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123results about How to "Large average pore size" patented technology

TWT impregnated Ba-W cathode and its preparation method

The invention discloses a dip-coated barium-tungsten cathode for traveling-wave tubes and a preparation method thereof. The dip-coated barium-tungsten cathode comprises a cathode drum, a cathode spongy body positioned inside the cathode drum. The invention is characterized in that the cathode spongy body is laminated by a tungsten spongy body and a tungsten-rhenium spongy body, wherein the tungsten-rhenium spongy body is coated with a noble metal film on the surface. With the above structure and preparation method, compared with the prior art, the cathode spongy body is a two-layered cathode spongy body laminated by the tungsten spongy body and the tungsten-rhenium spongy body, to replace the single-layer alloy substrate with uniform porosity in the prior art; the consumption of the noble metal Re is reduced; the porosity of the tungsten spongy body is increased; the storage level of cathode salts is increased; and the preferable proportion of the cathode salts allows both the emission behavior and the stability of salts better. With the noble metal Re coating, the cost of target materials is reduced. The consumption of noble metal is greatly reduced while ensuring the maximal emission and long service life of alloy substrate film-coated cathodes. The storage quantity of cathode salts is increased and the service life of cathode is prolonged.
Owner:HUADONG PHOTOELECTRIC TECHN INST OF ANHUI PROVINCE

Nickel base catalyst

The present invention relates to a nickel base catalyst, wherein problems of low nickel content and low active specific surface in the prior art are mainly solved with the present invention. The technical scheme comprises that the catalyst comprises the following components, by weight: a) 20-75 parts of metal nickel, and b) 25-80 parts of a composite oxide carrier comprising 20-40 parts by weight of aluminum oxide and 5-40% by weight of silicon oxide, wherein a specific surface area of the catalyst is 150-400 m<2> / g, a pore volume is 0.3-0.8 ml / g, and an average pore size is 5-15 nm. With the technical scheme, the problems in the prior art are well solved, and the catalyst can be widely used for industrial production of hydrotreating of light oil fractions, heavy oil fractions, unsaturated greases, cracking gasoline, and especially cracking C9 and hydrocarbons with a carbon atom number of more than 9.
Owner:CHINA PETROLEUM & CHEM CORP +1

Garbage penetrating fluid efficient wastewater treating agent based on modified fly ash and preparation method

The invention discloses a garbage penetrating fluid efficient wastewater treating agent based on modified fly ash and a preparation method. The composition is prepared from, by weight, 50-60 parts of fly ash fine powder, 8-10 parts of dicarbonate, 11-17 parts of poly dimethyl diallyl ammonium chloride, 9-10 parts of cation polyacrylamide, 10-20 parts of carboxymethyl chitosan, 10-20 parts of quaternary ammonium salt of chitosan, 20-24 parts of smectite powder, 6-10 parts of biological bacterial sludges, 12-15 parts of magnetic tourmaline powder, 8-10 parts of basic aluminum chloride, 40-50 parts of loofahs and an adequate amount of ethyl alcohol, deionized water and water. According to the garbage penetrating fluid efficient wastewater treating agent based on the modified fly ash and the preparation method, pretreatment is conducted on coal ash powder through the dicarbonate, the porosity and the specific surface area of the coal ash power are increased, further compound modification is conducted on activation compound powder, the adsorption efficiency is increased, and the garbage penetrating fluid efficient wastewater treating agent based on the modified fly ash and the preparation method have the advantages that the adsorbent of the coal ash powder is high in capacity and easy to separate and recycle.
Owner:TIANJIN ZHONGKE CHEM

