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132results about How to "Right melting point" patented technology

High-entropy brazing filler metal for brazing non-oxide ceramics and non-oxide ceramic composite material and preparation method of brazing filler metal

The invention relates to a high-entropy brazing filler metal and a preparation method thereof, and particularly relates to a high-entropy brazing filler metal for brazing non-oxide ceramics and the composite material of the non-oxide ceramics and the preparation method of the brazing filler metal, aiming to solve the problem that the brazing filler metal at the joint of the non-oxide ceramics and the ceramic composite material which are soldered together is unreliable in performance at a temperature higher than 500 DEG C in the prior art. The brazing filler metal comprises the following components in parts by weight: 18 to 24 parts of Ni, 14.3 to 19 parts of Cr, 16.8 to 22.5 parts of Co, 15.9 to 21 parts of Fe, 10.1 to 13.5 parts of Cu, and 0 to 24.9 parts of Ti or TiH2. The preparation method comprises the following steps of: carrying out vacuum melting on the weighed components at the temperature of 1200 to 1800 DEG C, performing linear cutting and carrying out foiling or composite tabletting on the components, so as to obtain the brazing filler metal; or the preparation method comprises the following steps of: carrying out ball-milling on the components in a ball material mass ratio of (12-16):1, and then tabletting and cleaning the components to obtain the brazing filler metal. The strength of the alloy joint obtained by using the method reaches 35 to 71 MPa, and the strength retention of the alloy joint at a high temperature of 800 DEG C exceeds 67%.
Owner:HARBIN INST OF TECH

Tundish covering flux

ActiveCN102581240ASuitable melting pointGood spreadabilitySlagMelting layer
The invention discloses a tundish covering flux, which comprises the following components by mass: 5-10% of CaCO3, 60-80% of CaO+SiO2, 3.0-6.0% of Al2O3, 6.0-10.0% of MgO, 1.0-3.0% of Na2O, 0-0.5% of fixed carbon, 0-10.0% of lightweight bulk material, 2-6.0% of binder, 0-0.5% of water and the balance of inevitable impurities, wherein the ratio of CaO to SiO2 is 1.1-1.5. The tundish covering flux is added into molten steel, and then a three-layer structure comprising a slag formation layer, a sintering layer and a melting layer is formed on the molten steel. The tundish covering flux does not incrust in a using process, and has a proper melting point, spreadability and high heat-preservation performance; and the excessive temperature drop of the molten steel in a tundish can be prevented, and a slag crust is prevented from being formed on the surface of the molten steel.
Owner:BAOSHAN IRON & STEEL CO LTD +1

High-temperature solder for brazing TiAl-based alloy and preparation method thereof

The invention discloses a preparation method of a high-temperature solder for brazing a TiAl-based alloy, and relates to the high-temperature solder and the preparation method thereof. The invention solves the problems that a TiAl-based alloy brazing joint obtained by using the conventional solder is low in use temperature and has low performance under a high-temperature environment, the used solder is high in price, and the solder preparation technology is complicated. The solder is made of Ti, Ni and V. The preparation method comprises the following steps of: weighing raw materials; 2, filling the raw materials in arc melting equipment, vacuumizing, filling argon, melting and alloying, and repeatedly melting and cooling. Compared with the conventional solder, the solder prepared by the invention has an appropriate melting point and good wetting property; the solder components are free of noble metals, such as Ag, Zr and the like, so the cost is low; the brazing joint has high strength under the high-temperature environment of 800 DEC, and is applicable to various joints; and the preparation method is simple and convenient.
Owner:HARBIN INST OF TECH

