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36results about How to "Improve electrode activity" patented technology

Method and device for treating oily sludge

InactiveCN102001806AImprove qualityQuickly break down complex structuresSludge treatment by oxidationElectrochemical responseMicro bubble
The invention relates to a method and a device for treating oily sludge. Under the action of an applied electric field and by adopting an electrochemical oxidation method, the oil-in-water and water-in-oil structure of emulsified oil is quickly broken, and the oily sludge serving as an electrolyte releases oil drops; oil is quickly taken by a large number of micro bubbles to the liquid level to be recycled under the action of applied air flotation; oily sludge flocs are subjected to electrochemical reaction on the surface to produce various active free radicals which have high activity and oxidability and mainly comprise hydroxyl, and organic pollutants are degraded to be converted into water and carbon dioxide; the active free radicals can destroy a microbial cell structure and kill sulfate reducing bacteria and saprophytic bacteria through a series of oxidation chain reactions; the sludge is powerfully dehydrated, so that the water quality of dehydrated water meets the water quality standard of oil field reinjection, and the sludge can be recycled; and a mud cake is nontoxic and harmless and can be used for soil improvement, fertilizers, building materials and the like.
Owner:朱同德 +1

Electrode for generation of hydrogen

The present invention provides an electrode for generation of hydrogen comprising: a conductive substrate; a catalytic layer formed on the conductive substrate and containing at least one platinum group metal selected from the group consisting of Pt, Ir, Ru, Pd and Rh; and a hydrogen adsorption layer formed on the catalytic layer. The present invention also provides an electrode for generation of hydrogen comprising: a conductive substrate, a catalytic layer formed on the conductive substrate and containing: at least one platinum group metal selected from the group consisting of Pt, Ir, Ru, Pd and Rh and / or at least one oxide of said platinum group metals; and at least one metal selected from the group consisting of lanthanum series metals, valve metals, iron series metals and silver and / or at least one oxide of said metals; and a hydrogen adsorption layer formed on the catalytic layer.
Owner:DE NORA PERMELEC LTD

Fuel cell using conductive polymer modified carbon based cobaltous hydroxide composite catalyst

The invention relates to the fuel cell field, aims to provide a direct liquid fuel cell using conductive polymer modified carbon based cobaltous hydroxide composite catalyst. The cell comprises a negative pole using foam nickel as matrix and a positive pole using hydrophobic processed carbon paper or carbon cloth as matrix; The negative pole is made by mixing the conductive polymer modified carbon based cobaltous hydroxide composite catalyst, water, perfluoro sulfonic group resin solution with concentration of 5wt% and anhydrous ethanol, blending into slurry, coating on foam nickel and drying in air naturally. The beneficial effects of the invention is: conductive polymer can increase electrode electrical conductivity, reduce electrode impedance, improve electrode activity, and improve the electricity generation performance of cell; the synthesized conductive polymer modified carbon based cobaltous hydroxide composite catalyst is non-Pt catalyst, has a low cost, is favorable to the popularization of fuel cell technology.
Owner:ZHEJIANG UNIV

Method for treating poisonous and organic pollutant atrazine through modified electrode in electrocatalytic oxidation mode

The invention discloses a method for treating poisonous and organic pollutant atrazine through a modified electrode in an electrocatalytic oxidation mode and belongs to the field of electrode electrocatalytic application. A titanium dioxide nanotube array (TiO2-NTs) is prepared, and layers of Ni are electroplated at the bottom of a substrate Ti and the bottom of TiO2NT; titanium dioxide nanotubes are coated with an intermediate layer SnO2-RuO2-Ce, components of deposition liquid are 18g of SnC14.5H2O, 0.1g of RuCl3, 0.7g of Ce(NO3)3.6H2O and 0.1g of sodium dodecyl benzene sulfonate, 2ml of HCl(37%) is dissolved in 100ml of an ethanol solution, and current density is 20mA / cm<2>; electro-depositing is carried out for 30 minutes at normal temperature, then the nanotubes are put into a muffle furnace of 500 DEG C to be calcined for 60 minutes, so that the intermediate layer SnO2-RuO2-Ce is obtained, and the lead dioxide and rare earth Y2O3 modified titanium dioxide nanotube electrode is prepared; the poisonous and organic pollutant atrazine is treated in the electrcatalytic oxidation mode. The self-made Y2O3-PbO2 doped modified high-activity Y2O3-PbO2 / SnO2-RuO2-Ce / Ni-TiO2-NTs / Ti modified electrode is adopted as an anode, the electrode is not suitable for inactivation in the electrolytic process, corrosion resistance of the electrode is good, and selectivity is good during degrading.
Owner:HUAINAN NORMAL UNIV

