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37 results about "Ethyl phosphonate" patented technology

Method for microwave synthesis of organic phosphine-functionalized imidazolium-based ionic liquid

The invention relates to a method for microwave synthesis of organic phosphine-functionalized imidazolium-based ionic liquid. The method is characterized by comprising the following steps of: mixing imidazole compounds with bromo-alkyl diphenyl phosphine oxide, bromo-alkyl phenyl ethyl phosphonate or bromo-alkyl diethyl phosphonate at a molar ratio of 1:(1-1.2) during preparation, putting the mixture into a microwave reacting device, reacting for 60-150 minutes at the microwave power of 280-500 W and the reaction temperature of 80-120 DEG C to obtain crude products, and removing unreacted raw materials, so as to obtain the organic phosphine-functionalized imidazolium-based ionic liquid. According to the method, a novel organic phosphine-functionalized imidazolium-based ionic liquid is provided and is simultaneously synthesized by utilizing microwave radiation and heating in an efficient, quick and low-cost manner, the reaction time is greatly shortened, the reaction rate is improved, and the yields of all the prepared ionic liquids are relatively high; the raw material utilization ratio is relatively high, no by-product is produced, and the synthesized ionic liquid is easy to purify.
Owner:NINGBO UNIV

High-adhesion high-gloss black UV inkjet ink and preparation method and application thereof

The invention relates to high-adhesion high-gloss black UV inkjet ink which comprises, by weight, 10-20 parts of black color paste, 10-20 parts of polyurethane acrylate resin, 50-70 parts of reactivediluents, 6-10 parts of photoinitiator and 3-4 parts of auxiliaries. The reactive diluents include, by mass part, a first reactive diluent, a second reactive diluent and a third reactive diluent according to a consumption ratio of 2-3:1-2:2-3; the photoinitiator is at least one of 1-hydroxy-cyclohexylbenzophenone, 2, 4, 6-trimethylbenzoyl-diphenyl phosphine oxide and 2, 4, 6-trimethylbenzoyl ethylphenyl phosphoinate; the auxiliaries include defoamer, leveling agent, adhesion accelerant and polymerization retarder. The invention provides a preparation method and application of the high-adhesion high-gloss black UV inkjet ink. The black UV inkjet ink has the advantages of high gloss value, high adhesion and high hardness.
Owner:SOUTH CHINA AGRI UNIV +2

Weeding composition containing herbicide O,O-dimethyl-1-(2,4-dichlorophenoxy acetoxy) ethyl phosphonate

The invention relates to a weed control composition for plant haulm treatment, which comprises compound an and compound b with the general formula (1) as active compositions, wherein b is selected from any of the following compounds, tribenuron-methyl, thifensulfuron methyl, metsulfuron-methyl, chlorsulfuron, bensulfuron-methyl, isoproturon, siduron, quinclorac, mefenacet,.alachlor, acetochlor, butachlor and metolachlor. The invention also discloses the preparation of the weed control composition, the method for weeds removing, and the use of the weed control composition as herbicide for haulm processing.
Owner:HUAZHONG NORMAL UNIV

Process for preparing methyl ethylphosphinate and methyl ethylphosphinate aluminum salt

The invention discloses a process for preparing methyl ethylphosphinate and methyl ethylphosphinate aluminum salt, and belongs to the technical field of flame-retardant materials, aiming to solve thedifficulty in realization of industrial production of the methyl ethylphosphinate in the prior art. The process for preparing the methyl ethylphosphinate and the methyl ethylphosphinate aluminum saltincludes taking sodium iodide as a catalyst, and reacting methyl diethylphosphinate at the temperature of 80-180 DEG C to generate the methyl ethylphosphinate; reacting the methyl ethylphosphinate with aluminum trichloride in a solvent to obtain the methyl ethylphosphinate aluminum salt. The process has the advantages that the low-purity methyl diethylphosphinate serves as a raw material, the methyl ethylphosphinate is obtained under a moderate condition and at high yield, and industrialization is realized easily; methyl ethylphosphinate aluminum flame retardants with high phosphorus content are further obtained, and are environment-friendly halogen-free flame retardants for polymer materials.
Owner:LIER CHEM CO LTD +1

