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553results about How to "Use low concentration" patented technology

Environment-friendly type composite pre-film reagent used for recirculated cooling water system pre-film processing and method of use thereof

The invention belongs to the circulating cooling water treatment technical field, and refers in detail to an environment-protecting composite pretreatment filming agent used for the pre-treatment filming in a circulating cooling water system and a use method thereof. The environment-protecting composite pretreatment filming agent comprises the main components of 2-phosphonobutane- 1, 2, 4-tricarboxylic acid and sodium of polyepoxysuecinic acid as well as a proper amount of carboxylic acid copolymer, benzotriazole, sodium molybdate, zinc sulphate and so on. When used, the composite pre-treatment filming agent is added into the circulating cooling water directly, and a corrosion-resistant protecting film is formed after 48 years of operation, the corrosion resistance of which to the standard copper sulphate drip solution is far better than the traditional phosphor-zinc pretreatment filming agent. The total phosphor content of the environment-protecting composite pretreatment filming agent is less than 7.5mg / l, and the water pH value does not have to be adjusted. After the pretreatment filming, the water is clear and transparent, and the normal operation can be started without replacing the water. Thus, not only the water to be replaced is saved, but also the chemical base investment expense during the normal operation after the water replacement is reduced. Meanwhile, no waste liquor of pretreatment filming is discharged, so the invention belongs to the environment-friendly pretreatment filming method.
Owner:TONGJI UNIV

Oil-displacing agent and oil-displacing method for enhancing recovery ratio of high-temperature, high-salinity and high-hardness reservoir crude oil

ActiveCN103254883ALow critical micellar concentrationStrong ability to reduce interfacial tensionFluid removalDrilling compositionChemistryAlkylphenol
The invention relates to an oil-displacing agent and an oil-displacing method for enhancing the recovery ratio of high-temperature, high-salinity and high-hardness reservoir crude oil. The oil-displacing agent is composed of the following components in percentage by mass: A, 0.05-0.07% of an amine oxide type amphoteric surfactant; B, 0.15-0.20% of alkylphenol ethoxylate carboxylate; and C, the balance of water. The oil-displacing method disclosed by the invention is implemented through injecting the oil-displacing agent into a natural core subjected to oil-displacing under the conditions that the oil reservoir temperature is 100-120 DEG C, the total salinity of formation water is (10-15)*10<4> mg / L, and the amount of calcium-magnesium divalent metal ions is 7000-10000 mg / L, so that residual oil is in contact with the oil-displacing agent, and then the residual oil is fully displaced. The oil-displacing agent provided by the invention reaches the magnitude order of 10<-3> mN / m under the condition of high-temperature, high-salinity and high-hardness salt reservoirs, and the interfacial tension still can be maintained in an ultra-low interfacial tension state after the oil-displacing agent is aged for a long time under the condition of oil reservoirs, therefore, the oil-displacing agent is applied to the tertiary oil recovery production of oil fields.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Nano-molybdenum sulfide antibacterial material and synthetic method thereof and application thereof

The invention discloses a nano-molybdenum sulfide antibacterial material and a synthetic method thereof and application thereof. The synthetic method comprises the following steps: (1) dissolving polyethylene glycol solid in water, performing ultrasonic processing in an ultrasonic pool until the polyethylene glycol is dissolved completely, adding ammonium heptamolybdate solid, and performing ultrasonic processing until the ammonium heptamolybdate is dissolved completely to obtain a mixed solution; and (2) dissolving thiourea solid in water, dissolving the thiourea with stirring, adding the dissolved thiourea into the mixed solution, stirring the mixture, putting the mixture into a hydrothermal reactor having a polytetrafluoroethylene inner container, sealing the reactor, and performing heating reaction to obtain a black precipitate which is the nano-molybdenum sulfide antibacterial material. The invention also provides the nano-molybdenum sulfide antibacterial material which is prepared by the synthetic method. The invention also provides application of the nano-molybdenum sulfide antibacterial material on synergistic anti-microbial combining biomimetic catalysis hydrogen peroxide and near-infrared optothermal. The nano-molybdenum sulfide antibacterial material prepared by the synthetic method in the invention has high yield, and can be captured easily by bacteria. Moreover, the antibacterial effect of the material is obviously better than that of single biomimetic catalysis anti-microbial or single near-infrared optothermal anti-microbial.
Owner:INST OF HIGH ENERGY PHYSICS CHINESE ACADEMY OF SCI

Compound guanidine disinfectant and preparation method of compound guanidine disinfectant

