The invention discloses a preparing method of
Nitrogen-
doped carbon nano-material modified by
metal cobalt. The preparing method comprises the first step of adopting
Ethylene glycol-bis-(2-aminoethylether)-N,N,N',N'-tetraacetic acid or
ethylenediaminetetraacetic acid as a
carbon source and adding the
carbon source into a
beaker; the second step of stirring the
carbon source and using a
nitrogen source to adjust the ph value of a solution to be neutral till the carbon source is completely dissolved; the third step of adding water into
cobalt nitrate or
cobalt acetate to dissolve cobalt
nitrate or
cobalt acetate, putting dissolved cobalt
nitrate or
cobalt acetate into the solution of which the pH value is already adjusted; the fourth step of stirring the solution and afterwards again adjusting the pH value to be neutral, and putting the prepared solution into a
rotary evaporator to
spin out moisture; the fifth step of placing the solution to an electrothermal blowing
dry box to dry the solution and obtaining a
solid body; the sixth step of
grinding the obtained
solid body into
fine powder and placing the
fine powder into a porcelain boat, under the condition of the protection of
nitrogen, placing the porcelain boat in a
vacuum tube type high-temperature
sintering furnace to be subjected to heating and
roasting to prepare the
Nitrogen-
doped carbon nano-material modified by
metal cobalt. According to the preparing method of the
Nitrogen-
doped carbon nano-material modified by
metal cobalt, the steps of synthesis of carbon nano-materials,
doping of
nitrogen, and modification of metal
ion cobalt are integrated into one, thus the obtained catalyst is large in superficial area, stable in structure and property, and is applicable to
heterogeneous catalysis such as epoxidation of
alkene.