Preparation method for adsorption catalyst for removing indoor formaldehyde

The invention discloses a preparation method for an adsorption catalyst for removing indoor formaldehyde. The method comprises the following steps that zeolite powder is added into a thick salpeter solution for even stirring, hydrogen peroxide is added for stirring, and then filtering is performed to obtain a first material; the first material is added into a sucrose solution for even stirring and standing, sintering is performed after filtering, and smashing is performed to obtain a second material; manganese nitrate and cerium nitrate are added into water to be dissolved thoroughly to obtain a mixed solution, the second material is added into the mixed solution for even stirring, sintering is performed after standing is performed, the material is taken out, smashed and put into an ammonium chloride solution for stirring and standing, and then drying is performed to obtain the adsorption catalyst for removing indoor formaldehyde. The preparation method is simple, raw materials are easy to obtain, the obtained adsorption catalyst for removing indoor formaldehyde is high in formaldehyde adsorption capacity, the formaldehyde can be oxidized and degraded while being adsorbed, and the formaldehyde removal effect is good.
Owner:ANHUI KEPU ENVIRONMENT TECH CO LTD

Preparation method of carbon-aluminum composite material

The invention discloses a preparation method of a carbon-aluminum composite material. Cheap aluminum smelting waste residues are used as an aluminum source, wood waste is used as a carbon source, a physical activation method and a chemical activation method are combined, in the pyrolysis process, the aluminum source and the carbon source form a co-melt, and a safe and green carbon-aluminum composite material is obtained. In the forming process of the carbon-aluminum composite material, the aromatic hydrocarbon polymerization degree in the carbon-aluminum composite material is increased, the physical and chemical microstructure of the carbon-aluminum composite material is improved, the adsorption performance of the cheap carbon-aluminum composite material is improved, and energy regeneration and reduction of wood waste and harmless and recycling utilization of aluminum smelting waste residues are achieved.
Owner:CHANGZHOU UNIV

Composite geopolymer lightweight moisture-regulating material and preparation method thereof

ActiveCN109250964AHigh strengthFast moisture absorption and desorption reactionCement productionPolymer scienceDesorption
The invention relates to a composite geopolymer lightweight moisture-regulating material and a preparation method thereof, and belongs to the technical field of composite materials. The moisture-regulating material is prepared from the following components: 100 parts by mass of a cementitious material, 105-115 parts by mass of an activator, and a light aggregate having the amount accounting for 2-5 times the volume of metakaolin, wherein the cementitious material is composed of 70-90 parts by mass of metakaolin and 10-30 parts by mass of modified diatomite, and the light aggregate is polystyrene particles. The preparation method comprises the steps: firstly, stirring solid powder evenly, adding the liquid activator, fully stirring in a concrete stirrer, then adding the polystyrene particles, stirring evenly, pouring into a mould smeared with demoulding oil in advance, placing the mould on a horizontal table top, allowing to stand, curing at room temperature for 1 d, then demoulding totake out a plate-shaped finished product. The prepared moisture-regulating material has the characteristics of high efficiency moisture absorption and desorption, light weight, heat preservation and high strength, no pollution in the preparation process, low energy consumption, no needing of pressure forming and simple process.
Owner:CHINA UNIV OF GEOSCIENCES (WUHAN)

Novel hydroxide lanthanum-modified hydroxyapatite material and preparation method and application thereof

The present invention provides a novel hydroxide lanthanum-modified hydroxyapatite material and a preparation method and application thereof. The preparation method comprises the following steps of dissolving lanthanum chloride or lanthanum oxide into an acid solution, adding hydroxyapatite, and adjusting the pH (potential of hydrogen) value of the mixed solution to the alkaline property by an alkaline solution; putting the mixed solution after stirring into an ultrasonic device, and treating by ultrasonic waves for a period of time; putting onto a stirrer, and continuing to stir for a certainperiod of time; sealing, aging, filtering, and drying, so as to obtain filter slag; roasting at high temperature, so as to obtain the novel hydroxide lanthanum-modified hydroxyapatite material. The novel hydroxide lanthanum-modified hydroxyapatite material has the characteristics that the particle size is controllable, the specific surface area is large, the hole size of the particle is large, and the loading is uniform; the material is applied to remove the phosphate radicals in wastewater, the removal rate of phosphate radicals reaches 97.5% or above, and the purpose of high-efficiency andhigh-load phosphor removal is realized.
Owner:NANCHANG HANGKONG UNIVERSITY

Synthetic method of aminated mesoporous silicon dioxide for modified cyanate ester resin