Nickel-based composite anode material of solid oxide fuel cell and application thereof

InactiveCN102651477AImprove dispersionHigh particle size and activityCell electrodesComposite oxideNickel oxides
The invention relates to a nickel-based composite anode material of a solid oxide fuel cell and an application thereof. The composition of the composite anode material can be expressed by Ni1-x-yMgxAlyO1 plus 0.5y, wherein x varies from 0.01 to 0.2 and y ranges from 0.001 to 0.2. The composite anode material is compounded with an electrolyte material to prepare an anode, and the weight percentage of magnesium oxide and aluminium oxide modified nickel-based composite oxide material is 30-70 percent. During practical application, the composite anode is put into use after reduction, the reduced anode contains the electrolyte material, metal micron-nickel and nano particles, magnesium oxide, aluminium oxide and a composite oxide formed by magnesium oxide, aluminium oxide and nickel oxide. The novel composite anode can be used for flat-plate-type, tubular, honeycomb-type and oblate-tube-type solid oxide fuel cells.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Metal boride water-splitting catalyst, preparation method and application of catalyst in electro-catalytic water splitting

The invention discloses a metal boride water-splitting catalyst, a preparation method and an application of the catalyst in electro-catalytic water splitting and belongs to the technical field of preparation of an electrocatalyst. The metal boride water-splitting catalyst is prepared with a solid-phase boriding method, transition metal is coated with a solid boriding agent, and boriding treatmentis performed through temperature programming heating. The boriding agent is prepared from a necessary boriding medium and an unnecessary filling agent. Compared with liquid boriding, a solid boridingmethod has the advantages that the surface clearing difficulty is low after boriding, requirements for equipment are low, and the method is applicable to boriding treatment of various transition metals. The catalyst has very good intrinsic catalysis activity and stability performance under the alkaline condition, and the required potential is 300-400 mV when the current density is 10 mA cm<-2>; the electro-catalytic water splitting oxygen evolution stability can be as long as at least 100 h while the performance is not attenuated, and the catalyst can replace noble metals to promote commercialapplication of electro-catalytic water splitting.
Owner:JILIN UNIV

Method for conducting electrocatalytic oxidation treatment on phenol organic wastewater through novel anode

The invention relates to the technical field of electrocatalytic degradation application, in particular to a method for conducting electrocatalytic oxidation treatment on phenol organic wastewater through a novel anode. The method includes the following steps of S1, preparing a titanium dioxide nanotube array; S2, modifying NiO in nanotubes through a pulse depositing method and a high-temperaturecalcination method to prepare a Ti / TiO2NTs-NiO electrode high in conductivity; S3, using the Ti / TiO2NTs-NiO electrode as a working electrode, and preparing a high-performance Ti / TiO2NTs-NiO / PbO2 anodematerial through pulses; S4, conducting electrocatalytic oxidation treatment on the phenol organic wastewater through the prepared Ti / TiO2NTs-NiO / PbO2 anode material. The Ti / TiO2NTs-NiO / PbO2 modifying electrode is used as the anode, electrocatalytic oxidation treatment is conducted on the toxic phenol organic wastewater in an electrolytic cell, the degradation efficiency is higher than that of anordinary lead electrode, the degradation rate of COD of the phenol organic wastewater can reach 92.7%, the average current efficiency in the degradation process is remarkably improved compared with that of the ordinary lead electrode, the average current efficiency reaches 34%, electric energy loss is effectively reduced, and meanwhile degradation efficiency is improved.
Owner:HUAINAN NORMAL UNIV

Electrode processing method applied to direct synthesis of hydrogen peroxide through oxygen electroreduction

The invention relates to a material processing method, in particular to an electrode processing method applied to direct synthesis of hydrogen peroxide through oxygen electroreduction, and belongs to the field of hydrogen peroxide direct synthesis through electrochemistrical oxygen reduction. A processing method for etching a graphite felt electrode through ferrocene-glacial acetic acid solution steam is designed; the glacial acetic acid-ferrocene solution steam is injected under the high-temperature oxygen-free condition to etch the surface of the graphite felt electrode, the original smooth graphite felt microcosmic surface becomes rough and porous through the etching process, and the specific surface area can be simply and effectively increased; and meanwhile, surface changes cannot influence the graphite felt structure, and the mechanical property is kept well. In this way, the aims of improving the electrode activity and being free of influences on stability are achieved. The problem that an existing technology for direct synthesis of hydrogen peroxide through electro-catalysis oxygen reduction is low in electrode catalysis activity is solved.
Owner:SUN YAT SEN UNIV

