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33results about How to "Rapid flowback" patented technology

High temperature resistant Gemini cationic viscoelastic surfactant (VES) and synthetic method thereof

The invention provides a high temperature resistant Gemini cationic viscoelastic surfactant (VES) and a synthetic method thereof, relating to the field of oil recovery technology and engineering in the petroleum industry. The synthetic method is characterized by reacting unsaturated long-chain fatty acid with N,N-dimethyl propanediamine to synthesize a fatty acid amide intermediate; reacting methylamine with epichlorohydrin to synthesize a chloramine intermediate; reacting the intermediates synthesized in the two above steps respectively to synthesize the high temperature resistant Gemini cationic VES. The VES and the synthetic method have the beneficial effects that a high temperature surface active diverting acid system reacts with rocks at 160 DEG C, so that the liquid obviously diverts to become viscous and is subjected to automatic gel breaking under the condition that the hydrochloric acid concentration is below 5%, thus achieving rapid flowback; the VES has good temperature resistance, is relatively low in price and is beneficial for popularization and application.
Owner:CHINA PETROLEUM & CHEM CORP +1

Method of fracturing coal-bed gas reservoir

The invention discloses a method of fracturing a coal-bed gas reservoir and belongs to the field of coal-bed gas exploitation. The method comprises following steps: after perforation in a middle-upper part of the coal bed and a coal bed top board above the coal bed, active water fracturing fluid is pumped and injected in the coal bed top board to form a first crack; low sand ratio sand-carrying fluid and high sand ratio sand-carrying fluid are successively pumped and injected into the first crack, and a second crack communicated with the first crack is formed in the coal bed, and the extension of the second crack is promoted to form multiple branchlike cracks containing sand support agent. The low sand ratio sand-carrying fluid comprises following components by percentage of mass: 0.1-0.3% carboxymethyl hydroxypropyl guanidine gum, 1-2% KCl, 0.5-1% discharge aiding agent, 8-12% sand support agent, and water as balance; the high sand ratio sand-carrying fluid comprises following components by percentage of mass: 0.1-0.3% carboxymethyl hydroxypropyl guanidine gum, 1-2% KCl, 0.5-1% discharge aiding agent, 12-48% sand support agent, and water as balance. The method provided by the invention can form a long distance supporting seam network in the coal-bed gas reservoir, and effectively improve the yield of the coal-bed gas reservoir.
Owner:PETROCHINA CO LTD

Method for detonation fracture acidizing combined operation

ActiveCN106246156AEnhancing the effectiveness of deflagration fracturingGuaranteed work effectFluid removalDrilling compositionWell killDetonation
The invention discloses a method for detonation fracture acidizing combined operation. The method comprises the steps of optimizing detonation fracture acidizing combined operation process parameters, performing operation preparation before detonation fracture and filling a pitshaft with liquid, testing stratum absorption amount before the detonation fracture, placing a detonation fracture operation tubular column to a predetermined operation depth, performing pressurization detonation of the tubular column, performing well killing operation, detonating the fracture operation tubular column, testing the stratum absorption amount after the detonation fracture, placing an acidizing operation tubular column, performing pumping injection acid liquid slug, lifting the acidizing operation tubular column, placing an electric pump production tubular column and performing electric pump liquid drainage and well opening alkalifying neutralization, placing an electric pump production Y tubular column without a Y tubular column, performing pumping injection of acid liquid slug, placing the Y tubular column, performing electric pump liquid drainage and well opening alkalifying neutralization and the like. The method has the advantages that detonation fracture and acidizing effects can be further enhanced, the acid liquid injection capability is enhanced, the acidizing radius is expanded, crack closure is further avoided, and a physical effect is enhanced; a detonation fracture effect can be enhanced, a follow-up acidizing step is selected flexibly, and the operation step is omitted while an operation effect can be guaranteed.
Owner:CHINA NAT OFFSHORE OIL CORP +1

Coiled tubing and packer combined staged fracturing string and method for slim hole well

