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97 results about "Tributyrin" patented technology
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Tributyrin is a triglyceride naturally present in butter. It is an ester composed of butyric acid and glycerol. Among other things, it is used as an ingredient in making margarine. It is present in butter and can be described as a liquid fat with an acrid taste.
Inclusion complexes and methods for making the same
ActiveUS20160263245A1Hydroxy compound active ingredientsPharmaceutical non-active ingredientsOral medicationΓ cyclodextrin
The invention provides novel formulations comprising a stable inclusion complex of tributyrin and a cyclodextrin. In one particular embodiment, the formulation comprises an oven dried inclusion complex of tributyrin and γ-cyclodextrin that is effective in minimizing or preventing the unpleasant taste and odor of tributyrin, thus making it suitable for oral administration and delivery to the digestive tract and intestines. The invention provides compositions of these inclusion complexes and methods of using them that are advantageous as food, medicinal and other products, where the negative sensory properties of tributyrin can be a liability.
Owner:THE BOARD OF TRUSTEES OF THE UNIV OF ILLINOIS
Additive for balancing gastrointestinal health of animals
InactiveCN102187945AFully digestedFully absorbedAnimal feeding stuffAccessory food factorsAnimal scienceTributyrin
The invention provides an additive for balancing the gastrointestinal health of animals, which is prepared by absorbing 3 to 15 percent of tributyrin, 21.5 to 52.5 percent of lactic acid and 3.5 to 7.5 percent of formic acid with special carrier white black carbon by grade and layer respectively and then combining the mixture with 1 to 10 percent of glutamine. The additive has the effects of controlling diarrhea and accelerating restoration of injured intestinal tract, and starting from a philosophy of balancing the relationship between the gastropore and the intestinal tract, saving resources, reducing environment loads and improving quality of livestock products, a comprehensive gastrointestinal health management scheme is provided.
Owner:SHANGHAI WELL ADD BIOTECH
Fiber-derived compound additive for pigs and preparation method thereof
ActiveCN103766655AImprove developmentGood for healthFood processingAnimal feeding stuffFood additiveFiber
The invention discloses a fiber-derived compound additive for pigs and a preparation method of the additive, and relates to the field of animal feed. The method takes tributyrin, rice hull powder, corncob, calcium acetate, sodium propionate, stearic acid and glyceride as raw materials, and comprises the steps of firstly preparing fatty acid particles coated by microencapsulations; after that, evenly mixing betaine, wheat bran, oat bran, psyllium, inulin, pectin, guar gum, sodium alginate and Arabic gum step by step, and adding the fatty acid particles coated by microencapsulations into the mixture; finally, adding corn starch, and evenly mixing to obtain the fiber-derived compound additive for the pigs. After the fiber-derived compound additive for the pigs is adopted, the development and health of intestinal tracts of piglets are effectively promoted, the reproductive performance of the pigs is improved, the health condition of the animal organism is improved, and the incidence rate of diseases can be reduced.
Owner:SICHUAN AGRI UNIV
Method for preparing tributyrin
ActiveCN104045556AAchieve the purpose of separationPreparation from carboxylic acid halidesGlycerolVaporization
The invention provides a method for preparing tributyrin. The method comprises the following steps: reacting glycerinum with butyryl chloride by taking organic alkali as a acid-binding agent, thereby obtaining a mixture containing tributyrin, wherein the mole ratio of the three materials, namely, glycerinum, butyryl chloride and organic alkali, is 1:(3-3.3):3.3. The method further comprises the following steps: extracting a mixture containing tributyrin by using water, collecting an organic phase, and performing reduction vaporization to remove a solvent in the organic phase, thereby obtaining tributyrin. In the method, the mole ratio of butyryl chloride to glycerinum is kept at (3-3.3):1 during reaction, and massive over amount is not needed. In addition, after the reaction is completed, residual trace butyryl chloride can be hydrated into butyric acid and hydrochloric acid in the following water washing process and can be carried away by a water phase together with residual glycerinum, thus a purpose that butyryl chloride is separated from a target object is achieved.
