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125 results about "Natural diamonds" patented technology

Method for preparing high-performance polycrystalline diamond by utilizing hinge-type cubic press

The invention discloses a method for preparing high-performance polycrystalline diamond by utilizing a hinge-type cubic press. The method is characterized in that diamond or diamond-containing carbon powder are taken as raw materials, and any metal or ceramic binder is not added. After purification, the powder surfaces are purified for 0.5 h-5 h at a vacuum degree of 4*10<-3>-4*10<-5> Pa, at the temperature of 800-1500 DEG C. The diamond powder with purified surfaces is pre-formed, placed on the hinge-type cubic press, sintered for 1-30 min at the temperature of 1400-2500 DEG C, under the pressure of 8-20 GPa to prepare high-performance polycrystalline diamond block materials. The high-performance polycrystalline diamond is single in phase, chemical bonds are formed among crystal grains, and integrated closely on a large scale to form high-strength diamond- diamond interfaces. The high-performance polycrystalline diamond is almost the same as natural diamond monocrystalline in hardness, and is better than binder-containing artificial polycrystalline diamond in heat stability and hardness.
Owner:SICHUAN UNIV

Hot pressed and diamond impregnated drill tooth applicable to strong abrasive hard formation

The invention provides a hot pressed and diamond impregnated drill tooth applicable to a strong abrasive hard formation, which consists of a composite matrix and a natural diamond and is composed by a hot pressing and sintering process, wherein the composite matrix consists of 25-43% of WC (wolfram carbide), 15-25% of casting WC, 15-30% of Cu, 13-20% of Co, 11-17% of Ni, 1-3% of Mn, 1-2% of P and 0.5-1% of artificial single-crystal diamond powder; the natural diamond is a titanium coated natural diamond, the particle size range is 40-100 meshes, and the concentration is 75-110%; and the drill tooth is cylindrical. The drill tooth provided by the invention can be inlaid on a bit matrix in the vertical and horizontal ways and has cutting and grinding combined functions for rock breaking in the soft and hard interlaced and abrasive formation, high rock breaking efficiency and long service life.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Method for processing polycrystalline diamond for diamond processing

The invention provides a method for processing polycrystalline diamond for diamond processing. The method comprises the following steps of: mixing diamond powder and metal nickel serving as basic raw materials with a certain amount of boron, and adding the mixture into a carbon synthetic die; heating the synthetic die in a vacuum furnace in vacuum; putting a vacuum heated semi-finished product into a diamond hexa-orientation press for high temperature high pressure synthesis, and releasing pressure to obtain the polycrystalline diamond PCD for diamond processing. When the polycrystalline diamond PCD prepared by the technical scheme is used for processing the diamond, the product is soft, and has good impact toughness and higher abrasion resistance. Compared with polycrystalline diamond TSP series for petroleum and core bits, the polycrystalline diamond PCD has much lower abrasion consumption; and compared with natural diamond, the polycrystalline diamond PCD has higher grinding efficiency. Furthermore, the product has good self-sharpening performance and high grinding efficiency.
Owner:ZHENGZHOU SANHE DIAMOND

Surface set natural diamond bit and production process

InactiveCN101086199AGuaranteed outputBezel set firmlyDrill bitsAlloyGraphite
The invention discloses a surface set natural diamond bit, the carcass surface is inserted with natural diamond. Its production processes are: the first step, bit carcass cold-pressed forming, and binding natural diamond on the pre-modeling blocks; the second step, putting the pre-modeling blocks into the graphite mold; the third step, laying steel body on the graphite mold; the fourth step, non-pressure sintering; the fifth step, machining and finishing the products. The surface set natural diamond bit produced through the invention cam avoid the defect of diamond can not be used fully of the ordinary man-made diamond bit working layer, the cold-pressed forming also avoids the phenomenon of metal powder leak in the heat pressing forming sintering process, the consumption of metal (or alloy) is saved. The drilling efficiency of the surface set natural diamond bit is increased 30%, the drilling life is increased 100%. The invention is a manufacture process of surface set natural diamond bit has long use life of nit, low sintering temperature and short sintering time.
Owner:长沙锐合钻石工具有限公司

