35results about How to "Solve sintering" patented technology

The invention discloses a method for oxygen-enriched calcification calcination of high-grade vanadium slag. The method comprises the following steps of mixing high-grade vanadium slag and a calcification agent to obtain a mixture and carrying out calcination of the mixture in an atmosphere having oxygen volume content of 12 to 21%. The method for oxygen-enriched calcification calcination of high-grade vanadium slag greatly reduces a calcification calcination temperature of high-grade vanadium slag, solves the problem that in calcification calcination of high-grade vanadium slag, abnormal running problems such as material agglomeration and calcination equipment ring-forming are caused by a high calcination temperature, and improves an industrialization technology of calcification calcination of high-grade vanadium slag.

The invention discloses a metal oxide nanoparticle and a preparation method of the metal oxide nanoparticle, which comprises the following steps: preparing an organosol containing the metal element, mixing the organosol with a water-soluble salt, performing standing or centrifuging to precipitate the water-soluble salt, removing the superfluous organosol at the upper part, and keeping the temperature to convert the organosol into gel; along with evaporation of the solvent, shrinking the gel, and coating the surfaces of the water-soluble salt particles with a layer of xerogel film; and calcining the sample at a high temperature between 400 DEG C and a salt melting point, converting the dry gel film into metal oxide nanoparticles, dispersing and attaching the nanoparticles to the surfaces ofwater-soluble salt particles, cooling, and washing with water to remove the salt, thereby obtaining the high-dispersion metal oxide nanoparticles; if the calcined product is reduced in a reducing atmosphere, converting the metal oxide nanoparticles attached to the surfaces of the water-soluble salt particles into corresponding metal nanoparticles, cooling, and washing with water to obtain the high-dispersion metal nanoparticles. According to the method, the high-crystallinity and high-dispersion metal oxide and metal nanoparticles can be rapidly prepared in batches.

The invention discloses a tensile fixture for a platy sample, characterized by comprising fixture bodies (3 and 5) each of which provided with a pinhole (7) in one end and which are connected to tensile tester connection rods (1 and 6) through pins (2) so that axes of test tensile force, the fixture and a test piece are superposed; the other ends of the fixture bodies (3 and 5) are each provided with a vertical slot running through the fixture, the bottom of each groove slot is provided with a sample groove (8), the width of the sample grooves (8) is slightly greater than the thickness of the test piece (4) so that it is ensured that the test piece (4) may be placed in the fixture bodies (3 and 5) for a tensile test. The invention also discloses a tensile test method employing the fixture. According to the scheme of the invention, the end of each fixture body is provided with the vertical slot running through the fixture, and it is possible to carry out a tensile test for various samples of high strength, high hardness and high processing difficulty.

The invention discloses a preparation method of a high temperature stable titanium dioxide nanotube powder. According to the preparation method, firstly, a titanic acid nanotube powder is prepared via hydro-thermal synthesis, a silicon dioxide/titanium dioxide composite nanotube powder is obtained via surface modification and high temperature calcinations, and at last, silicon dioxide is removed via etching in a low-concentration sodium hydroxide solution so as to obtain the high temperature stable titanium dioxide nanotube powder. The high temperature stable titanium dioxide nanotube powder is capable of maintaining favorable tubular morphology at a high temperature higher than 400 DEG C, possesses excellent anatase crystal form and excellent catalytic effect, can be widely used in fields such as photocatalysis, lithium battery, solar cell, confinement catalysis, medical science, and catalytic combustion, and is capable of solving problems of the prior art that sintering, breaking, or even collapse of titanium dioxide nanotube are caused by surface or interlayer dehydration via calcination of titanic acid nanotube at a temperature higher than 400 DEG C.

The invention discloses a reaction device for preparing synthesis gas through catalytic reforming of methane and carbon dioxide, and belongs to the technical field of energy utilization. The reaction device comprises a gas distributor, a shell-pass shell and a gas collector which are connected in sequence, multiple gas reaction tubes are contained in an inner cavity of the shell-pass shell and are arrayed in a regular hexagon shape, one ends of the gas reaction tubes are arranged in the gas distributor, the other ends of the gas reaction tubes are arranged in the shell-pass shell, at least two layers of flame nozzles are connected to the outer surface of the shell-pass shell, and at least one layer of flame nozzles are matched with the corresponding gas reaction tubes and are arranged annularly. According to the reaction device for preparing synthesis gas through catalytic reforming of methane and carbon dioxide, the flame nozzles of the shell-pass shell are uniformly distributed along the side boundary of the hexagon array of the gas reaction tubes in the same direction, and the effects of stable and uniform heat transfer and easy temperature control are achieved.