Owner:FEED RESEARCH INSTITUTE CHINESE ACADEMY OF AGRICULTURAL SCIENCES
Creep feed for enhancing piglet immunity of piglets and preparation method thereof
PendingCN110934232AEasy feedingPromote early developmentFood processingAnimal feeding stuffBiotechnologySucrose
The invention discloses a creep feed capable of enhancing immunity of piglets and a preparation method thereof. The creep feed comprises the following components in parts by weight: 20 to 40 parts ofcorn, 5 to 15 parts of puffed corn; 5 to 15 parts of whey powder; 5 to 10 parts of puffed soybeans; 5 to 15 parts of soybean meal, 1 to 5 parts of fermented soybean meal; 5 to 10 parts of skim milk powder; 1 to 5 parts of sucrose, 1 to 5 parts of fish meal, 0.5 to 2 parts of soybean oil, 0.1 to 0.2 part of tributyrin; 1 to 1.5 parts of an organic compound acidifier; 0.5 to 1.0 part of an organic mineral substance premixing agent; 0.02 to 0.05 part of a vitamin premix; 0.05 to 0.2 part of a compound enzyme preparation; 0.1 to 0.2 part of a composite micro-ecological preparation; 0.1 to 0.5 partof oligosaccharide, 0.01 to 0.05 part of plant essential oil, 0.1 to 0.8 part of stone powder, 0.6 to 1.5 parts of calcium hydrophosphate, 0.1 to 0.4 part of table salt, 0.6 to 1.5 parts of compoundamino acid, 0.05 to 0.3 part of choline chloride and 0.03 to 0.08 part of a mildew preventive; the cfeed can promote ingestion of the piglets, guarantee normal physiological functions of organisms, promote development of immune organs, improve immunity of the piglets, enhance disease resistance and reduce diarrhea of the weaned piglets.
Owner:HUNAN JIUDING TECH GROUP
Tributyrin solid granular preparation, and preparation method and application thereof
InactiveCN104106734AEasy to prepareSuitable for industrial productionAnimal feeding stuffAccessory food factorsSilica gelTributyrin
The invention discloses a tributyrin solid granular preparation. Liquid tributyrin is absorbed or bonded on the surface or in pores of a granular white carbon black silica gel. The preparation disclosed by the invention realizes solid granular treatment of the liquid tributyrin, increases stability and bioactivity of tributyrin, and enables tributyrin to have a controlled sustained release effect in animal intestines.
Owner:ZHEJIANG UNIV
Liquid feed capable of improving immunologic function and antioxidative function of live pigs and preparation method thereof
InactiveCN106212948AEnhance immune functionImprove growth functionFood processingAnimal feeding stuffWeight gainingAnimal science
The invention discloses liquid feed capable of improving the immunologic function and antioxidative function of live pigs and a preparation method thereof. According to the liquid feed, wheat middling is taken as a main raw material and cooperates with tomato meal, broccoli residues, red beans, iron glycine, a lotus leaf fermentation substance and the like, therefore, the immunologic function of the live pigs can be improved, the ill getting rate is decreased, growth and weight gain of the pigs are accelerated, the oxidation resistance of the pigs is enhanced, and the nutrition and mouthfeel of port are improved; the wheat middling can replace usage of the raw materials such as soybean meal and corn, and therefore the feed cost is reduced; lily seeds, green plum pulp and dendrobe flowers are cooperatively used, therefore, the growth mechanism of the pigs can be improved, and growth and development can be promoted; tributyrin, alanyl glutamine dipeptide and calcium propionate are cooperatively used, therefore, the palatability of the feed can be improved, and the nutritional value of the feed can be increased.
