The invention discloses a preparation method for a para-aminophenol ordered
mesoporous carbon catalyst. The preparation method is characterized in that
chitosan is taken as a
raw material, and non-
precious metal compounds are used as a
doping source, meanwhile, a triblock
copolymer surfactant is added, after performing self-produced
high pressure treatment under a high temperature hydrothermal condition, filtering is performed so as to obtain a dark brown
solid product, the
solid product is dried, ground, and then put into a tubular calcinator, and high temperature
carbonization under
inert gas
atmosphere protection is performed, so as to obtain a high-stable
metal-
doped carbon-based catalyst with different ordered mesoporous structures. The
catalytic efficiency of the high-stable
metal-
doped carbon-based catalyst for para-
nitrophenol hydrogenation catalysis generating para-aminophenol is investigated. The operation process has the main characteristics that the
biomass resource
chitosan is used as a
raw material and is
environmentally friendly, cheap and available; the surfactant is added, so that the formation of the ordered mesoporous structure is effectively controlled, the effective contact area between the reactant and the catalyst is increased, and the
reaction conditions are mild; an
active center and a carbon material are generated simultaneously, so that the structureis more stable, and the reaction process operationis simple.