Mg-Gd-Y-Zr magnesium alloy refining flux and producing method thereof

The invention provides an Mg-Gd-Y-Zr magnesium alloy refining flux and a production method thereof. The chemical components of the flux are mixed according to the following mass percentages: potassium chloride of ranging from 30 to 50 percent, barium chloride of ranging from 5 to 20 percent, sodium chloride of ranging from 2 to 10 percent, calcium chloride of ranging from 10 to 20 percent, calcium fluoride of ranging from 2 to 8 percent, cryolite of ranging from 1 to 5 percent, gadolinium compound of ranging from 3 to 8 percent, yttrium compound of ranging from 3 to 8 percent, and zirconium compound of ranging from 2 to 8 percent, wherein, the gadolinium compound is gadolinium chloride, gadolinium carbonate or gadolinium fluoride, the yttrium compound is yttrium chloride, yttrium carbonate or yttrium fluoride, the zirconium compound is zirconium tetrachloride or potassium zirconium fluoride. The flux has good melting point, viscosity, wettability and the slag removing performance which is improved greatly. Because the flux does not contain magnesium chloride or react with the lanthanon such as gadolinium and yttrium, the chemical reaction loss of the lanthanon in the refining process is not caused, thereby being particularly suitable for the refining purifying process of the Mg-Gd-Y-Zr magnesium alloy and improving the refining effect of the magnesium fused mass.
Owner:SHANGHAI JIAO TONG UNIV

High-entropy alloy for brazing of TiAl and nickel-based high-temperature alloy and preparation method

The invention discloses a high-entropy alloy for brazing of TiAl and nickel-based high-temperature alloy and a preparation method. The high-entropy alloy comprises the following chemical components inatomic percent: 15-25% of Al, 10-20% of Cu, 10-20% of Co, 10-20% of Fe, 10-20% of Cr, 5-15% of Ni and 5-15% of Ti. The preparation method comprises the following steps: weighing raw materials required by smelting according to the components of brazing filler metal; smelting the raw materials to obtain a high-entropy alloy brazing filler metal ingot; and preparing a high-entropy alloy amorphous foil belt by utilizing a vacuum quenching rapid solidification technology, or preparing high-entropy alloy brazing filler metal powder by adopting a vacuum gas atomization technology. The high-entropy alloy brazing filler metal has very high mixed entropy, the structure of the high-entropy alloy brazing filler metal is mainly a solid solution structure, the high-entropy alloy brazing filler metal can be used for brazing connection between two extremely different materials, namely TiAl alloy and nickel-based high-temperature alloy, and can keep good compatibility with the two welded base materials simultaneously, and high connection strength is obtained.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS

Welding method of four-wing octagonal radio frequency quadrupole cavity

The invention relates to a welding method of a four-wing octagonal radio frequency quadrupole cavity. The welding method includes the steps that finish machining is conducted on the inner surfaces and the outer surfaces of electrodes and side wings; the electrodes and the side walls are cleaned; electrode soldering flux tanks are arranged, and soldering flux filling is conducted; the electrodes and the side wings are combined and spliced; the assembling gap of welding faces is measured and regulated; and a vacuum cavity is formed by welding the electrodes and the side wings through a vacuum brazing furnace. The cavity prepared through the method mentioned above comprises the horizontal electrodes, the vertical electrodes and the side wings; and the corresponding electrode soldering flux tanks are arranged on the two sides of each electrode, the soldering flux tanks are filled with silver-copper alloy soldering flux, and the size of the soldering flux welding tanks is regulated according to the size of the welding faces. The welding method has the beneficial effects that the welding process is simple; by selecting the soldering flux and controlling the temperature of the welding process, outflow of the soldering flux towards the interior of the cavity is reduced to a great extent, and the soldering flux is uniformly diffused; and no soldering flux exits in the cavity, the problem that high-pressure ignition is generated when the RFQ cavity operates at a high frequency can be solved, and normal operation of the RFQ cavity is ensured.
Owner:上海克林技术开发有限公司

Method for preparing ternary nitric acid molten salt phase change heat storage material