ActiveCN112211601AAvoid the risk of inaccurate pre-perforated sectionsLong extension distanceFluid removalSealing/packingSand blastingCoiled tubing
The invention provides a coiled tubing and packer combined staged fracturing string and method for a slim hole well. The string comprises a casing pipe, a coiled tubing, a connector, a hydraulic safety release, a hydraulic sandblaster, an upper packer, a sliding sleeve base, a reducing release tie-back barrel, a lower packer, an oil pipe, a plurality of bottom packers, a float collar, a guide screen pipe and an open hole section, the coiled tubing is located in the casing pipe, and the lower end of the coiled tubing is connected with the hydraulic safety release through the connector. The string is lowered to a preset position of a target reservoir, steel balls of the specified specification are pumped to set the packer, the fracturing string is released, packing of an original reservoir and a new reservoir transformation section is achieved, then segment-by-segment transformation is conducted through the fracturing string, after transformation is completed, the fracturing string is pulled out, and a production string is lowered; and after the reservoir is transformed, a wellbore has a full bore, the later wellbore maintenance and treatment difficulty and operation risk are reduced, and later secondary transformation is facilitated.
Owner:PETROCHINA CO LTD

Filtrate loss reducer and application thereof to non-tackifying pure liquid-state CO2 sand fracturing

The invention discloses a filtrate loss reducer. The filtrate loss reducer is prepared from the following raw materials in parts by weight: 10-25 parts of 5# white oil, 0.5-2 parts of NP-1, 0.1-1 part of TX-4, 1-10 parts of n-caprylic acid, 1-10 parts of KCl, 4-15 parts of a carboxymethyl guanidine gum solution with the concentration of 1%. According to the filtrate loss reducer, the sand carrying capability of pure liquid-state CO2 fracturing liquid can be improved and the loss of the fracturing liquid is effectively reduced. Meanwhile, the invention further provides application of the filtrate loss reducer to a pure liquid-state CO2 sand fracturing process; the filtrate loss reducer is pumped into a stratum before pure liquid-state CO2 fracturing is constructed, and the sand fracturing is carried out; the filtrate loss reducer has the advantages of rapid backflow, increased backflow rate, shortened period of putting into production and the like; and water-based fracturing liquid does not need to be prepared in the process and backflow liquid does not need to be treated, so that the environment pollution degree is reduced, and the filtrate loss reducer has relatively good practical significance on regions with lacked water resources and regions with fragile ecological environments.
Owner:RES INST OF SHAANXI YANCHANG PETROLEUM GRP

Multi-hydrogen acid system suitable for reservoir plugging-removing acidification and preparing method thereof

InactiveCN109777389AHigh activityStrong smooth performanceDrilling compositionPhosphoric acidPotassium
The invention belongs to a multi-hydrogen acid system suitable for reservoir plugging-removing acidification and a preparing method thereof. The multi-hydrogen acid system is prepared from, by weight,30-60 parts of hydrochloric acid, 7-12 parts of multi-hydrogen acid, 3-6 parts of a multipurpose additive, 2-4 parts of a shrinking agent, 1-3 parts of an activating agent, 3-8 parts of an initiatingagent, 2-4 parts of a corrosion inhibitor and 3-52 parts of water; the hydrochloric acid is selected from industrial hydrochloric acid with the HCL content of 28% to 31%; the multi-hydrogen acid is selected from one of citric acid, phosphoric acid, oxalic acid and sulfuric acid or a mixture of citric acid, phosphoric acid, oxalic acid and sulfuric acid; the multipurpose additive is a mixture of afluorocarbon surfactant, potassium amine triacetate, potassium chloride and water; the activating agent is selected from one of a demulsifying agent AE1910, a demulsifying agent 1031 and polyethenoxyether or a mixture of a demulsifying agent AE1910, a demulsifying agent 1031 and polyethenoxy ether; the initiating agent is peracetic acid. The multi-hydrogen acid system has the advantages that theacid liquor activity, H+ mild releasing and the buffering effect are achieved, and the multi-hydrogen acid system is suitable for reservoir plugging-removing acidification.
Owner:北京国海能源技术研究院

A high-efficiency self-produced gas foam fracturing fluid and its construction method

The present invention provides a high-efficiency self-generated gas foam fracturing fluid and a construction method. The foam fracturing fluid is composed of a base fluid, a gas-generating fluid and a heat-generating agent, wherein the mass ratio of the base fluid, gas-generating fluid, and heat-generating agent is 100: (30‑42): (5‑9). During construction, the base fluid and the gas-producing fluid are pumped downhole together through the suction of the sand mixing truck according to the mass ratio, and the heat generating agent is pumped into the downhole along with the proppant. The invention does not need liquid nitrogen accompanying injection, simplifies the on-site process and reduces the construction cost, and a large amount of gas generated through the chemical reaction achieves the purpose of increasing the energy of the formation, improving the flow capacity of the reservoir liquid, and increasing the output. It can quickly generate a large amount of inert and safe gas, and will not produce toxic gas of nitrogen oxides, reducing construction risks. At the same time, the alkaline environment generated by the reaction product is conducive to the formation of fracturing fluid gel and the corrosion protection of downhole pipe strings. By generating foam, the Jiamin effect is used to increase the net pressure of the formation, which can quickly flow back, generate heat in the deep formation to promote gel breaking, and reduce the damage of fracturing fluid to the reservoir.
Owner:PETROCHINA CO LTD