Activation method of carbon fiber electrode material using polyacrylonitrile carbon fiber

The invention belongs to an activation method of a carbon fiber electrode material. The invention adopts polypropylene carbon fiber weaved cloth soaked with epoxy resin as a raw material, and comprises the following steps of injecting air in a short time at a low vacuum condition with a temperature 600-700 DEG C, then performing vacuumization and natural cooling; thereby the surface properties of the carbon fiber cloth are improved, and the electrode activity is increased by more than 3 times.
Owner:DALIAN XINGKE CARBON FIBER

Solid-oxide fuel battery anode catalysis material containing rare earth element

The present invention relates to a solid oxide fuel battery anode catalytic material, in particular to a lanthanon-containing solid oxide fuel battery anode catalytic material. The formula comprises NiOxReyOz; wherein, Ni stands for nickel, Re stands for lanthanide rare earth element and O stands for oxygen; y is more than 0 and less than 0.5, x is more than 0 and less than 2 and z is more than 0 and less than 1. The present invention is characterized in that the anode catalytic material is modified by adding lanthanide elements such as lanthanum, cerium, praseodymium, neodymium, samarium gadolinium, etc.; in the anode made from electrolyte, the material can prevent anode catalyst particle from growing, improve the interface contact between the anode catalytic material and the electrolyte, reduce the polarization resistance of the battery, improve the activity and the output performance of the battery.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Metal electrode activation method for oxygen-metal battery

The invention relates to a metal electrode activation method for an oxygen-metal battery. By forcedly oxidizing a substrate, the volume of the substrate is expanded, and the stress is increased to lead the substrate to peel off. According to the metal electrode activation method, oxygen content in an electrolyte is increased by increasing oxygen partial pressure on an electrolyte level, oxygenating microbubbles and through stirring and oxygenating modes; oxygen is diffused and penetrates through a compact oxygen membrane of a metal electrode under the driving of oxygen concentration and fluid pressure of the electrolyte, enters the oxygen membrane and is combined with metal to generate an oxide, the volume of the metal after combined with the oxygen through diffusion is expanded, the hard and brittle oxygen membrane is broken and peeled off due to stress, and the metal substrate is exposed, therefore, the purpose of metal electrode activation before battery discharging is achieved.
Owner:BEIHANG UNIV +1

A non-plated terminal electrode silver paste for inductors

The invention relates to the technical field of electronic materials used in electronic components, in particular to an inductive plating-free terminal electrode silver paste. by weight of spherical silver powder25 -35%, flake silver powder 15%- 25%, silver oxide powder 10%- 15%, glass powder and other inorganic materials 2%- 4%, organic carry 20%-25%, and that sum of the weight percentages of each substance is 100%. A silver paste for inductance non-plating terminal electrode produced by the silver paste of the invention has the advantages of high drying intensity, good appearance quality ofthe sealing terminal, compact electrode layer after firing, high terminal adhesion, no jump sheet meeting SMT packaging requirements, low resistivity, small DC resistance RDC, environmental protectionand non-plating..
Owner:肇庆市辰业电子有限公司

Magnesium-containing catalytic material for anode of solid oxide fuel cell, preparation and application thereof

The invention relates to a catalytic material for the anode of a solid oxide fuel cell, in particular to a magnesium-containing catalytic material for the anode of a solid oxide fuel cell, preparation and application thereof. The magnesium-containing catalytic material comprises the component of NiOxMgyOz, wherein Ni represents nickel, Mg represents magnesium, O represents oxygen, y is larger than 0 and smaller than 0.5, x is larger than 0 and smaller than 2, and z is larger than 0 and smaller than 0.5. Characterized by using the catalytic material for the anode, the invention can reduce the polarization resistance of the cell, increase the activity of the electrodes and improve the output performance of the cell.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Plating-free terminal electrode silver paste for inductor