The invention discloses a casting mold for a multiple directional control valve. The casting mold for the multiple directional control valve comprises a sand box, outer shells and a mud core. The mudcore is horizontally arranged in the outer shells, and the outer shells are embedded in the sand box. A cavity for the multiple directional control valve is formed between the outer shells and the mudcore. The number of the outer shells is two, the outer shells refer to the outer shell I and the outer shell II, the outer shell I and the outer shell II are arranged in the sand box side by side, and the two corresponding outer side surfaces of the outer shell I and the outer shell II are attached to each other. The mud core comprises a main core and a plurality of small cores, the main core andthe multiple small cores are assembled into the whole mud core through auxiliary holes, a core rod for forming the multiple directional control valve is arranged in the whole mud core, an air outlethole is formed in the top of the whole mud core, and the air outlet hole is guided out through a steel wire. By means of the casting mold for the multiple directional control valve, assembling difficulty of the mud core can be solved, and the number of defects of castings can be reduced.

The invention discloses an airtight sintering device of glass tubes and MEMS chips, which comprises a main frame, a heating furnace body, a lifting adjusting member, and a lifting pressure adjusting handle, a stop valve, an air exhaust connecting member, and the like. In the device of the invention, two MEMS chips are sintered together with a glass tube; the glass tube is connected to a vacuum-pumping device for vacuum pumping; the glass tube is sintered together with two MEMS chips through glass powder so as to form a vacuum microcavity; the invention solves the problem in traditional devices that organic gas which is generated during glass slurry sintering and is released into the vacuum microcavity can not be removed; the vacuum degree is up to 5*10-5 Pa, and the qualified rate of high-precision resonance-type pressure sensors is increased. The invention is applicable to fields of packaging technology of resonance-type pressure sensors in micro-electro-mechanical system manufacturing, and integrated circuit manufacturing.

The invention provides a rectangular open magnetic field type electromagnetic vibration table magnetic circuit structure with double-magnetic-circuit two-end symmetric excitation, belonging to the field of vibration measurement technology. A rectangular open type magnetic field structure design is provided. Two permanent magnets are symmetrically installed at two ends of a center magnet yoke and face magnetic poles. Two symmetric closed magnetic circuits are formed by magnet yokes. The magnetic induction intensity distribution with high uniformity is generated in air gaps. After a working coil is energized, the working coil is affected by Lorentz force in a magnetic field, and precisely controllable electromagnetic drive force is generated. The surfaces of the magnet yokes adjacent to the air gaps are provided with an array type micro structure in the form of deep trenches, and the eddy current loss can be effectively inhibited. According to the rectangular open magnetic field type electromagnetic vibration table magnetic circuit structure, large stroke, high magnetic field uniformity, high thrust and a linear electromagnetic driving force characteristic can be considered, the disadvantages in the existing technical scheme can be effectively solved, and a high precision and large stroke electromagnetic vibration table magnetic circuit structure technical scheme is provided for low-frequency/ultra-low frequency vibration calibration.

The invention provides a method for preparing yttrium aluminum garnet nanoparticles, which comprises the following steps: preparing organic sol containing aluminum and yttrium, mixing the organic solwith water-soluble salt, performing standing or centrifuging to precipitate the water-soluble salt, removing superfluous organic sol at the upper part, and keeping the temperature to convert the organic sol into gel; along with evaporation of the solvent, contracting the gel, and coating the surfaces of the water-soluble salt particles with a layer of xerogel film, and calcining a sample at a hightemperature between 600 DEG C and a salt melting point, converting a dried gel film into yttrium aluminum garnet nanoparticles, dispersing and attaching the yttrium aluminum garnet nanoparticles to the surfaces of water-soluble salt particles, cooling, and washing with water to remove the salt, thereby obtaining the yttrium aluminum garnet nanoparticles with favorable dispersity and crystallinity. According to the method, the high-dispersion and high-crystallinity yttrium aluminum garnet nanoparticles can be rapidly prepared in batches, and the method is suitable for preparing LED fluorescentpowder, YAG transparent ceramic and other materials.

The invention relates to a modified boron nitride loaded nickel-based methane dry reforming catalyst as well as a preparation method and application thereof. According to the method, different stripping methods are used for modifying the boron nitride, then the modified boron nitride is used as a carrier for supporting the active metal Ni, and the excellent sintering resistance and carbon deposition resistance are achieved in the methane dry reforming reaction. According to the invention, the content of Ni is adjusted by using a simple impregnation method, and the modified boron nitride loaded nickel catalyst with high activity and high stability is obtained. The catalyst can be used for solving the problems of sintering and serious carbon deposition of active components in a methane dry reforming reaction. The catalyst has the advantages of simple preparation process, low cost and high catalytic efficiency.

The invention relates to the technical field of welding, and aims to provide a stop-off agent for stainless steel vacuum brazing. The stop-off agent comprises, by weight percentage, 5-10% of zirconiapowder, 5-10% of titanium oxide powder, 35-55% of aluminum oxide powder, 0.5-5% of neodymium oxide powder, 0.15-0.5% of carbomer 940, 4.0-9.0% of VAE emulsion, 1.5-5% of methylcellulose, 2-4% of propylene glycol and 18-30.35% of deionized water. By means of the stop-off agent for stainless steel vacuum brazing, the problem that in the processing procedure of stainless steel vacuum brazing, oxide components in stop-off agents are sintered and cause hard aggregation or caking is solved. The stop-off agent can be removed through non-destructive modes like water washing and blowing after brazing,and the surface of a workpiece is not damaged.