Method of Treating Citrus Plants to Reduce Bacterial Infections

A method of treating a citrus plant is provided to reduce the incidence of one or more insect-vectored bacterial infections such as citrus greening. The method comprises the step of applying a treatment composition one or more times to the plant, wherein the treatment composition comprises an effective amount of aluminum tris(O-ethyl phosphonate).
Owner:BAYER CROPSCIENCE AG

Triazine triphenyl phosphinic acid ethyl ester flame retardant composition and application method thereof

The invention relates to a triazine triphenyl phosphinic acid ethyl ester flame retardant composition and an application method thereof. The flame retardant composition is prepared by compounding and uniformly mixing any two, three or four of melamine cyanurate (MCA), melamine pyrophosphate (MPP), 9, 10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) and pentaerythritol methyl silicate (PEMS) with triazine triphenyl phosphinic acid ethyl ester (TTPE) at any proportion, wherein the weight part of the TTPE is greater than zero. The flame retardant composition provided by the invention has the advantages of multielement synergic effect, good flame retardancy, good compatibility with materials, low cost, zero halogen, environmental protection and the like, can be used as a flame retardant for polyester PET, polyester PBT, polyurethane, polypropylene, epoxy resin and other materials, and has excellent application and popularization prospects.
Owner:SHANDONG XINGQIANG CHEM IND TECH RES INST CO LTD

Organic phosphine-functionalized pyridine-based ionic liquid and preparation method thereof

The invention relates to organic phosphine-functionalized pyridine-based ionic liquid and a preparation method thereof. The preparation method is characterized by comprising the following steps of: mixing pyridine compounds with bromo-alkyl diphenyl phosphine oxide, bromo-alkyl phenyl ethyl phosphonate or bromo-alkyl diethyl phosphonate at a molar ratio of 1:(1-1.2), adding organic solvents, putting the mixture into a microwave reacting device, carrying out stirring for reaction for 60-150 minutes at the microwave power of 350-500 W and the reaction temperature of 80-110 DEG C to obtain crude products, and removing unreacted raw materials, so as to obtain the organic phosphine-functionalized pyridine-based ionic liquid. According to the method, the novel organic phosphine-functionalized pyridine-based ionic liquid is provided and simultaneously is synthesized by utilizing microwave heating, the reaction time is greatly shortened, and the reaction rate is improved; the raw material utilization ratio is relatively high, no by-product is produced, and the synthesized ionic liquid is easy to purify and has the characteristics of high efficiency, speediness and low cost.
Owner:NINGBO UNIV

Axitinib sustained-release implplant treating for solid tumor

The invention relates to an Axitinib sustained-release implant for treating a solid tumor, which is characterized in that: the sustained-release implant contains an effective anticancer amount of Axitinib and sustained-release excipients and a certain amount of sustained-release regulator. The solid tumors include the liver cancer, the lung cancer, the esophageal canner, the gastric canner, the breast canner, the ovarian canner, the prostate canner, the bladder canner and the rectum canner. The sustained-release excipients are mainly a copolymer of polylactic acid, glycollic acid and hydroxyacetic acid and one of the three materials, polifeprosan, poly-(L-lactide-co-ethyl phosphonate) and Poly(L-lactide-co-propyl phosphonate) or a combination of the three materials, in the degradation and absorption process of which the Axitinib is sustainedly released to part of the tumor, thus the entire toxicity of the Axitinib is significantly reduced while an effective medicine consistency is maintained on part of the tumor. That the sustained-release implant is implanted inside part of the tumor can not only reduce the entire toxicity of the Axitinib, but also enhance the medicine consistency on part of the tumor, thereby increasing the curing effect of non-operative therapeutics such as chemotherapeutic drugs and radiotherapy.
Owner:JINAN SHUAIHUA PHARMA TECH

Preparation method of 2,4,6-trimethyl benzoyl phenyl ethyl phosphinate

The invention relates to a preparation method of 2,4,6-trimethyl benzoyl phenyl ethyl phosphonate, and in particular relates to a method for preparing 2,4,6-trimethyl benzoyl phenyl ethyl phosphonate through the steps of carrying out substitution condensation reaction on dichlorophenyl phosphine and ethanol to obtain an intermediate; performing condensation reaction on the intermediate and 2,4,6-trimethyl benzaldehyde under an alkaline condition, and finally performing oxidation by using an oxidant under catalysis of a catalyst. The preparation process of 2,4,6-trimethyl benzoyl phenyl ethyl phosphonate, disclosed by the invention, has the advantages as follows: the influences of an acidic medium on the intermediate can be avoided; the requirements of the condensation reaction between 2,4,6-trimethyl benzaldehyde and phenyl ethyl hypophosphite for reaction equipment can be reduced; meanwhile, the reaction yield can be ensured; the preparation process is simple in operation and is suitable for industrial production.
Owner:CHANGZHOU JIURI CHEM CO LTD