Owner:MAANSHAN WUGU POULTRY IND SPECIALIZED COOP
Trifloxystrobin synthesizing method
The invention discloses a trifloxystrobin synthesizing method, and relates to the preparation of trifloxystrobin in organic chemicals. The trifloxystrobin synthesizing method comprises the following steps of using hydroxy methyl phenylacetic acid lactone as raw material to react with TBN (tributyrin), absolute methanol and sodium methoxide to obtain (E)-3-keto-4-(isonitroso)isochroman; using the (E)-3-keto-4-(isonitroso)isochroman to react with acetone and potassium carbonate, and dropwise adding the acetone solution of dimethyl sulfate after a large amount of bright yellow solids occurs, so as to obtain (E)-3-keto-4-(methoxyimino)isochroman; dissolving the obtained (E)-3-ketone-4-(methoxyimino)isochroman by methanol, and dropwise adding thionyl chloride under the low-temperature condition to prepare (E)-2-chlororated methyl-alpha-methoxyimino methyl phenylacetate; after the catalysis of 3-(trifluoromethyl)acetophenone and hydroxylamine hydrochloride, using absolute ethyl alcohol and as solvent to obtain light earthy yellow solid (E)-3-(trifluoromethyl)acetophenone oxime; enabling the (E)-2-bromomethyl-alpha-methoxyimino methyl phenylacetate and the (E)- 3-(trifluoromethyl)acetophenone oxime to react in a DMF (dimethyl formamide) solution of the potassium hydroxide, so as to obtain the white solid of trifloxystrobin.
Owner:JIANGSU CHANGQING AGROCHEMICAL CO LTD
Formula feed for mixedly breeding shrimps and preparation method thereof
InactiveCN106260588AReduce anti-nutritional factorsImprove absorption and utilizationFood processingClimate change adaptationAnimal scienceDigestion
The invention relates to a formula feed for mixedly breeding shrimps and a preparation method thereof. In the formula, fermented soybean meal is used, and anti-nutritional factors contained in soybean meal vegetable protein are effectively decreased; the advantage of improving palatability is achieved, and nutrient digestion and absorption and intestinal health are improved; by adding wall-broken yeast powder, the shrimp immunity can be improved, and bacteriotoxin, aflatoxin, vomitoxin and the like in the feed can be adsorbed; by adding the raw materials such as fish meal, domestic fish meal, shrimp meal, the fermented soybean meal and squid liver paste, nutrition arrangement is reasonable, the attractant effect is good, the absorption and utilization rate of the feed is effectively increased, and the feed safety is effectively improved; by adding tributyrin, epithelial cells of the shrimp intestines can be repaired, the intestinal health is maintained, and occurrence of enteritis is reduced; by adding bile acid and an agent beneficial for the liver and the gall, the shrimp liver health is effectively guaranteed, and the shrimp constitution is improved.
Owner:TIANJIN CHENHUI FEED
Tributyrin microcapsule with maltodextrin and cyclodextrin as wall material
InactiveCN108770948AGood solubility of powderImprove odorEdible oils/fats ingredientsEdible oils/fats production/working-upSolubilityWater baths
Belonging to the technical field of grease microcapsulation, the invention discloses a tributyrin microcapsule with maltodextrin and cyclodextrin as the wall material. The preparation process includes: adding maltodextrin and cyclodextrin into distilled water, conducting water bath heating at 50-80DEG C, and mixing the substances evenly, then adding tributyrin and an emulsifying agent, and fully stirring the substances evenly; and carrying out shearing, homogenizing and spray drying on the obtained mixture so as obtain a tributyrin microcapsule powder product. The method adopted by the invention has the characteristics of simple process and convenient operation. The prepared tributyrin microcapsule powder has the characteristics of small peculiar smell, and good stability and solubility, obviously improves the defects of peculiar smell, insolubility in water, poor fluidity and the like in tributyrin, and expands the application of tributyrin.
Owner:JIANGNAN UNIV
Method for clathrating tributyrin by enzyme method
ActiveCN108642105AReduce separation and purification stepsSimple processAnimal feeding stuffAccessory food factorsCyclodextrinTributyrin
The invention discloses a method for clathrating tributyrin by an enzyme method, and belongs to the technical field of grease microencapsulation. According to the method, cyclodextrin synthesized by the enzyme method and tributyrin clathrated by cyclodextrin are combined. The method comprises the step of preparing the cyclodextrin by the enzyme method using CGT enzymes; the tributyrin is added inthe preparation process; after the reaction, Tween is added; and homogenizing and spray drying are performed. The effect of the finally obtained tributyrin powder is much better than the single cyclodextrin clathration effect. The method provided by the invention has the advantages that the process is simple; the cost is low; the operation is convenient; non-toxic harmless and pollution-free effects are achieved in the reaction process; no toxic reagent is remained; the clathration effect is obvious; and the better utilization of a nutritive additive of the tributyrin in the practical production is facilitated.
