378 results about "Chemical laboratory" patented technology

The invention discloses a preparation method for a co-doped type and separately-coded type ZnInS/ZnS dual-emitter quantum dot. The preparation method comprises preparation of white-light emitting ZnInS:Ag/ZnS/ZnS:Mn/ZnS and ZnInS:Ag & Mn/ZnS/ZnS/ZnS nano materials, wherein by adopting a core-shell structure, the ZnInS:Ag/ZnS/ZnS:Mn/Zn nano material is synthesized by the following steps of: (1) preparing a color-adjustable ZnInS: Ag core; (2) carrying out core-covering on a first molar layer ZnS; and (3) adsorbing Mn ions and carrying out cover-covering on second and third molar layers; and for the preparation of the ZnInS:Ag & Mn/ZnS/ZnS/ZnS nano material, injecting time of a Mn precursor in the step (3) is advanced to injecting time of an S precursor in the step (1). The preparation method adopts a single-pot thermal injection process, is simple in process, easy to operate, capable of being completed in common chemical laboratories, and easy to popularize; and raw materials are convenient to supply, and are low in price.

The invention relates to a full automatic extraction device, which is used for extraction experiment in a chemical laboratory. The device comprises a shell, a getter device, an extraction container and a tap funnel which are fixedly arranged on the shell, wherein the tap funnel is positioned on the upper part of the extraction container; the extraction container is communicated with the getter device through an air duct and connected positions are all closed; the bottom end of the extraction container is provided with an imbibition long tube; the imbibition long tube passes through an opening on the top part of the tap funnel to the bottom of the tap funnel; the bottom of the tap funnel is provided with a drain pipe; the drain pipe is provided with a control valve; and the getter device is arranged in the shell, an outlet of the getter device is connected with a vent pipe, and the vent pipe extends outside the shell. The device adopts batch type vacuumizing principle, guides organic phase and aqueous phase to come and go rapidly in the extraction container and the tap funnel so as to make a target compound sufficiently transfer from the aqueous phase to the organic phase, thereby realizing liquid-liquid extraction and separation. The device can replace manual operation and save time and labor, and has good uniformity, an experimenter cannot breathe harmful gas, so the device is favorable for protecting human body from harm.