Pirarubicin sustained-release implant treating for solid tumor

The invention relates to a Pirarubicin sustained-release implant for treating a solid tumor, which is characterized in that: the sustained-release implant contains an effective anticancer amount of Pirarubicin and sustained-release excipients and a certain amount of sustained-release regulator. The solid tumors include the esophageal canner, the gastric canner, the breast canner, the ovarian canner, the prostate canner, the bladder canner, the liver canner, the lung canner, and the rectum canner. The sustained-release excipients are mainly a copolymer of glycollic acid and hydroxyacetic acid and one of the two materials, polifeprosan and poly-(L-lactide-co-ethyl phosphonate), or a combination of the two materials, in the process of degradation and absorption of which the Pirarubicin is sustainedly released to part of the tumor, thus the entire toxicity of the Pirarubicin is significantly reduced while an effective medicine consistency is maintained on part of the tumor. That the sustained-release implant is implanted inside part of the tumor can not only reduce the entire toxicity of the Pirarubicin but also enhance the medicine consistency on part of the tumor, thereby increasing the curing effect of non-operative therapeutics such as chemotherapeutic drugs and radiotherapy.
Owner:JINAN SHUAIHUA PHARMA TECH

Combustible cartridge case/box slurry formula and preparation method of combustible cartridge case/box

The invention provides a combustible cartridge case / box slurry formula and a preparation method of a combustible cartridge case / box. The formula comprises 100 parts of acrylic resin, 1-4 parts of a photoinitiator, 40-100 parts of a reactive diluent and 100-246 parts of explosive crystals, wherein the explosive crystals are one or a mixture of 1, 3, 5-trinitro-1, 3, 5-triazacyclohexane and 1, 3, 5, 7-tetranitro-1, 3, 5, 7-tetraazacyclooctane, the acrylic resin is epoxy acrylic resin, polyurethane acrylic resin or a mixture of the epoxy acrylic resin and the polyurethane acrylic resin, the photoinitiator is one or a mixture of 2, 4, 6-trimethylbenzoyl phenyl phosphonic acid ethyl ester and 4, 6-trimethylbenzoyl-diphenyl phosphine oxide, and the reactive diluent is one or a mixture of 2-(2-ethyoxyl ethyoxyl) ethyl acrylate and trimethylolpropane triacrylate. The formula provided by the invention can be used for 3D printing preparation. The powder force of the prepared combustible cartridge case / box reaches 845 J / g, the 5s explosion point is 356.6 DEG C, the spontaneous combustion resistance temperature at the temperature of 245 DEG C is larger than 300 s, and the hygroscopicity under the conditions that the temperature is 25 DEG C and the relative humidity is 89% is 0.5%.
Owner:XIAN MODERN CHEM RES INST

Preparation method of UV LED photoinitiator

PendingCN114478844ALow mobilityInitiation rate is fastPhenacylP-Cresol
The invention discloses a UV LED photoinitiator preparation method, which comprises: (1) dissolving a carbazole derivative in an organic solvent, adding an inorganic alkali, stirring, adding a bromo-alkenyl derivative, completely reacting, carrying out a quenching reaction, and purifying to obtain a product 1; (2) dissolving the product 1 in the step (1) in an organic solvent, adding into 2, 4, 6-trimethylbenzoyl ethyl phosphonate, dropwise adding p-cresol, and stirring; performing reflux reaction and purification to obtain a product 2; (3) dissolving the product 2 in the step (2) and methyltriphenylphosphonium bromide in N, N-dimethylformamide, stirring and reacting, and purifying to obtain a product 3; and (4) dissolving the product 3 in the step (3) in an organic solvent, adding zinc trichloride, stirring for reaction, and purifying to obtain the UV LED photoinitiator. The compound is used for a UV-LED photocuring coating and has the advantages of being low in migration rate, high in initiation rate, easy to dissolve and the like, and the synthesis method is high in yield.
Owner:深圳市科信新材料科技有限公司

High performance liquid phase continuous automatic production and co-production technology of organic phosphine compound