Owner:JIANGNAN UNIV
Preparation method of low-calorie functional fat
ActiveCN102191285ADetermine the processDetermine parametersFermentationLipid formationReaction temperature
The invention relates to a preparation method of low-calorie functional fat, belonging to the research field of functional lipid. The method comprises the following steps: tributyrin and methyl stearate are used as raw materials and 1,3-specific Lipozyme RMIM is used as catalyst to perform ester exchange reaction under the conditions of reduced pressure, heating and rotating, cooling, dissolving and centrifuging are performed after some time to remove enzyme, and rotary steaming is performed to obtain the low-calorie functional fat. The conversion rate of methyl stearate in the reaction product, the content of low-calorie functional fat (SSL and LLS) and the content of the unexpected product glycol tristearate are used as indexes and the factors such as reaction time, substrate molar ratio, the additive amount of enzyme and reaction temperature are optimized to determine the preparation technology. The method lays foundations for the regulations of the short carbon chains and long-carbon-chain fatty acid of triglyceride and the construction of the low-calorie functional fat processing technology which can meet different demands on processability.
Owner:JIANGNAN UNIV
Feed with function of protecting intestinal barriers of piglets
InactiveCN108294181AIncrease feed intakeIncrease daily weight gainFood processingAnimal feeding stuffBiotechnologyWeight gaining
The invention provides a feed with a function of protecting intestinal barriers of piglets. The feed is comprised of the following raw materials: puffed corn, glucose, whey powder, wheat bran, puffedsoybeans, fermented soybean meal, soy protein isolate, 10-20 g / kg calcium hydrogen phosphate, calcium carbonate, sodium chloride, sodium butyrate, ethoxyquin, L-lysine hydrochloride, DL-methionine, threonine, glycine, L-cysteine, L-glutamine, L-arginine, tributyrin, vitamin A, choline chloride, 1% of a composite feed additive and the like. Experiment results show that the feed provided by the invention has the functions of obviously improving the feed intake and average daily weight gain of piglets, reducing feed conversion ratio and disease incidence and protecting intestinal barriers.
Owner:天津市农业科学院
Feed additive for preventing and treating hemorrhagic dysentery of pig as well as preparation method and application thereof
PendingCN109198187AHigh antibacterial activityGood effectAntibacterial agentsHydroxy compound active ingredientsEugenolSolvent
The invention discloses a feed additive for preventing and treating the hemorrhagic dysentery of a pig as well as a preparation method and application thereof. The additive provided by the invention is prepared from thymol, carvacrol, cinnamaldehyde, eugenol, mannan oligosaccharide, tributyrin, a latent solvent and a carrier. The thymol, the carvacrol, the cinnamaldehyde, the eugenol, the latent solvent and the carrier in the additive feed are added with water in a mixing tank and are uniformly mixed; next, a prepared intermediate material is subjected to homogenization through a high-pressurehomogenizer and spray draying; the intermediate material is next added into a mixing machine together with mannan oligosaccharide and tributyrin; and the feed additive for preventing and treating thehemorrhagic dysentery of the pig is prepared after uniform mixing. By using the feed additive provided by the invention, the hemorrhagic dysentery of the pig can be obviously prevented, treated and cured; moreover, the growth performance of the pig can be also improved; and the feed additive has no residue and a withdrawal period, and is green and safe.