The invention relates to the technical field of the electronic material for the electronic component, and especially relates to plating-free terminal electrode silver paste for an inductor. The plating-free terminal electrode silver paste is prepared from the following raw materials in weight percent: 25%-35% of spherical silver powder, 15%-25% of silver flake, 10%-15% of silver oxide powder, 2%-4% of glass powder and 2%-4% of other inorganic material, and 20%-25% of organic carrier, the sum of the weight percent of various substance is 100%. The plating-free terminal electrode silver paste for the inductor is large in drying strength, good in blocking appearance quality, and the sintered electrode layer is compact, the tip adhesive force is high, the SMT package requirement is satisfied,the plate skipping is avoided, the resistivity is low, the DC resistance RDC is small, the electrode silver paste is environment-friendly and plating-free, and the environment can be protected.
Owner:肇庆市辰业电子有限公司

Electrode binder solution composition for polymer electrolyte fuel cell

InactiveUS20090280379A1Increasing electrode active surface areaPrevent cohesionActive material electrodesSolid electrolyte fuel cellsSlurrySolvent
The present invention relates to an electrode binder solution composition for a polymer electrolyte fuel cell comprising a mixture of a solvent and a nonsolvent. The electrode binder solution composition can significantly improve electrode activity by maximizing formation of a three-phase interface of catalyst, binder and fuel at the electrode catalytic layer of the polymer electrolyte fuel cell. The present invention relates to a preparation method of an electrode binder solution for a polymer electrolyte fuel cell, the electrode binder solution for a polymer electrolyte fuel cell comprising a sulfonated proton exchange hydrocarbon-based polymer and a mixture of a solvent and a nonsolvent. The present invention also relates to a preparation method of an electrode catalyst slurry comprising the steps of: mixing an electrode binder solution composition for a polymer electrolyte fuel cell with a platinum catalyst and drying the mixture; and heat-treating the dried mixture to maximize interface between the electrode binder and the catalyst.
Owner:HYUNDAI MOTOR CO LTD +1

A kind of composite titanium dioxide mesoporous film electrode material and preparation method thereof

The invention discloses a composite titanium dioxide mesoporous thin-film electrode material and a preparation method thereof. The preparation method comprises: adding a titanium source and an antimony source compound to a hydrochloric acid solution, stirring and mixing to obtain a precursor solution after hydrothermal reaction, and spraying the solution Drying and calcining at high temperature to obtain mesoporous hollow spherical antimony-doped titanium dioxide composite material; placing in hydrochloric acid solution, ultrasonically dispersing, adding pyrrole monomer under stirring condition, stirring uniformly, adding oxidant dropwise, standing after completion of the reaction, filtering, drying to obtain polypyrrole@antimony / titanium dioxide composite material; uniformly mix the prepared polypyrrole@antimony / titanium dioxide composite material with polyvinylidene fluoride, add 1-methyl-2-pyridinone to prepare a slurry, It is uniformly coated on the conductive substrate, and calcined after drying to obtain the thin film electrode material. The composite thin film material prepared by the invention significantly improves the photoelectric performance of the titanium dioxide electrode material, and has a compact structure and stable performance.
Owner:FOSHAN UNIVERSITY

A titanium-based iridium oxide electrode, its electrochemical preparation method and application

The invention discloses a titanium-based iridium oxide electrode, the base of which is titanium metal, and the surface layer is an iridium oxide layer; the iridium oxide layer is formed by stacking micron sheets with a relatively uniform size of 0.5-1 μm, and its specific surface area is 200-1 μm. 300m 2 / g. The invention also discloses the preparation method and application of the titanium-based iridium oxide electrode.
Owner:TIANJIN UNIV

Liquid anode and method for enriching and separating anions in water body

The invention discloses a liquid anode which is composed of hydrophobic liquid, a hydrophilic immobilization film and a conductive electrode; a bag made of the hydrophilic immobilization film is filled with the hydrophobic liquid, and then the conductive electrode is placed in the bag, and therefore, the liquid anode can be prepared; the hydrophobic liquid is hydrophobic ionic liquid or hydrophobic conductive liquid. Compared with a traditional anode material, the liquid anode is simple in preparation method, large in electrode specific surface area and large in capacitance; physical adsorption, chemical adsorption and electric adsorption are organically coupled, so that the liquid anode is suitable for treating complex anions in water, and the problems of small current density, failure torealize efficient mass transfer, low electrolysis efficiency and large power consumption of a conventional electrode electrolyzing low-concentration wastewater can be solved.
Owner:KUNMING UNIV OF SCI & TECH