The invention relates to the field of photocuring functional new material chemicals, and discloses a high performance liquid phase streamline type continuous automatic production technology of an acylphosphine oxide organic phosphine compound for the first time, which not only can produce a single specific target product, but also can co-produce a product mixture of two or more than two of the products of the type. The process technology has outstanding low-cost economic competitiveness and environment-friendly characteristics for large-scale manufacturing of target products. The target product comprises sym-trimethylbenzoyl diphenyl phosphine oxide (also known as 2, 4, 6-trimethylbenzoyl diphenyl phosphine oxide, trade name TPO), sym-trimethylbenzoyl phenyl ethyl phosphonate (trade name TPO-L) and structural analogues thereof, and a mixture of the sym-trimethylbenzoyl diphenyl phosphine oxide and the sym-trimethylbenzoyl phenyl ethyl phosphonate. The organic phosphine compound is an olefinic bond-containing (C=C) unsaturated radiation polymerization system photoinitiator and / or flame retardant and the like with wide application.
Owner:SHENZHEN UV-CHEMTECH CO LTD

Sorafenib sustained-release implant treating for solid tumor

The invention relates to a Sorafenib sustained-release implant for treating a solid tumor, which is characterized in that: the sustained-release implant contains an effective anticancer amount of Sorafenib and sustained-release excipients and a certain amount of sustained-release regulators. The solid tumors comprise the esophageal canner, the gastric canner, the breast canner, the ovarian canner, the prostate canner, the bladder canner, the liver canner, the lung canner, and the rectum canner. The sustained-release excipients are mainly a copolymer of glycollic acid and hydroxyacetic acid and one of the two materials, polifeprosan and poly-(L-lactide-co-ethyl phosphonate), or a combination of the two materials, in the process of the degradation and absorption of which the Sorafenib is continuously released to part of the tumor, thus the entire toxicity of the Sorafenib is significantly reduced while an effective medicine consistency is maintained on part of the tumor. That the sustained-release implant is implanted inside part of the tumor can not only reduce the entire toxicity of the Sorafenib but also enhance the medicine consistency on part of the tumor, thereby increasing the curing effect of non-operative therapeutics such as chemotherapeutic drugs and radiotherapy.
Owner:JINAN SHUAIHUA PHARMA TECH

Anti-aging PC-ABS alloy material and preparation method thereof

PendingCN111363294AImprove performanceHigh light and heat resistanceEthyl phosphonateMeth-
The invention relates to the technical field of modified materials, and concretely relates to an anti-aging PC-ABS alloy material and a preparation method thereof. The PC / ABS alloy material comprises,by weight, 28-35 parts of PC resin, 55-65 parts of ABS resin, 3-5 parts of an anti-aging agent, 10-15 parts of epoxy acrylate resin, 1-2 parts of 2,4,6-trimethylbenzoyl ethyl phosphonate, 3-8 parts of a compatilizer, 3-8 parts of a flexibilizer and 2-6 parts of a filler. The anti-aging PC-ABS alloy material disclosed by the invention is high in anti-aging performance, high in strength, high in impact resistance and excellent in comprehensive performances. The preparation method of the anti-aging PC-ABS alloy material is simple to operate, convenient to control, low in production cost and highin product quality, so that the prepared anti-aging PC-ABS alloy material is stable in performances, high in photo-thermal resistance and resistant to aging, and can be used for large-scale production.
Owner:东莞市高能高分子材料有限公司

Method for synthesizing alpha-aryl ethyl phosphonate

The invention discloses a method for synthesizing alpha-aryl ethyl phosphonate.The method comprises the following steps that alpha-aryl vinyl phosphonate, potassium phosphate and o-nitro-benzenesulfonyl hydrazide are added into a reactor; after vacuumizing is conducted, N2 is introduced to remove oxygen; under the protection of N2, anhydrous acetonitrile is added, and stirring is conducted for 5-10 h at room temperature; after the reaction is finished, water is added into a reaction mixture for dilution, extraction is conducted with ethyl acetate, drying is conducted with sodium sulphate anhydrous, mixed liquor of petroleum ether and ethyl acetate serves as eluent, column chromatography isolation is conducted, distillation is conducted finally, and alpha-aryl ethyl phosphonate is obtained.According to the method for synthesizing alpha-aryl ethyl phosphonate, transition metal does not participate, the substrate universality is good, the compatibility of a functional group is high, the reaction condition is mild, the reaction efficiency is high, and operation is safe, easy and convenient.
Owner:NINGBO UNIVERSITY OF TECHNOLOGY