Owner:山川生物科技(武汉)有限公司
Formula and production process of compound feed
InactiveCN111000035AGrowth inhibitionOvercoming the characteristics of high temperature pelleting of intolerant feedFood processingAnimal feeding stuffBiotechnologySucrose
The invention provides a formula and a production process of a compound feed, wherein the components of the formula comprise the following components in parts by weight: 20-40 parts of corn, 10-15 parts of puffed corn, 10-15 parts of whey powder, 6-10 parts of puffed beans, 7-15 parts of bean meal, 1-4 parts of fermented bean meal, 2-5 parts of skim milk powder, 3-5 parts of whole milk powder, 1-3parts of sucrose, 1-3 parts of fish meal, 0.5-1.5 parts of bean oil, 0.05-0.1 part of tributyrin, 0.5-1.0 part of an organic mineral substance premixing agent, 0.02-0.05 part of a vitamin premix, 0.05-0.2 part of a compound enzyme preparation, 0.3-0.8 part of stone powder, 0.6-1.5 parts of calcium hydrogen phosphate, 0.1-0.4 part of edible salt, 0.04-1.2 parts of lysine, 0.01-0.3 part of methionine, 0.01-0.3 part of threonine, 0.01-0.3 part of tryptophan, 0.01-0.3 part of phytase, 0.03-0.08 part of a mildew-proof agent, 0.1-0.5 part of chitosan oligosaccharide and 1-3 parts of plant essentialoil. According to the invention, the compound feed does not use any antibiotics, does not have the problem of antibiotic residues, is environmentally friendly, improves the intestinal tract resistance of piglets, is balanced in nutrition, can generate good economic effect, and is beneficial to popularization.
Owner:辽宁大成农牧实业有限公司
Green synthesis method for tributyrin for high-content feed
InactiveCN105801413AEasy to storePromote decompositionOrganic compound preparationCarboxylic acid esters preparationSynthesis methodsDistillation
The invention belongs to the technical field of fine chemical synthesis, and particularly relates to a green synthesis method for tributyrin for a high-content feed. According to the method, a super strong acid catalyst is utilized; with nitrogen as a protecting agent and water-carrying agent, the tributyrin is obtained through rectification and reduced pressure distillation; the purity reaches 95% or over; the moisture content is smaller than 100ppm; the super strong acid catalyst can be simply filtered and separated from a product, and does not need alkali washing, washing and drying processes; no wastewater and waste solid are generated; the catalyst can be repeatedly used; the water solution of which the butyric acid content is smaller than or equal to 20% obtained by distillation in the reaction process can be applied to synthesis of a feed additive sodium butyrate; and no less than 80% of butyric acid can be recycled by reduced pressure distillation to return to first-step synthesis.
Owner:上海旭牧联生物科技有限公司
Composite additive for preventing prawn intestinal injury under condition of low-fish-meal and high-soybean-meal feed and preparation method of composite additive
InactiveCN105433042AImprove growth performanceImprove utilization efficiencyFood processingClimate change adaptationDipeptideGut flora
The invention discloses a composite additive for preventing prawn intestinal injury under the condition of low-fish-meal and high-soybean-meal feed and a preparation method of the composite additive and belongs to the technical field of aquatic feed additives. The composite additive comprises components in parts by mass as follows: 25-30 parts of fructooligosaccharide, 5-10 parts of tributyrin, 15-25 parts of glutamine dipeptide, 10-20 parts of white carbon black and 15-45 parts of defatted rice bran. The invention further discloses the preparation method of the composite additive for preventing the prawn intestinal injury under the condition of the low-fish-meal and high-soybean-meal feed. The composite additive can control breeding of pathogenic bacteria of prawn intestinal tracts under the condition of the low-fish-meal and high-soybean-meal feed, adjusts balance of intestinal flora, repair intestinal mucosa and maintain health of the intestinal mucosa. Besides, the activity of digestive enzyme of the intestinal tracts can be improved, the immune function is activated, and the prawn growth performance and the feed utilization efficiency are improved.
Owner:JIMEI UNIV
Oplegnathus punctatus multi-functional composite feed and preparation method thereof
InactiveCN110754587AGrow fastImprove feeding capacityClimate change adaptationAnimal feeding stuffCelluloseVitamin C
The invention provides an oplegnathus punctatus multi-functional composite feed and a preparation method thereof. The multi-functional composite feed comprises 25-30 parts of fish meal, 10-15 parts ofbroad bean powder, 10-20 parts of dextrin, 10-15 parts of cellulose, 2-3 parts of fish oil, 0.5-1 part of soybean lecithin, 1-2 parts of a mineral mixture, 0.3-0.5 part of a vitamin mixture, 0.1-0.2part of choline chloride, 0.1-0.5 part of calcium dihydrogen phosphate, 0.01-0.05 part of a tributyrin mixture and 0.01-0.03 part of a compound enzyme preparation, wherein the tributyrin mixture comprises 1-2 parts of butyrin, 1-3 parts of dibutyrin, 3-5 parts of tributyrin, 1-2 parts of vitamin C-phosphate ester and 1-3 parts of mannan oligosaccharides. The multi-functional feed can strengthen the immunomodulation of intestines of fish, can increase the growth speed, and can improve the growing performance, so that the fish muscle is tight in grains, and the fish is elastic and good in chewiness.
