The invention discloses a magnetic hollow micro-nano material, a preparation method and application thereof, and belongs to the technical field of nano materials. According to the magnetic hollow micro-nano material and the preparation method and application thereof, the magnetic hollow
micro nano material prepared by a one-step liquid-phase reduction-oxidation method has novel structure and formation mechanism, the contents of Cu and Ni and the composition, feature, and structure of the magnetic hollow micro-nano material can be regulated by changing the
reaction temperature, time, stirring speed, gas flow size, and reactant concentration, wherein the
diameter of a micro-
nano tube is 0.1 to 2 [mu]m, the length is 2 to 12 [mu]m, and the wall thickness is 10 to 140 nm; the
diameter of a micro-nano sphere is 0.2 to 5 [mu]m, and the wall thickness is 10 to 180 nm. Because the magnetic hollow micro-nano material is good in dispersibility, good in homogeneity and has good
microwave absorption characteristics, the magnetic hollow micro-nano material is widely used in the fields such as
microwave absorbing and shield, electrocatalysis,
lithium ion batteries and
surface enhanced Raman spectroscopy. In addition, the disclosed preparation method is easy to operate, the environment-friendly effect is realized, industrial application potential is good, and the magnetic hollow micro-nano material and the preparation method are suitable for market promotion and application.