InactiveCN105055642ATurn up charge densityStrong adsorption and killing effectAntibacterial agentsOrganic active ingredientsDisinfectantChemistry
The invention provides a compound guanidine disinfectant, which comprises the following ingredients in percentage by weight: 0.5 to 4.0 percent of guanidine disinfectants, 0.05 to 0.2 percent of low-molecular-weight chitosan, 0.5 to 2.5 percent of high-molecular-weight chitosan, 0.1 to 0.5 percent of Chinese herbal medicine extracts, 0.1 to 1.0 percent of surfactants, 0.1 to 1.0 percent of penetrants, 0.1 to 0.5 percent of skin protectants, 0.1 to 0.5 percent of macromolecule film forming agents and the balance water; and the pH value of the compound guanidine disinfectant is regulated to 7.0 to 7.5 by pH regulating agents. Through the proportional combination of all the ingredients of the compound guanidine disinfectant, a good synergistic effect is achieved; and good sterilization and antibiosis capability is realized on bacterial reproductive bodies, fungi and partial viruses. The invention also provides a preparation method of the compound guanidine disinfectant. The compound disinfectant has the advantages that the preparation process is simple; the operation is convenient; the production cost is low; the scale production is convenient; meanwhile, the property of the disinfectant is stable; and the compound disinfectant is safe and nontoxic and can be easily stored.
Owner:SHANGHAI YUKING NEW MATERIAL TECH

Low-dosage guar multinuclear cross-linking agent

The invention relates to a low-dosage guar multinuclear cross-linking agent for the field of petrochemical engineering, the low-dosage guar multinuclear cross-linking agent is prepared from water, polyhydric alcohol, polyol, carbohydrate, boron compound and inorganic acid salt. The preparation method of the cross-linking agent comprises the following steps: putting water, polyhydric alcohol and polyol in a reactor to heat to 60 DEG.C, reacting for 90-120min, and then adding a boron compound, carbohydrate and the inorganic acid salt, warming to 80-90 DEG.C, reacting for 3-6 hours, regulating pH to 8-10 by using sodium hydroxide, reacting for 1-3 hours to obtain the low-dosage guar multinuclear cross-linking agent. The low-dosage guar multinuclear cross-linking agent is capable of providing a plurality of cross-linking centers, the use concentration of the guar can be greatly reduced, the concentration of the guar is reduced to more than 30% of conventional system dosage, the dosage of the cross-linking agent is less, and the cross-linking is delayed, the damage of the guar system fracturing fluid to the stratum is obviously reduced, and the use performance of the fracture fluid is guaranteed.
Owner:SHAANXI RES DESIGN INST OF PETROLEUM CHEM IND

Coagulation-reducing viscosity-reducing agent for high-coagulation thickened oil

The invention relates to a coagulation-reducing viscosity-reducing agent for high-coagulation thickened oil. By weight percentage, the coagulation-reducing viscosity-reducing agent for the high-coagulation thickened oil comprises the following materials: 0.1% to 0.2% of anion polyacrylamide, 5% to 10% of sodium acrylate-setanol acrylate copolymer, 5% to 15% of sodium dodecyl benzene sulfonate, 1%to 2% of mixture of hexafluoropropylene oxide dipolymer amide sulphobetaine and hexafluoropropylene oxide dipolymer amide amine oxide, 1% to 2% of sodium hydroxide and the balance water. The coagulation-reducing viscosity-reducing agent can disperse high-coagulation thickened crude oil, reduces the freezing point of the crude oil to above 0 DEG C and enables the viscosity of the crude oil to be smaller than 300mPa*s at the normal temperature. The using concentration of the coagulation-reducing viscosity-reducing agent can be controlled at 0.1% to 0.5%, is lower by one magnitude order than that (3% to 7%) of a traditional surfactant, is not limited by hydrophile-lipophile balance values and phase inversion temperature (PIT) and can emulsify the high-coagulation thickened oil at the temperature above the freezing point of the crude oil.
Owner:PETROCHINA CO LTD

Preparation methods of antioxidant, water-retaining agent, mixture, and modified fuel cell membrane electrode

