and reliable.