A kind of synthetic method of two (2-methoxyphenyl) phosphine oxides

The invention belongs to the technical field of fine chemicals, and in particular relates to a synthetic method of bis(2-methoxyphenyl)phosphine oxide, which comprises the following steps: a) reacting anisole and triethyl phosphate in a solvent , to obtain bis(2-methoxyphenyl) ethyl phosphonate; b) the bis(2-methoxyphenyl) ethyl phosphonate is hydrogenated and reduced in a solvent to obtain bis(2-methoxy phenyl)phosphine oxide. The present invention takes anisole as the starting material, first reacts with triethyl phosphate to obtain bis(2-methoxyphenyl) ethyl phosphonate, and then synthesizes bis(2-methoxyphenyl) through hydrogenation reduction ) phosphine oxide, the method has simple reaction, high conversion rate, excellent product quality, and the content of bis(2-methoxyphenyl) phosphine oxide produced is more than 98%, which satisfies the technology of producing relevant polyketone ligands in the market Requirements, and the operation steps are simple, the required equipment is simple, and the energy consumption is low.
Owner:CHAMBROAD CHEM IND RES INST CO LTD

Preparation method of ethyl methylethyl phosphinate

The invention relates to the technical field of methyl phosphinate, and discloses a preparation method of ethyl methylethyl phosphinate. The method comprises the following steps: mixing a substrate with a catalyst, then adding diethyl methylphosphite dropwise into the reaction system, and carrying out reaction to generate ethyl methylethyl phosphinate. According to the preparation method of ethylmethylethyl phosphinate, through a dropwise adding method, the probability of temperature rush due to rising of a highest temperature can be prevented from increasing, the safety risk is effectively reduced, and large-scale industrial production is facilitated. According to the method, while the usage amount of the catalyst is effectively reduced, the reaction rate does not show a decreasing trend, the advantages of safety, simple operation and the like are achieved, the purpose of large-scale industrial production can be achieved, and the problems that potential safety hazards exist in a one-pot method conversion process, the one-pot method reaction rate and efficiency are relatively low, the safety risk is high, and large-scale amplification is difficult are solved.
Owner:LIER CHEM CO LTD +1

Production method for medicine for preventing and treating verticillium dahliae

The invention discloses a production method for a medicine for preventing and treating verticillium dahliae. The production method comprises the following steps: A preparing materials including 50% copper(succinate+glutarate+adipate), 60% aluminum tris(-O-ethyl phosphonate), 86.2% cuprous oxide wettable powder, artemisinin, pulsatilla chinensis saponin, glycyrrhizic acid, Shuanghuanglian and pericarpium citri reticulatae; B carrying out alcohol digestion on an extracting solution of the Shuanghuanglian and the pericarpium citri reticulatae; C compounding the 50% copper(succinate+glutarate+adipate), the 60% aluminum tris(-O-ethyl phosphonate), the 86.2% cuprous oxide wettable powder, the artemisinin, the pulsatilla chinensis saponin and the glycyrrhizic acid with the extracting solution obtained in the step B; and agitating uniformly and carrying out ultraviolet sterilization to obtain the medicine for preventing and treating the verticillium dahliae. The production method is simple and the produced medicine is easy in proportioning and convenient to use, and has the good effect of treating eggplant verticillium; tests prove that a 400-600-time diluting solution of the mixture has an obvious inactivation effect on te fungi imperfecti verticillium dahliae and the sterilizing effect is good.
Owner:QINGDAO MAOFENG ORGANIC VEGETABLE

Preparation method and application of functionalized magnetic adsorption material

The invention discloses a preparation method of a functionalized magnetic adsorption material, and the method is characterized by comprising the following steps: adding ethyl 2, 5-dihydroxy-1, 4-benzene diphosphonate and / or diethyl 2, 5-dihydroxyphenyl phosphonate into a solvent A, adding nano ferroferric oxide, and reacting at a certain temperature to obtain a reacted material; cooling the reacted material, performing filtering and separating, washing the solid with a solvent B, and performing drying to obtain the functionalized magnetic adsorption material. The functionalized magnetic adsorption material prepared by the invention is of a porous structure, is formed by sparsely stacking spherical particles, and has rich functional groups such as hydroxyl groups and phosphorus oxygen groups; the functionalized magnetic adsorption material prepared by the method has the advantages of simplicity in synthesis, low cost, good selectivity, large adsorption capacity, convenience in collection after adsorption and the like, can be actually used for adsorbing, enriching or removing uranium in an aqueous solution, and is high in practicability.
Owner:SOUTHWEAT UNIV OF SCI & TECH