Multilayer film material

The invention discloses a multilayer film material. The preparation method comprises the steps: adding a titanium source compound and an antimony source compound into a hydrochloric acid solution; stirring and mixing, inserting conductive glass into the mixed solution, carrying out hydrothermal reaction, and calcining at high temperature to obtain an antimony-doped titanium dioxide nano-electrode;then putting the antimony-doped titanium dioxide nano-electrode into a phosphoric acid aqueous solution, and carrying out hydrothermal treatment to obtain an antimony-doped titanium dioxide nano-electrode; and carrying out electro-polymerization deposition by taking the antimony-doped titanium dioxide nano-electrode as a working electrode to obtain the polypyrrole / antimony-doped titanium dioxidemultilayer film electrode. According to the prepared polypyrrole / antimony-doped titanium dioxide multilayer film electrode, antimony ion doping is carried out, the activity of TiO2 under visible lightis improved, polypyrrole nanowires are deposited on the surface of a titanium dioxide film to form p-n heterojunctions, and directional movement of electrons and holes is induced, so that the recombination probability of electron-hole pairs is reduced, and the electrode activity of the material is further improved.
Owner:FOSHAN UNIVERSITY

Electrode treated by persulfate and application thereof

The invention discloses an electrode treated by persulfate and application of the electrode in a zinc-iron flow battery, an electrode material is soaked in an aqueous solution of persulfate for treatment, and compared with an original untreated electrode material, the electrode material has higher electrode activity, the conductivity of the battery can be effectively improved, and the cycle performance and the efficiency of the battery are improved; meanwhile, the charge-discharge capacity and the energy density of the battery are greatly improved.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Preparation method of high-performance electrode material for high concentration rate operation of circulating water

The invention relates to a preparation method of a high-performance electrode material for high concentration rate operation of circulating water. The method includes the following steps: dispersing and suspending graphite powder in deionized water; adding a multi-walled carbon nanotube; preparing a required solution; dropping a SnCl2 solution and a ReCl2 solution into the mixture; dropping a PtCl4 solution; adding a NaOH solution into the mixture until pH reaches 9; adding ammonia water into the mixture until the pH reaches 10, and cooling the mixture to room temperature for clarification; sucking a supernatant solution out, and cleaning a reaction product until the pH of an eluate is reduced to 7.5; adding deionized water into the reaction product and stirring the mixture; adding a prepared NaBH4 solution into the mixture and cooling the mixture to room temperature for clarification; pumping-filtering the mixture; placing a filter cake into a baking oven for drying; and obtaining thehigh-performance electrode material, and pressing the high-performance electrode material for forming. The high-performance electrode material can be used for treatment of circulating water and can ensure the low-cost high-concentration rate operation of a circulating water system.
Owner:HUADIAN ELECTRIC POWER SCI INST CO LTD

Preparation method of pt/ito electrode for high-efficiency electrocatalytic oxidation of ammonia

The invention discloses a preparation method for a Pt / ITO (Indium Tin Oxide) electrode of efficient electro-catalysis ammonia oxidate. The method comprises the following steps: step 1, preparing a working electrode: (a), cleaning ITO, (b), connecting a conducting wire with the conductive surface of the ITO cleaned in step (a) and packaging to obtain the working electrode; steps 2, connecting a Pt counter electrode, a saturated calomel reference electrode, the working electrode and electrolyte to form a loop so as to constitute a three-electrode system, wherein the electrolyte is a mixture of H2PtCl6 solution and HCl solution; and step 3, connecting the three-electrode system into an electrochemical workstation for electrodeposition. According to the invention, after chloride ions are injected into electroplating solution, the diameters of Pt prills obtained through electrodeposition can be reduced effectively, so that nanosheet-shaped particles can be obtained, and meanwhile, the dispersivity of the prills on the surface of ITO, the catalysis efficiency of Pt and the utilization ratio of Pt can be improved. The preparation method has the advantages of simple procedure, easiness in operation, low cost, environmental friendliness and obvious effect and has better properties when being compared with the current commercial catalysis electrode.
Owner:SHANGHAI JIAO TONG UNIV

Double-layer composite structure ceramic, preparation method of the ceramic, self-adsorption lithium-air battery and preparation method of the battery