The invention relates to a preparation method of a molybdenum modified molecular sieve loaded nickel-based methane dry reforming catalyst. The catalyst takes a molecular sieve as a carrier, nickel and molybdenum are respectively loaded on the molecular sieve by a sequential impregnation method, and dispersion of active species and strong interaction with the carrier are realized. The molybdenum-modified molecular sieve supported nickel catalyst is obtained through drying, high-temperature calcination and programmed heating reduction, the catalytic activity can be effectively improved, and carbon deposition in the reaction is effectively eliminated through dynamic conversion of molybdenum oxide and molybdenum carbide on the molecular sieve constructed in the reaction. Finally, the catalytic material with high sintering resistance and carbon deposition resistance is obtained. The catalyst has the advantages of simple preparation process, low cost and high catalytic efficiency.

The invention discloses an Rh@CuSiO3 nano-structure hydrogenation catalyst and a preparation method of same. The preparation method includes the steps of: 1) synthesizing silicate nanotubes in an ethanol-water system through a hydrothermal method, and controllably synthesizing cupric silicate nanotubes by adjusting experimental conditions; 2) supporting metal rhodium in the cupric silicate nanotubes through an impregnation method. In the Rh@CuSiO3 hydrogenation catalyst, the structural confinement effect of the core-sheath material and synergistic effect among the components are coupled, so that dispersity of active components is increased and interaction between the active components and the supporter is improved, thereby improving the catalytic performance in the hydrogenation. The catalyst has extensive application prospect.

The invention discloses a cooling core puller. The cooling core puller comprises a core-pulling fixing base and a core pulling body which is detachably connected to the core-pulling fixing base, wherein one end, away from the core-pulling fixing base, of the core pulling body is a shaping end; the shaping end comprises an outer shaping part and an inner shaping part; the outer shaping part surrounds the inner shaping part, and a gap is formed between the outer shaping part and the inner shaping part; a first cooling water channel is arranged in the core pulling body; from the mounting end, away from the shaping end, of the core pulling body, the first cooling water channel sequentially passes through the inner shaping part and the outer shaping part, and finally returns to the mounting endof the core pulling body, so that a cooling water channel with inner and outer layers is formed in the core pulling body, and thus, cooling water uniformly cools the core pulling body by circulatinginside the core pulling body. The shaping end of the core pulling body is a structure with inner and outer layers, and the cooling water channel with inner and outer layers is arranged in the core pulling body, so that the cooling effect of a workpiece is improved, and the surface sintering and workpiece expanding and blocking problem is solved.

The invention provides a double-permanent-magnetic-tube two-end symmetric excitation cylindrical closed magnetic field type electromagnetic vibration table magnetic circuit structure with eddy current compensation, belonging to the field of vibration measurement technology. A cylindrical closed type magnetic field structure design is provided. Two cylindrical permanent magnetic tubes are symmetrically installed at two ends of a magnetic circuit structure and face magnetic poles. Two symmetric closed magnetic circuits are formed by magnet yokes. The magnetic induction intensity distribution with high uniformity is generated in air gaps. After a working coil is energized, the working coil is affected by Lorentz force in a magnetic field, and precisely controllable electromagnetic drive force is generated. The surfaces of the magnet yokes adjacent to the air gaps are provided with an array type micro structure in the form of deep trenches, and the eddy current loss can be effectively inhibited. According to the double-permanent-magnetic-tube two-end symmetric excitation cylindrical closed magnetic field type electromagnetic vibration table magnetic circuit structure, large stroke, high magnetic field uniformity, high thrust and a linear electromagnetic driving force characteristic can be considered, and a high precision and large stroke electromagnetic vibration table magnetic circuit structure technical scheme is provided for low-frequency/ultra-low frequency vibration calibration.

The invention discloses a pyrolysis raw gas high-temperature efficient dust removal method which comprises the following steps of externally connecting an enclosure with induced draft equipment to form negative pressure in a gas purification chamber, and pumping high-temperature dust-containing raw gas into a pre-dust remover from an outlet of a coal gasifier to perform primary dust removal, enabling the pre-dedusted raw gas to enter a dust collection chamber, performing fine dedusting by utilizing a ceramic fiber filter tube, and enabling the pre-dedusted raw gas to enter a gas purification chamber to obtain high-temperature purified gas, transferring the high-temperature clean gas into a washing tower and a drop catcher for deep purification and cooling to finish dust removal, and afterlong-time work, using a high-pressure blowback system to perform blowback ash removal on the ceramic fiber filter tube. According to the dust removal method, high-temperature dust-containing raw gas can be directly filtered, the situation that the raw gas needs to be cooled before being filtered by a cloth bag dust removal device in an existing coal-to-gas process is improved, and the problem thatdust below 2 mum is removed and separated again is effectively solved.