The invention discloses preparation methods of an antioxidant, a water-retaining agent, a mixture and a modified fuel cell membrane electrode. The invention discloses a preparation method of the modified fuel cell membrane electrode, which comprises the following steps: a) preparing an antioxidant, or a water-retaining agent, or a mixture with antioxidant and water-retaining functions, and preserving the mixed solution for later use; b) coating two sides of a microporous reinforced membrane with the mixed solution obtained in the step a) by using a coating device, and drying the membrane to obtain a modified perfluorosulfonic acid proton exchange membrane; c) processing the modified PEM membrane to prepare the fuel cell membrane electrode. The invention further discloses a formula and a preparation method of the antioxidant, a formula and a preparation method of the water-retaining agent, a formula and a preparation method of the mixture with antioxidant and water-retaining functions, and applications of all the products hereinabove in the fields of membrane electrodes and fuel cells. According to the invention, the chemical structure degradation phenomenon of the proton exchange membrane caused by free radicals is effectively relieved, the lasting water retention performance of the proton exchange membrane is improved, the proton conductivity is improved, and the mechanical property of the membrane electrode is improved by adopting the enhanced microporous membrane, so that the stability of the membrane electrode is enhanced, and the service life of the membrane electrode is prolonged.
Owner:SHENZHEN GENERAL HYDROGEN ENERGY TECH CORP LTD

Rhodamine B targeted lysosome pH fluorescent probe with cysteine ethyl ester structure and application of rhodamine B targeted lysosome pH fluorescent probe

The invention discloses a rhodamine B targeted lysosome pH fluorescent probe with a cysteine ethyl ester structure, wherein the rhodamine B targeted lysosome pH fluorescent probe has the structure as shown in a formula (I). Meanwhile, the invention discloses an application of the probe as a living cell lysosome pH fluorescent probe. Experiments show that the probe provided by the invention does not generate fluorescence under the neutral and alkaline conditions, the fluorescence intensity is rapidly enhanced along with the reduction of the pH value of the solution, is up to the maximum value when the pH value is about 4.0 and is enhanced by about 150 times when the pH value ranges from 7.51 to 3.53, and the probe has favorable antijamming capability and reversibility in the presence of various metal ions. An intracellular colocalization experiment and an interlysosome pH regulation experiment prove that the probe can specially mark a lysosome and sensitively monitor the small change of the interlysosome pH value. A cell survival rate experiment shows that the probe is nontoxic to cells, which indicates that the probe disclosed by the invention has an important application value in the aspects of imaging the cells and monitoring the change of the interlysosome pH value.
Owner:SHANDONG UNIV

Preparation method of depolymerized and dispersed viscosity reducer of heavy oil

InactiveCN101560380ADepolymerization, dispersion and viscosity reduction remain unchangedUse low concentrationDrilling compositionSolventBenzyl chloride
The invention discloses a preparation method of a depolymerized and dispersed viscosity reducer of heavy oil. The preparation method comprises selecting N,N-Dimethyloctadecylamine as a hydrophobic group monomer, and diethylene triamine, epoxy chloropropane and benzyl chloride as hydrophilic group monomers, and ethanol as a solvent. The preparation method sequentially comprises the following steps: (1) adding the N,N-Dimethyloctadecylamine (N,N-Dimethylhexadecylamine) and the ethanol to a reaction vessel with a stirring device, evenly mixing and keeping the mixture at constant temperature for 0.5h; (2) slowly dripping the epoxy chloropropane with a dropping funnel to the reaction vessel, heating to 70 DEG C-75 DEG C, and reacting for 1-4h to generate HDI-1; (3) dripping the epoxy chloropropane to the diethylene triamine at room temperature to generate HDI-2; (4) allowing reaction products in (3) and (2) to react to generate HDI-3; and (5) dripping the benzyl chloride with the dropping funnel to the HDI-3, evenly stirring the mixture, and reacting at increased temperature of 90-95 DEG C for 2-5h to obtain the target product HD.
Owner:RES INST OF PETROLEUM ENG SHENGLI OIL FIELD SINOPEC

Natural gas hydrate inhibitor

The invention provides a high effective synthetic inhibitor for inhibiting the formation of gas hydrate which is prepared by using polyvinylpyrrolidone, polyether amine and ethylene glycol butyl ether in combination according to a weight ratio of 1:1:1. When using, the total mass concentration of the inhibitor is 0.2-2.0%. The inhibitor of the invention is mainly used to inhibit the formation of natural gas hydrate in gas-oil pipelines and can be also used in oil-gas field exploitation systems. The inhibitor has obvious inhibition effect, low dosage and little damage to the environment so that the inhibitor has the advantage of high efficiency, economy and environmental friend.
Owner:GUANGZHOU INST OF ENERGY CONVERSION - CHINESE ACAD OF SCI
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