Owner:HAINAN CHENHAI AQUATIC CO LTD
Micropterus salmoides low-fish-meal-content compound feed capable of improving intestinal health and preparation method thereof
The invention discloses a micropterus salmoides low-fish-meal-content compound feed capable of improving the intestinal health The micropterus salmoides low-fish-meal-content compound feed is formed by the following components in percentage by weight: 12-15% of fish meal, 5-12% of soybean protein concentrate, 10-20% of fermented soybean meal, 8-10% of enzymolysis soybean meal, 5-10% of chicken meal, 5-7% of corn protein powder, 5-8% of meat and bone meal, 8-12.38% of high gluten flour, 1-5% of fish oil, 3-7% of soybean oil, 0.2-1.0% of soybean lecithin, 0.2-1.0% of choline chloride, 0.5-1.0% of vitamin premix, 0.5-1.0% of mineral premix, 0.5 to 1.0 percent of calcium dihydrogen phosphate, 0.1 to 0.5 percent of L-lysine, 0.1 to 0.5 percent of L-methionine, 0.2 to 0.5 percent of taurine, 0.25 to 1.0 percent of tributyrin and 0.02 to 0.5 percent of alpha-ketoglutarate. The invention further provides a preparation method of the micropterus salmoides low-fish-meal-content compound feed. According to the invention, 70% of fish meal in an existing micropterus salmoides feed formula can be effectively replaced; the feed cost is remarkably reduced; and the growth performance of micropterus salmoides is fully guaranteed due to the fact that the intestinal health degree and the immune barrier function of micropterus salmoides are improved.
Owner:珠海海壹水产饲料有限公司 +1
Inclusion complexes and methods for making the same
ActiveUS20190099501A1Hydroxy compound active ingredientsPharmaceutical non-active ingredientsOral medicationGlyceryl tributyrate
Owner:THE BOARD OF TRUSTEES OF THE UNIV OF ILLINOIS
Heat stress resistant yellow feather broiler feed
ActiveCN104757294AAnti-heat stress helpsAnti-heat stress reliefFood processingAnimal feeding stuffBetaineTributyrin
The invention discloses a heat stress resistant yellow feather broiler feed, and belongs to the technical filed of poultry feeds. The feed contains plant extract products (comprising a perilla seed extract product and a Gleditsia sinensis extract product which are based on saponin), contains tributyrin mainly used for maintaining the broiler intestinal tract health closely related with the feed intake and the growth performances, and also contains natural anhydrous betaine used for alleviating the heat stress of broilers. A lot of researches prove that betaine can alleviate the heat stress of the broilers, synthetic betaine contains a large content of trimethylamine and chloride ions, and has negative influences on animals, and natural betaine is an effective component extracted from beet, and contains no trimethylamine or water to prevent caking. The broilers fed with the broiler feed under summer heat stress conditions are in good healthy state, and have high feed intake and excellent growth performances.
Owner:WENS FOOD GRP CO LTD
Antibiotic-free child-care concentrated feed
PendingCN111449174APromote growthImprove developmentFood processingAnimal feeding stuffBiotechnologyWeight gaining
The invention discloses an antibiotic-free child-care concentrated feed favorable for improvement of diarrhoea of child-care piggies. The antibiotic-free child-care concentrated feed comprises the rawmaterials of permeate high protein powder, soybean oil, puffed dehulled soybean meal, puffed soybeans, super steam fish meal, stone powder, calcium hydrogen phosphate, sodium chloride, a vitamin premix for piggies, a trace lemenent premix for piggies, choline chloride, arginine, lysine, methionine, antibacterial peptide, lysozyme, an acidulant, tannin, plant soot, tributyrin, coated sodium butyrate, prebiotics, probiotics, acidic protease, mannase, phytase, a mildewproof agent, an antioxidant and flour. The antibiotic-free child-care concentrated feed solves the problems that the child-care piggies are insufficient in immune function, weak in disease resistance, insufficient in secreted digestive enzymes, imperfect in development of digestive tracts, poor in absorptive capacity, easy to cause diarrhoea, slow in growth and the like, and protein raw materials which can cause risks for virus diseases of piggies and are biologically homologous with the piggies, are not used, so that the daily weight gain of the piggies can be increased, and the diarrhoea rate can be reduced.