Preparation method of methyl propanal ethyl phosphonate as glufosinate-ammonium intermediate

The invention relates to a preparation method of methyl propanal ethyl phosphonate as a glufosinate-ammonium intermediate and belongs to the field of organic chemistry. The preparation method comprises the following steps: (1) taking 3,3-diethoxy propyl methyl ethyl phosphonate as a raw material, catalyzing and hydrolyzing via a catalyst to prepare methyl propanal ethyl phosphonate, wherein the catalyst is sulfonic acid resin, strong acid ion exchange resin or perfluorinated sulfonic acid resin; and (2) filtering the product obtained in the step (1) for recycling sulfonic acid resin, and carrying out pressure-reduced desolvation of filtrate to obtain methyl propanal ethyl phosphonate. The specific preparation method is as shown in the description. According to the preparation method of methyl propanal ethyl phosphonate as the glufosinate-ammonium intermediate, through optimization of the catalyst, the reaction time is greatly reduced; the yield is improved; meanwhile, the catalyst is easy to recycle and is reusable; the production cost is reduced.
Owner:内蒙古佳瑞米精细化工有限公司

Inorganic compound synthesized plastic filler and preparation method thereof

The invention provides inorganic compound synthesized plastic filler and a preparation method thereof. The filler is prepared from raw materials as follows: 3-4 parts of perfluoroalkyl ethyl phosphonate, 4-5 parts of polyethylene glycol, 5-8 parts of nano-carbon fiber, 3-5 parts of isocyanate, 4-8 parts of glycidol phenyl ether, 5-12 parts of diphenyl silanediol, 1.5-3.5 parts of polyester acrylate, 8-12 parts of alum, 3-7 parts of aluminum oxide, 3-7 parts of glycidol phenyl ether, 5-9 parts of an auxiliary and a plurality of parts of deionized water. The inorganic compound synthesized plastic filler prepared with the method has good lipophilicity and good compatibility with plastic, can improve the strength and the impact resistance of plastic and is good in self-lubricating property and low-temperature resistance.
Owner:青阳县吉祥塑胶有限公司

Efficient thick copper plate solder resist printing method

The invention discloses an efficient thick copper plate solder resist printing method. Ink adopted in the high-efficiency thick copper plate solder resist printing method mainly comprises the following raw materials by mass: 3, 4-epoxy cyclohexyl methyl methacrylate, amido resin, titanium dioxide, 3-methacryloyloxy propyl trimethoxy silane, propylene glycol methyl ether acetate and 2, 4, 6-trimethylbenzoyl phenyl ethyl phosphonate, and all the substances interact with one another, so that the ink can be used for preparing the high-efficiency thick copper plate solder resist printing ink. The ink has the advantages of favorable curing property, favorable adhesive force, excellent heat resistance, excellent weather resistance and high curing speed.
Owner:BAIQIANG ELECTRONICS SHENZHEN

The preparation method of ethyl 2,4,6-trimethylbenzoylphenyl phosphinate

The invention relates to a preparation method of 2,4,6-trimethyl benzoyl phenyl ethyl phosphonate, and in particular relates to a method for preparing 2,4,6-trimethyl benzoyl phenyl ethyl phosphonate through the steps of carrying out substitution condensation reaction on dichlorophenyl phosphine and ethanol to obtain an intermediate; performing condensation reaction on the intermediate and 2,4,6-trimethyl benzaldehyde under an alkaline condition, and finally performing oxidation by using an oxidant under catalysis of a catalyst. The preparation process of 2,4,6-trimethyl benzoyl phenyl ethyl phosphonate, disclosed by the invention, has the advantages as follows: the influences of an acidic medium on the intermediate can be avoided; the requirements of the condensation reaction between 2,4,6-trimethyl benzaldehyde and phenyl ethyl hypophosphite for reaction equipment can be reduced; meanwhile, the reaction yield can be ensured; the preparation process is simple in operation and is suitable for industrial production.
Owner:SHANDONG JIURI CHEM TECH CO LTD
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