The invention belongs to the field of preparation of inorganic nonmetallic materials, and particularly relates to a preparation method of a
copper cobaltate porous microrod and
nickel foam
composite electrode material. The preparation method comprises the steps that clean
nickel foam is soaked in an
oxalic acid aqueous solution, and a mixed
aqueous solution of soluble
copper salt and soluble
cobalt salt is dropwise added into the
oxalic acid aqueous solution under the condition of stirring at
room temperature; stirring reaction is conducted till micron-structure precursors grow out on the surface of the
nickel foam, the nickel foam is taken out, cleaning,
drying and calcining are sequentially conducted, and the
copper cobaltate porous microrod and nickel foam
composite electrode material is obtained. According to the preparation method of the copper cobaltate porous microrod and nickel foam
composite electrode material, the technology is simple and easy to carry out, the product purity is high, the preparation cost is low, the
diameter of a copper cobaltate microrod ranges from 0.5
micrometer to 2 micrometers, the length of the copper cobaltate microrod is about 5-10 micrometers, the size of a nano pore channel ranges from 10 nm to 50 nm, the uniformity and the
dispersity of the product are both good, the copper cobaltate porous microrod and nickel foam composite
electrode material can be directly applied to
electrode materials of supercapacitors, the production technology is simple, and the preparation method is prone to be applied to practical large-scale production.