The invention discloses a method for preparing a ternary nitric acid molten salt phase change heat storage material. The method comprises the steps of 1, weighing sodium nitrate, potassium nitrate and neodymium nitrate, and crushing sodium nitrate, potassium nitrate and neodymium nitrate through a mechanical crushing method to obtain sodium nitrate powder, potassium nitrate powder and neodymium nitrate powder; 2, mixing the sodium nitrate powder, the potassium nitrate powder and the neodymium nitrate powder to obtain a ternary nitric acid molten salt phase change heat storage material prefabricated body; 3, first melting the ternary nitric acid molten salt phase change heat storage material prefabricated body and then sequentially performing drying and ball milling crushing treatment to obtain the ternary nitric acid molten salt phase change heat storage material. According to the method for preparing the ternary nitric acid molten salt phase change heat storage material, the problems that an existing molten salt phase change heat storage material is high in cost, long in production cycle and complex in process in the preparation process are solved, and the prepared ternary nitric acid molten salt phase change heat storage material has the advantages of being wide in use temperature range, high in heat storage capability, low in corrosiveness and good in liquidity.
Owner:辽宁卓仑科技有限公司

Low-silver copper-based solder free of spillover phenomenon during weld period

The invention discloses a low-silver copper-based solder free of a spillover phenomenon during a weld period. Aiming at the defect that the spillover phenomenon of the solder often occurs when brazing is performed by using traditional low-silver copper-based solder, the invention aims to provide the low-silver copper-based solder which is controllable in flowability and is free of the spillover phenomenon of the traditional low-silver copper-based solder during a process of welding copper and copper alloy. The low-silver copper-based solder disclosed by the invention is realized through the following technical scheme: the low-silver copper-based solder free of the spillover phenomenon during the weld period comprises the following components in weight percent: 6.6-7.8 percent of phosphorus (P), 0.5-2.2 percent of silver (Ag), 0.01-0.4 percent of indium (In), 0.001-0.2 percent of silicon (Si), 0.001-0.1 percent of rare earth and the balance copper (Cu).
Owner:浙江信和科技股份有限公司

Method for recovering rhodium from inactive rhodium-containing homogeneous catalyst

The invention mainly belongs to the technical field of rhodium recovery and particularly relates to a method for recovering rhodium from an inactive rhodium-containing homogeneous catalyst. The methodcomprises the following steps that organic matter in the rhodium-containing homogeneous catalyst is recovered in a distillation mode at first, and rhodium concentrate is obtained; then the rhodium concentrate is mixed with transitional metal M, a reduction agent and a slag former, rhodium is recovered in a smelting manner and forms a low-melting-point Rh-M alloy together with the transitional metal M, then the Rh-M alloy is subjected to electrolysis or acidolysis to obtain rhodium powder, finally the rhodium powder is smelted through an electric-arc furnace, and accordingly a rhodium ingot isobtained. The method is suitable for various inactive rhodium-containing homogeneous catalysts, the situation that the organic matter is directly incinerated to cause air pollution is avoided, meanwhile, the high-melting-point rhodium can be converted into the low-melting-point high-reactivity Rh-M alloy, and subsequent rhodium smelting and purification are facilitated. The method has the advantages of being high in rhodium recovery rate and production efficiency, free of pollution and suitable for industrial application.
Owner:UNIV OF SCI & TECH BEIJING

High-entropy alloy brazing filler metal and preparation method thereof

The invention discloses high-entropy alloy brazing filler metal and a preparation method thereof. The high-entropy alloy brazing filler metal comprises the following chemical components in atomic percent: 10-20% of Al, 10-20% of Cu, 10-20% of Co, 10-20% of Fe, 10-20% of Ni, 10-20% of Cr, 4-12% of Si and 4-12% of B. The preparation method comprises the following steps: weighing raw materials required for smelting according to the components of the brazing filler metal; smelting the raw materials to obtain a high-entropy alloy brazing filler metal ingot; and preparing a high-entropy alloy amorphous foil belt by utilizing a vacuum quenching rapid solidification technology, or preparing high-entropy alloy brazing filler metal powder by adopting a vacuum gas atomization technology. The high-entropy alloy brazing filler metal has very high mixed entropy, the structure of the high-entropy alloy brazing filler metal is mainly a solid solution structure, the high-entropy alloy brazing filler metal can be used for brazing connection between two extremely different materials, namely TiAl alloy and nickel-based high-temperature alloy, and can keep good compatibility with the two welded base materials simultaneously, and high connection strength is obtained.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS
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