The invention belongs to the field of
metal material structure analysis sample preparation and structure observation characterization, and particularly relates to an in-situ EBSD
observation method for microcosmic orientation evolution of recrystallized grains of
magnesium alloy. The method comprises the steps of firstly, carrying out mechanical
polishing on a
magnesium alloy sample, then preparing indentation mark points on the surface to be detected, and conducting EBSD observation for the first time on a target area after
ion etching; and taking out the sample, carrying out recrystallization annealing heat treatment and
ion etching, finding the same area according to the indentation mark points, carrying out EBSD observation for the second time, and similarly, completing subsequent required in-situ EBSD observation. According to the method, in-situ tracking characterization of recrystallization
nucleation,
grain growth and microscopic orientation evolution in the same area in the recrystallization annealing process of the
magnesium alloy is achieved, and the problems that the
magnesium alloy is low in calibration rate due to a
surface stress layer, an
oxide layer and pollutants,accurate positioning cannot be achieved, and in-situ EBSD observation is difficult to achieve are solved. The process is simple and controllable, the technical requirements on
sample preparation of experimenters are low, and the experiment success rate is high.