Owner:FUZHOU ZHENGYANG FEED
Preparation method for low-calorie structure lipid containing conjugated linoleic acid and application
The invention relates to a preparation method for low-calorie structure lipid containing conjugated linoleic acid and application; the preparation method comprises the following steps: mixing tributyrin with conjugated linoleic acid or ethyl ester thereof to obtain the first mixture; performing contact between the first mixture and the lipase, at certain reaction temperature, vacuum degree and blending condition, performing the reaction for a period of time, and taking the percent conversion of the tributyrin as the index to obtain the second mixture; removing lipase in the reactant, distilling and recovering conjugated linoleic acid or ethyl ester thereof in the second mixture and obtaining the structure lipid containing conjugated linoleic acid. The product prepared by the preparation method is the structure lipid having low-calorie and related function of conjugated linoleic acid.
Owner:JIANGNAN UNIV
Efficient liver and intestinal tract repair agent, and bait
InactiveCN108635369ARestoratives restore functionImprove actual functionsHydroxy compound active ingredientsInorganic active ingredientsAnti stressBetaine
The invention discloses an efficient liver and intestinal tract repair agent. The efficient liver and intestinal tract repair agent is characterized by being prepared from the following raw materialsin parts by weight: 40 to 50 parts of betaine and derivatives thereof, 5 to 8 parts of tributyrin, 8 to 10 parts of vitamins and electrolytes, 20 to 30 parts of starch, and 8 to 10 parts of silica. The invention further discloses bait. The bait is prepared from the following raw materials in parts by weight: 0.2 to 0.5 parts of the repair agent, 20 to 30 parts of silkworm pupa meal, 0.5 to 0.8 parts of eggshell powder, 10 to 15 parts of soybean cake, 3 to 8 parts of bran powder, 2 to 5 parts of distillers grains, 0.5 to 0.9 parts of soybean oil, 5 to 8 parts of spirulina powder, and 9 to 15 parts of alginic acid. The repair agent disclosed by the invention has the advantages that the liver function is restored, liver and intestinal cells are repaird, detoxification and elimination of toxicants are realized, steatolysis is realized, the production speed of various enzymes in the liver is accelerated, and beneficial intestinal flora are reconstructed; the repair agent has significant effects of rapidly recovering intestinal tract and liver functions and improving anti-stress ability.
Owner:山东祥维斯生物科技股份有限公司
Pet beverage containing functional fatty acids and preparation method of pet beverage
InactiveCN111990545AMaintain healthLower cholesterol levelsFood processingAnimal feeding stuffBiotechnologyNutrition
The invention discloses a pet beverage containing functional fatty acids and a preparation method of the pet beverage. Each 500ml of the pet beverage containing functional fatty acids comprises the following raw materials components of 1-10g of medium chain triglyceride, 1-10g of concentrated linolein, 0.1-1g of glycerol monolaurate, 0.2-2g of tributyrin, 0.1-1g of a composite emulsifying agent, 2-20g of a carrier and 0.005-0.05g of a composite antioxidant. The pet beverage containing functional fatty acids is used for balanced supplementing of fatty acids in bodies of pets, can effectively reduce cholesterol level in the bodies of the pets, and solves the problems that a conventional pet beverage is single in functions and poor in balance of nutrients. The preparation method of the pet beverage containing functional fatty acids adopts a microcapsule packing technique, so that the functional fatty acids are coated with the carrier, the stability and the solubility of the functional fatty acids in the pet beverage can be greatly improved, and efficient absorption of nutrient substances in the pet beverage by pets can be facilitated.