A double-layer composite structure ceramic, a preparation method of the ceramic, a self-adsorption lithium-air battery and a preparation method of the battery relate to the technical field of lithium-air batteries. The invention aims to solve the problem that the water in the traditional water-based lithium-air battery is continuously consumed but it is inconvenient to add it in time. The invention adopts dry pressing, spin coating, and sintering methods to successfully realize the preparation of a double-layer composite structure electrolyte, and uses the methods of impregnation and vacuum drying to prepare a water vapor adsorption layer in the porous electrode, and uses the water vapor adsorption layer to achieve water absorption and water retention. Objective To solve the problem of water addition in aqueous lithium-air batteries. The invention is applicable to the field of preparation of self-adsorption lithium-air batteries.
Owner:HARBIN INST OF TECH

An electrode treatment method applied to the direct synthesis of hydrogen peroxide by oxygen electroreduction

The invention relates to a material processing method, in particular to an electrode processing method applied to direct synthesis of hydrogen peroxide through oxygen electroreduction, and belongs to the field of hydrogen peroxide direct synthesis through electrochemistrical oxygen reduction. A processing method for etching a graphite felt electrode through ferrocene-glacial acetic acid solution steam is designed; the glacial acetic acid-ferrocene solution steam is injected under the high-temperature oxygen-free condition to etch the surface of the graphite felt electrode, the original smooth graphite felt microcosmic surface becomes rough and porous through the etching process, and the specific surface area can be simply and effectively increased; and meanwhile, surface changes cannot influence the graphite felt structure, and the mechanical property is kept well. In this way, the aims of improving the electrode activity and being free of influences on stability are achieved. The problem that an existing technology for direct synthesis of hydrogen peroxide through electro-catalysis oxygen reduction is low in electrode catalysis activity is solved.
Owner:SUN YAT SEN UNIV

A kind of preparation method of efficient and stable ruthenium dioxide-based acidic oxygen evolution electrocatalyst

The invention provides a method for preparing an efficient and stable ruthenium dioxide-based acidic oxygen evolution electrocatalyst. In the method, carbon cloth is used as a base, ruthenium trichloride solution is dipped and coated on the carbon cloth, and then heat treatment is performed to oxidize ruthenium trichloride into ruthenium dioxide. The obtained ruthenium dioxide is supported on the carbon cloth in the form of nano-scale particles, has the characteristics of high catalytic activity and stable catalytic effect, and can be used as an anode of an industrial acidic water electrolysis hydrogen production device.
Owner:NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI

Metal boride water splitting catalyst, preparation method and application in electrocatalytic water splitting

Metal boride water splitting catalysts, preparation methods and applications in electrocatalytic water splitting belong to the technical field of electrocatalyst preparation. The metal boride catalyst of the present invention is prepared by a solid-phase boronizing method, using a solid boronizing agent to coat the transition metal, and performing boronizing treatment by programmed temperature heating. The boronizing agent consists of the necessary boronizing medium and optional activators and optional fillers. Compared with liquid boronization, the solid boronization method is less difficult to clean the surface after boronization, has low equipment requirements, and is suitable for the boronization treatment of various transition metals. The catalyst of the invention has excellent intrinsic catalytic activity and stability under alkaline conditions: the current density is 10mA cm ‑2 At this time, the required overpotential is 300mV ~ 400mV; and the stability of electrocatalytic water splitting and oxygen desorption can be as long as at least 100 hours, and the performance does not decay. It can replace precious metals and promote the commercial application of electrocatalytic water splitting.
Owner:合肥动量守恒绿色能源有限公司

Preparation method of Pt-Ag/porous polyaniline electrode material

The invention belongs to the field of a fuel cell, and particularly relates to a preparation method of a Pt-Ag / porous polyaniline electrode material. Specific to the shortcomings of limited resourcesand high cost of a Pt catalytic material, the invention provides the preparation method of Pt-Ag / porous polyaniline. Porous polyaniline is prepared by adopting a chemical method, and then a Pt-Ag / porous polyaniline nanocomposite is prepared by adopting an electro-deposition method; electrocatalytic oxidation effects of Pt / porous polyaniline composite electrodes modified by different metals of Fe,Mn and Sn on glycerinum are compared synchronously, and it is determined that the Pt-Ag / porous polyaniline material has the best electrocatalytic oxidation effect on glycerinum; then influence of Pt,and Ag deposition sequences and deposition number of turns on electrocatalytic oxidation of glycerinum are further compared; and it is determined that the best electrode performance of the Pt-Ag / porous polyaniline can be achieved by deposition of Pt first and then deposition of At later at the deposition number of turns of 300. Therefore, the composite fuel has the potential application prospect on the aspect of the fuel cell.
Owner:CHANGZHOU UNIV
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