Multi-stage filleted high-pressure anvil

The invention discloses a multi-stage filleted high-pressure anvil and relates to exploration of synthesizing preparation tools for novel superhard materials such as diamond, cubic boron nitride and products thereof, and novel materials which cannot be prepared at normal pressure, and belongs to the technical field of ultra-high pressure. The top of the multi-stage filleted high-pressure anvil has a multi-stage platform structure with fillets; the bottom of the multi-stage filleted high-pressure anvil is a column with fillets; the transition between the top and the bottom is realized by a symmetrical curved surface or a fan-shaped bevel; and the high-pressure anvil is made of steel, hard alloy, a diamond sintered body, a cubic boron nitride sintered body or natural diamond and other high-hardness materials. The defects of structural design of corners and a first-stage platform of the conventional anvil are overcome; the stress concentration effect of the anvil can be reduced; the service life of the anvil can be prolonged; the cavity pressure of hundreds of thousands to millions of atmosphere pressures can be obtained; and the multi-stage filleted high-pressure anvil can be widely applied to an anvil device, a multi-surface ejecting high-pressure device and a multi-stage boosting device, and can meet research requirements of high-pressure physics and high-pressure biology on a matter system at high temperature and high pressure.
Owner:JILIN UNIV

Superfine particulate diamond sintered product of high purity and high hardness and method for production thereof

Disclosed is a high-purity high-hardness ultrafine-grain diamond sintered body having a grain size of 100 nm or less, which is produced by subjecting an ultrafine-grain natural diamond powder having a grading range of zero to 0.1 μm to a desilication treatment, freeze-drying the desilicated powder in solution, enclosing the freeze-dried powder in a Ta or Mo capsule without a sintering aid, and heating and pressurizing the capsule using an ultrahigh-pressure synthesizing apparatus at a temperature of 1700° C. or more and under a pressure of 8.5 GPa or more, which meet the conditions for diamond to be the thermodynamically stable. The present invention can synthesize a diamond sintered body under a lower pressure than that in a conventional method, with a diamond's original hardness and without containing any sintering aid.
Owner:JAPAN SCI & TECH CORP +1

Quick detection method and detection device of diamond luminescent spectrum

The invention discloses a quick detection method and detection device of a diamond luminescent spectrum. The method includes the following steps that the surface of a diamond sample is irradiated by lasers with the wavelength of 405 nm; after the lasers irradiate features of lattice defects on the surface of the diamond sample, a photoluminescence phenomenon is generated, and the spectrum is formed; the spectrum is received by a spectrograph through an optical fiber mechanism and transmitted to a computer display screen; peak position feature spectrum charts of the corresponding lattice defects are displayed by the computer display screen according to different features of the diamond sample; according to the peak position features of the spectrum charts, it is confirmed that diamond is natural or synthesized; when the peak positions of the spectrum position are at the 415 nm position and the 741 nm position, it can be confirmed that the diamond is natural diamond; if the peak position of the spectrum position is at the 737 nm position and no 415 nm peak position exists, it can be confirmed that the diamond is synthesized through the chemical vapor deposition method; if the peak positions of the spectrum position are on the 883 nm position and the 884 nm position, it can be confirmed that the diamond is high-temperature high-pressure synthesized diamond. The method and device have the advantages that detection is easy, operation is convenient and distinguishing is accurate.
Owner:珠宝玉石首饰国检集团深圳研究所有限公司

Method and device for batch inspection of diamonds

The invention discloses a method and device for batch inspection of diamonds. The diamonds to be inspected are placed on a working table. A Y type optical fiber comprises a light inlet, a light outlet and a lighting opening, wherein the light inlet of the Y type optical fiber is connected with a light source, the light outlet of the Y type optical fiber is connected with a spectrograph, and the lighting opening of the Y type optical fiber corresponds to the diamonds being inspected in position; a driving device is arranged between the lighting opening and the working table and can drive the lighting opening and the working table to move relatively, and the diamonds to be inspected on the working table are scanned and inspected one by one through the relative movement of the lighting opening. According to the device and method, the driving device is adopted for driving the lighting opening and the working table to move relatively, manual movement is not needed, and then inspection speed and stability are improved; a light extinction layer serves as the surface layer of the working table and can reduce background reflectance during inspection and improve inspection precision; full-spectrum analysis is adopted, so that identification precision is improved and synthetic diamonds and natural diamonds are effectively distinguished.
Owner:BIAOQI ELECTRONICS TECH