Owner:佛山泰立美生物科技有限公司 +1
Inclusion complexes and methods for making the same
ActiveUS10098964B2Hydroxy compound active ingredientsPharmaceutical non-active ingredientsOral medicationΓ cyclodextrin
The invention provides novel formulations comprising a stable inclusion complex of tributyrin and a cyclodextrin. In one particular embodiment, the formulation comprises an oven dried inclusion complex of tributyrin and γ-cyclodextrin that is effective in minimizing or preventing the unpleasant taste and odor of tributyrin, thus making it suitable for oral administration and delivery to the digestive tract and intestines. The invention provides compositions of these inclusion complexes and methods of using them that are advantageous as food, medicinal and other products, where the negative sensory properties of tributyrin can be a liability.
Owner:THE BOARD OF TRUSTEES OF THE UNIV OF ILLINOIS
Method for preparing tributyrin
InactiveCN107673970AHigh selectivityShort reaction timeOrganic compound preparationCarboxylic acid esters preparationReaction temperatureGlycerol
The invention discloses a preparation method of tributyrin. The method comprises the following steps: adding tributyric acid and glycerin according to a mol ratio being 3:(0.8-1) in order, stirring the materials, gradually increasing the reaction temperature to 100-110 DEG C, adding an acidic ion-type liquid catalyst accounting for 1-5% of total mass of tributyric acid and glycerin, and reacting the materials for 2-8 h to obtain the tributyrin product with a conversion rate being 70-90%. Compared with the traditional catalyst, the catalyst prepared by tributyric acid and glycerin has higher selectivity, the esterified tributyrin is easily separated from a reaction system, the separated ionic liquid can be continuously used, and the catalytic activity can be kept better. The preparation method has the advantages of simple process, low production cost, and convenient operation, can rapidly prepare the tributyrin product, and is suitable for industrial large-scale production.
Owner:LUTIAN CHEM CORP
Method for preparing tributyrin by utilizing PVC (Polyvinyl Chloride) reisn-supported heteropolyacid catalyst
InactiveCN106946699AEmission reductionHigh catalytic activityOrganic compound preparationCarboxylic acid esters separation/purificationActivated carbonHeteropoly acid
The invention discloses a method for preparing tributyrin by utilizing a PVC (Polyvinyl Chloride) reisn-supported heteropolyacid catalyst. The method comprises the following steps of (a) pre-mixing glycerinum, butyric acid and a water-carrying agent, preheating, then feeding in a reaction column filled with the catalyst for carrying out esterification reaction, wherein the esterification reaction temperature is controlled to be 120 to 160 DEG C, the reaction time is 18 to 25h, the catalyst is the macroporous PVC reisn-supported heteropolyacid catalyst, and heteropoly acid is at least one of phosphotungstic acid and silicotungstic acid; (b) after finishing esterification reaction, utilizing vacuum distillation for removing the butyric acid, and then adopting organic alkali as an acid-binding agent for absorbing residual butyric acid; (c) then adopting activated carbon for decoloring and deodorizing, and refining to obtain a tributyrin finished product. Through the manner, the method provided by the invention is not only high in catalytic activity, good in selectivity and good in recycling, but also environmental-friendly, the production efficiency is greatly improved, and the discharge of the three wastes is reduced.
Owner:JIANGSU RUICHEN CHEM
Feed additive, preparation method, and application of feed additive in resisting piglet diarrhea
InactiveCN111631315AReduce dosageReduce decompositionInorganic active ingredientsDigestive systemBiotechnologyGlycerol
The invention discloses a feed additive, a preparation method thereof and an application of the feed additive in resisting piglet diarrhea. The preparation method comprises the following steps: (1) adding glycerol monolaurate and tributyrin into a container, and performing heating until the glycerol monolaurate and tributyrin are molten; (2) adding zinc oxide and performing uniform stirring; and (3) adding silicon dioxide and performing uniform stirring. By compounding glycerol monolaurate, tributyrin and zinc oxide, a good anti-diarrhea effect can still be achieved when the usage amount is reduced by one order of magnitude compared with that of single use of glycerol monolaurate, tributyrin or zinc oxide,, and the feed additive has the advantages of low dosage and high efficiency.
Owner:无锡利必多生物科技有限公司
Oleogel composition containing tributyrin and phospholipid
Owner:JIANGNAN UNIV
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