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235results about How to "Avoid phase separation" patented technology

Preparation method for multi-component net-shaped nanofiber membrane

The invention relates to a preparation method for a multi-component net-shaped nanofiber membrane. The preparation method includes the detailed steps that step1, mixing and beating are performed on meta-position aramid fibers, halogen salt and organic solvent by the mass ratio of 1:0.004-0.4:2.996-18.6, and a meta-position aramid fiber solution is prepared through mixing; step2, functionality high-molecular polymers and the solvent are mixed by the mass ratio of 1:5.4-98.99, then nano-particles are added, and heating and mixing are performed to prepare a functionality high-molecular solution, wherein the mass fraction of the nano-particles in the solution is 0.01-5%; step3, the meta-position aramid fiber solution obtained in the step1 and the functionality high-molecular solution obtained in the step2 are mixed by the mass ratio of 1:0.05-0.5 in a dripping mode, and then ultrasonic treatment is performed to obtain a spinning solution; step4, under the conditions of 20 DEG C-30 DEG C indoor temperature and 20-70% relative humidity, the spinning solution is used for electrostatic spinning, and finally the multi-component net-shaped nanofiber membrane with a 5nm-20nm net-shaped nanofiber diameter and reaches over 95% in net-shaped structure coverage rate is obtained. The preparation technology is simple and low in cost, tensile strength of material reaches 100MPa-2000MPa, and the functionality advantage is remarkable.
Owner:DONGHUA UNIV

Aqueous alkyd acrylic resin paint and preparation method thereof

The invention relates to an aqueous alkyd acrylic resin paint and a preparation method thereof. According to the invention, high-molecular alkyd resin with main chain containing unsaturated double bond is synthesized through molecular design. Alkyd resin is subjected to free radical graft copolymerization with acrylic monomer. A reaction system is neutralized by using an amine compound, such that water-reducible alkyd acrylic resin is synthesized. Molecular chains of alkyd and acrylic resins are connected through chemical bond, such that the compatibility of the two resins is improved. In a material curing and shaping process, phase separation of the resin is avoided. Deionized water, a pigment, a filling material, an antifoaming agent, a dispersing agent, a siccative, and alkyd acrylic hybrid emulsion are uniformly dispersed, such that the aqueous alkyd acrylic resin paint is obtained. The aqueous alkyd acrylic resin paint comprises the components of: aqueous alkyd acrylic resin 65%-80%, the pigment 3%-4%, the filling material 6-10%, deionized water 10%-20%, the dispersing agent 0.05%-0.5%, the antifoaming agent 0.10%-0.30%, and the siccative 0.9%-3.5%.
Owner:LANZHOU UNIVERSITY OF TECHNOLOGY

Ethylene/alpha-olefin/non-conjugated polyene copolymer, and production process and use thereof

ActiveUS20160355622A1Small long-chain branch contentExcellent curing propertyPlastic/resin/waxes insulatorsSpecial tyresChemistryStructural unit
A novel ethylene / α-olefin / non-conjugated polyene copolymer comprising structural units derived from ethylene (A), an α-olefin (B) of 3 to 20 carbon atoms, and a non-conjugated polyene (C) containing intramolecularly two or more partial structures in total selected from the group consisting of structures of Formulae (I) and (II), and having a small number of long-chain branches,The novel ethylene / α-olefin / non-conjugated polyene copolymer contains a non-conjugated polyene such as VNB as a copolymerization component and a small long-chain branch content and is excellent in curing properties in the case of crosslinking using peroxide; and a process for producing the ethylene / α-olefin / non-conjugated polyene copolymer, and a use thereof are provided.
Owner:MITSUI CHEM INC

Method for preparing stable-dispersibility pigment/polymer core-shell structure composite granules by using by polymer-wrapped pigment particles

The invention relates to a method for preparing stable-dispersibility pigment / polymer core-shell structure composite granules by using polymer-wrapped pigment particles. The method comprises the following steps of: preparing an amphipathic macromolecular dispersing agent by the soap-free emulsion polymerization in the presence of 1,1-diphenyl ethylene (DPE); adding pigment particle disperse liquid subjected to ultrasonic dispersion into a system; and heating the pigment particle disperse system to the temperature of 80 DEG C again, wherein the surface of the pigment particle disperse system is grafted, and an amphipathic macromolecular dispersing agent is adsorbed to the surface of the pigment particle disperse system, dripping a hard monomer into the system, grafting, and triggering the hard monomer added into the system to perform in-situ polymerization on the surfaces of the pigment particles to form a polymer shell layer by amphipathic macromolecules which are adsorbed to the surfaces of the pigment particles and contain DPE active structures. The appearance and the surface macromolecular shell layer of the pigment / polymer core-shell structure composite granules are subjected to characterization by using a transmission electron microscope, an ultraviolet absorption spectrum, nuclear magnetic resonance hydrogen, a carbon spectrum and a thermogravimetric analyzer.
Owner:NORTHWESTERN POLYTECHNICAL UNIV