Photoluminescent diamond detection method and photoluminescent diamond detection device

The invention discloses a photoluminescent diamond detection device. The photoluminescent diamond detection device comprises a light source, a workbench, an array detector and a data processing terminal. A to-be-detected sample is placed on the workbench. The light source is monochromatic light or hybrid light with the wavelength of smaller than or equal to 410nm. The light source emits the light to the to-be-detected sample, the to-be-detected sample acquires energy and is excited to emit light, luminous light rays are emitted into the array detector to be detected, photon information of the luminous light rays is converted into an electric signal according to wavelength sequence, the electric signal is converted into a digital signal through analog-digital conversion, the digital signal is transmitted to the data processing terminal to form a real-time photoluminescent spectrogram. The photoluminescent diamond detection device has the advantages that multiple peak positions can be measured at a time by a photoluminescence method, the problems such as whether the to-be-detected sample is a diamond, a compound diamond or a natural diamond or not are solved, detection sensitivity and detection speed are high, and detection cost is low.
Owner:BIAOQI ELECTRONICS TECH

Diamond-impregnated bit with double cutting structures

The invention discloses a diamond-impregnated bit with double cutting structures, belonging to the technical field of drilling equipment for petroleum and natural gas, mine engineering, building foundation engineering construction, geology, hydrology and the like, and solving the problems in the prior art that a diamond-impregnated bit with a single cutting structure is short in service life in the complex stratum which is difficult to be drilled and thus adverse effects on geological exploration are caused. The diamond-impregnated bit comprises an API joint and a bit body connected with the API joint, wherein a center water channel, a plurality of blades and water channels between two adjacent blades are arranged on the bit body; double cutting structure impregnated A1 type teeth, impregnated A type teeth, impregnated B type teeth, impregnated C type teeth and double cutting structure impregnated A2 type teeth are arranged on the upper surfaces of the blades; large granular natural diamonds are impregnated on the cutting surfaces of the double cutting structure impregnated A1 type teeth and the double cutting structure impregnated A2 type teeth, and artificial small granular diamonds are uniformly and orderly arranged in the double cutting structure impregnated A1 type teeth and the double cutting structure impregnated A2 type teeth; and small granular diamonds are arranged in the impregnated A type teeth, the impregnated B type teeth and the impregnated C type teeth. The diamond-impregnated bit disclosed by the invention is used for drilling.
Owner:CCDC PETROLEUM CORING TECH

Manufacturing method of double-cutting diamond impregnated insert

The invention discloses a manufacturing method of a double-cutting diamond impregnated insert. Diamond particles are wrapped and embedded to the surface of an impregnated insert by a sintered layer through a thermocompression steeping sintering process. The sintered layer comprises the following components in percentage by weight: 30-55% of tungsten carbide, 10-20% of hard alloy, 5-12% of nickel, 3-12% of manganese and 17-36% of copper alloy. The thermocompression steeping sintering process comprises the following steps: putting the natural diamond particles, sintered layer powder and the impregnated inserts into a graphite die; heating at a heating speed of 80-120DEG C/min and applying a pressure of 12-18Mpa; when the temperature is increased to 900-1100DEG C, performing heat preservation for 250-350 seconds under pressure; cooling to 700-750DEG C at a cooling speed of 150-180DEG C/min under pressure; cooling to room temperature at a cooling speed of 150-180DEG C/min without pressure; tightly bonding the sequentially-arrayed impregnated inserts and the natural diamond particles together by virtue of the thermocompression steeping sintering process, so as to form an organic combination body with a double-layer cutting structure, so that the purpose of double-layer stepped cutting is realized.
Owner:CCDC PETROLEUM CORING TECH
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