A kind of fluid loss reducer and its non-viscosifying pure liquid co 2 Application in sand fracturing

The invention discloses a filtrate loss reducer. The filtrate loss reducer is prepared from the following raw materials in parts by weight: 10-25 parts of 5# white oil, 0.5-2 parts of NP-1, 0.1-1 part of TX-4, 1-10 parts of n-caprylic acid, 1-10 parts of KCl, 4-15 parts of a carboxymethyl guanidine gum solution with the concentration of 1%. According to the filtrate loss reducer, the sand carrying capability of pure liquid-state CO2 fracturing liquid can be improved and the loss of the fracturing liquid is effectively reduced. Meanwhile, the invention further provides application of the filtrate loss reducer to a pure liquid-state CO2 sand fracturing process; the filtrate loss reducer is pumped into a stratum before pure liquid-state CO2 fracturing is constructed, and the sand fracturing is carried out; the filtrate loss reducer has the advantages of rapid backflow, increased backflow rate, shortened period of putting into production and the like; and water-based fracturing liquid does not need to be prepared in the process and backflow liquid does not need to be treated, so that the environment pollution degree is reduced, and the filtrate loss reducer has relatively good practical significance on regions with lacked water resources and regions with fragile ecological environments.
Owner:RES INST OF SHAANXI YANCHANG PETROLEUM GRP

A kind of fracturing method of coalbed methane reservoir

The invention discloses a method of fracturing a coal-bed gas reservoir and belongs to the field of coal-bed gas exploitation. The method comprises following steps: after perforation in a middle-upper part of the coal bed and a coal bed top board above the coal bed, active water fracturing fluid is pumped and injected in the coal bed top board to form a first crack; low sand ratio sand-carrying fluid and high sand ratio sand-carrying fluid are successively pumped and injected into the first crack, and a second crack communicated with the first crack is formed in the coal bed, and the extension of the second crack is promoted to form multiple branchlike cracks containing sand support agent. The low sand ratio sand-carrying fluid comprises following components by percentage of mass: 0.1-0.3% carboxymethyl hydroxypropyl guanidine gum, 1-2% KCl, 0.5-1% discharge aiding agent, 8-12% sand support agent, and water as balance; the high sand ratio sand-carrying fluid comprises following components by percentage of mass: 0.1-0.3% carboxymethyl hydroxypropyl guanidine gum, 1-2% KCl, 0.5-1% discharge aiding agent, 12-48% sand support agent, and water as balance. The method provided by the invention can form a long distance supporting seam network in the coal-bed gas reservoir, and effectively improve the yield of the coal-bed gas reservoir.
Owner:PETROCHINA CO LTD

Polymer perforating fluid and preparation method thereof

The invention discloses a polymer perforating fluid and a preparation method thereof. The polymer perforating fluid comprises, by mass, 0.25 to 0.45% of a polymer densifier, 12 to 26% of a weighting agent, 0.02 to 0.08% of a cleanup additive, 0.015 to 0.03% of a gel breaker and 0.55 to 2.5% of a temporary plugging agent, with the balance being water. The polymer perforating fluid provided by the invention has a density adjustable in a range of 1.10 to 1.25 g / cm<3> and has a viscosity of 50 mPa.s or above after shearing for 60 min under the conditions of a temperature of 50 to 100 DEG C and a rotating speed of 1000 / s; a gel-broken fluid has a viscosity of no more than 2 mPa.s and low interfacial tension and can rapidly flow back after construction; and the polymer perforating fluid is especially applicable to high-porosity high-permeability alkali-sensitive strata with abnormally high pressure and has the characteristics of adjustable density, leak-proof and leak-stopping performance, resistance to temperature and shearing, low fluid loss, low corrosion rate, low damage to rock cores, thorough gel breaking and easiness in flowback.
Owner:CHINA PETROLEUM & CHEM CORP +1
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