Aqueous alkyd acrylic resin printing ink and preparation method thereof

The invention relates to an aqueous alkyd acrylic resin printing ink and a preparation method thereof. According to the invention, high-molecular alkyd resin with main chain containing unsaturated double bond is synthesized through molecular design. Alkyd resin is subjected to free radical graft copolymerization with acrylic monomer. A reaction system is neutralized by using an amine compound, such that water-reducible alkyd acrylic resin is synthesized. Molecular chains of alkyd and acrylic resins are connected through chemical bond, such that the compatibility of the two resins is improved. In a material curing and shaping process, phase separation of the resin is avoided. Deionized water, a pigment, a filling material, an antifoaming agent, a dispersing agent, a siccative, and alkyd acrylic hybrid emulsion are uniformly dispersed, such that the aqueous alkyd acrylic resin printing ink is obtained.
Owner:LANZHOU UNIVERSITY OF TECHNOLOGY

Inorganic hydrous salt phase change energy storage microcapsule and preparation method thereof

The invention discloses an inorganic hydrous salt phase change energy storage microcapsule and a preparation method thereof. According to the microcapsule, an inorganic hydrous salt phase change material serves as a core material, and a high polymer serves as a capsule wall material. By means of a selection of an appropriate organic solvent, a surface active agent serves as a supplement, polymer monomer materials of the core material and the capsule wall material form an evenly dispersed mixed solution under the ultrasonication action, by means of an addition of functional additives of an initiating agent, a lubricating agent, a stabilizing agent, and a retarder and the like, under the reaction condition, the polymer monomers are subjected to suspension polymerization and solidification in the mixed solution, and then the core material is coated by the polymer monomers to form a phase change energy storage microcapsule. The preparation method is simple in operation and low in equipment requirements, the preparation method range of an inorganic core microcapsule is effectively widened, and by means of the sealing form of the microcapsule, the problems of the supercool and the phase separation of the hydrous salt phase change material are solved.
Owner:GUANGDONG UNIV OF TECH

Preparation method of nylon-6-based polyesteramide fiber

ActiveCN109706536ASuperposition of excellent characteristicsLarge irregularityMonocomponent copolyamides artificial filamentPolyesterPolymer science
The invention relates to a preparation method of a nylon-6-based polyesteramide fiber. The method comprises the steps of carrying out melt spinning on a nylon-6-based polyesteramide polymer to obtainthe nylon-6-based polyesteramide fiber. A preparation method of the nylon-6-based polyesteramide polymer comprises the steps of mixing nylon-6 prepolymer ester with a polyester prepolymer and then carrying out an ester exchange reaction to obtain the nylon-6-based polyesteramide polymer. The nylon-6 prepolymer ester is prepared by firstly synthesizing a dibasic-acid-terminated nylon-6 prepolymer and then adding dihydric alcohol to enable dihydric alcohol to react with carboxyl of terminal groups. According to the preparation method of the nylon-6-based polyesteramide fiber, the nylon-6-based polyesteramide polymer is obtained through a copolymerization approach, so that the uniformity of nylon-6 and polyester blocks is improved, and the phase domain is controllable; polyesteramide slices containing polyester chain segments at different ratios can be obtained by changing the addition quantity of the polyester prepolymer, so that the sequence structure is controllable, and the polymerization process is flexible. The prepared fiber has high spinnability and stiffness and can be applied to the fields of clothing, home textiles, automobile interior decoration and the like.
Owner:JIANGSU NEW HORIZON ADVANCED FUNCTIONAL FIBER INNOVATION CENT CO LTD

Paraffin suppressant compositions, and methods of making and using

Disclosed herein are graphene quantum dot tagged paraffin suppressants such as graphene tagged paraffin inhibitors and paraffin dispersants and methods of making and using thereof. The graphene quantum dots are covalently bound to residues of paraffin inhibitors or dispersed with paraffin dispersants to form tagged paraffin suppressants active in inhibiting paraffin crystallization or dispersing crystalized paraffin wax in crude oils and compositions comprising crude oils. The dots can be tailored to fluoresce at wavelengths with minimized correspondence to the natural fluorescence of crude oils, enabling the measurement of the concentration of the paraffin suppressants in crude oils or compositions comprising crude oils. The tagged suppressants are used to trace the dispersion and disposition of the paraffin suppressants in oils and compositions comprising them, for example within crude-oil recovery, production, processing, or conveyance and transportation, by in situ sampling the oil or composition and measuring the fluorescence of the sampled material.
Owner:CHAMPIONX USA INC
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