InactiveCN107522902ASave material and energyEasy to prepareChemistryCyanate ester
The invention discloses a synthetic method of aminated mesoporous silicon dioxide for modified cyanate ester resin and belongs to the technical field of a basis material for a high frequency printing board. The method comprises the following steps: roasting; extracting; and preparing a POSS-MPS / CE composite material. The mesoporous silicon dioxide is synthesized by means of an extraction method. The aminated mesoporous silicon dioxide which is intact in mesoporous structure and relatively great in pore diameter is obtained by means of a method of grafting amino first and then dissolving a template agent. The template agent plays roles of protecting and supporting the porous structure in the whole process.
Owner:NORTHWESTERN POLYTECHNICAL UNIV

Nickel base catalyst preparation method

The invention relates to a nickel base catalyst preparation method, wherein technical problems of low specific surface and small average pore size in the prior art are mainly solved with the present invention. The technical scheme comprises: adopting an alumina sol as a carrier precursor, and adding a nickel salt aqueous solution or a nickel-ammonia complex to the alumina sol at a temperature of 45-80 DEG C to obtain a nickel-aluminum sol; at a temperature of 45-120 DEG C, carrying out standing aging on the nickel-aluminum sol or carrying out heating decomposition on the nickel-ammonia complex to obtain a nickel-aluminum gel; and carrying out washing, drying, forming, calcination and reduction on the obtained gel to obtain the required nickel base catalyst, wherein the gel is subjected to vacuum freeze drying after being washed, a vacuum freeze drying time is 20-40 h, and a vacuum degree is 30-100 KPa. With the technical scheme, the problems are well solved, and the preparation method can be widely used for hydrogenation industrial production.
Owner:CHINA PETROLEUM & CHEM CORP +1

Preparation method of biomass derivative carbon material used for sodium-ion batteries

The invention belongs to the field of electrochemistry and energy material, and discloses a preparation method of a biomass derivative carbon material used for sodium-ion batteries. According to the preparation method, soybean is taken as a biomass source, KOH is taken as an activator, high temperature calcining is carried out so as to obtain the porous biomass derivative carbon material. Soybeanis a natural product, is abundant in sources, is high in protein content, contains a large amount of nitrogen element, and is capable of forming a natural nitrogen doped carbon material; the nitrogendoped carbon material can be used for providing Na<+> with sufficient sodium embedding vacancies, providing substantial fake capacitance in sodium-ion battery charging and discharging process, and increasing battery specific capacity; and in addition, nitrogen element doping is capable of improving material conductivity, and increasing iron transmission efficiency; KOH activation is capable of increasing porous structure specific surface area further, it is beneficial for electrolyte infiltration, and increasing of ion and electron transmission efficiency. The biomass derivative carbon material possesses the above advantages, so that when the biomass derivative carbon material is taken as a sodium ion anode material, relatively high reversible specific capacity and excellent circulation stability are achieved.
Owner:JIANGSU UNIV

High-flocculability crane electroplating wastewater disposal agent based on modified coal ash and preparation method of high-flocculability crane electroplating wastewater disposal agent

The invention discloses a high-flocculability crane electroplating wastewater disposal agent based on modified coal ash. After coal ash is modified, the modified coal ash is added into raw materials to replace partial phosphorite, so that the exploitation quantity of natural phosphorite is reduced, environmental pollution caused by coal ash accumulation is further solved effectively, and the flocculability of the product is improved; meanwhile, after mulberry branches are modified organically, the modified mulberry branches are added into the raw materials as an adhesive compatible with effective chemical adsorbents, the adhesive is good in compatibility with organic pollutants and high in adsorption rate, and finally abundant pores and high-strength cohesive bodies are formed after pelleting and high-temperature roasting fabrication processing; moreover, a compound is formed by the added adhesive and other substances in the roasting process, so that the phase change of natural phosphate rock powder occurring in different temperature intervals is suppressed, the generation of internal stress is reduced, the pulverization degree is reduced, and the prepared disposal agent is high in porosity and surface area ratio, large in adsorption efficiency and high in flocculability.
Owner:ANHU WUHU CHANGJIANG JACK UP EQUIP CO LTD
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