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151 results about "Organotitanium compound" patented technology

Organotitanium compounds in organometallic chemistry contain carbon-to-titanium chemical bonds. Organotitanium chemistry is the science of organotitanium compounds describing their physical properties, synthesis and reactions. They are reagents in organic chemistry and are involved in major industrial processes.

High performance lithium titanium spinel li4t15012 for electrode material

The invention concerns a process for producing a spinel compound of formula Li4Ti5O12, comprising a step of preparing a mixture of an organo-lithium compound selected from lithium alcoholates with an organo-titanium compound selected from titanic acid esters, in a liquid medium, and a step of hydrolyzing the mixture of said compounds. The invention also concerns a Li4Ti5O12 particulate material which may be produced according to the previous cited process and which has a BET surface area of at least 10 m<2> / g. The material is particularly useful in the manufacture of Lithium Ion batteries.
Owner:FRANCOIS SUGNAUX +1

Active carbon fiber containing nano titanium dioxide particles and its preparation method and uses

This invention relates to a method for preparing an activated carbon fiber of Titania particle having nanometer and its usage. The fiber is formed from the activated carbon fiber material loaded with the Titania particles, wherein the mass ratio of the Titania particles is 5~25%. The preparing method uses the sol-gel processing: a) hydrolyzing organic titanium compounds of the TiO2 to the TiO2 collosol, and depositing on the activated carbon fiber, b) drying the colloslo and getting the jel, c) annealing, and transforming to nanometer TiO2 particles compounded in the surface of the fiber, then getting the fiber. The fiber not only maintains the poriness but also enhances the optical catalytic activity of the Titania particle, and can be used for removing the volatile organic contaminant with low concentration, wherein its absorbance can reach to 500mg / g and its optical catalytic dissolution rate can reach to 36%.
Owner:SUN YAT SEN UNIV

Preparation method of carbon-coated sodium-micron-scale lithium titanate composite anode material

The invention relates to a preparation method of a carbon-coated sodium-micron-scale lithium titanate composite anode material. The method comprises steps as follows: lithium salt is dissolved in an aqueous solution of absolute ethyl alcohol, and the solution is marked a solution a; an organic titanium compound and a carbon source are dissolved in absolute ethyl alcohol, and the solution is marked a solution b; a chelating agent M is dissolved in absolute ethyl alcohol, ultrasonic dispersion is performed, and the solution is marked a solution c; the solution c is slowly dropwise added to the solution b while stirring, and white sol is obtained; then the solution a is slowly dropwise added to the white sol; after the sol is aged, heating, stirring, drying, grinding, sieving and calcination are performed, and the carbon-coated lithium titanate composite anode material is obtained. Lithium titanate has narrower particle size distribution and more uniform particle distribution, and sodium-micron-scale particles are uniformly inlaid to form particles with high tap density; the particle structure is loose and porous, the specific surface area of a formed electrode is larger, getting off of lithium ions in the lithium titanate material is facilitated, and the stability of the crystal structure of the lithium ions in the charge and discharge process is guaranteed.
Owner:SHANDONG YUHUANG NEW ENERGY TECH

Undercoating layer material for lithography and wiring forming method using the same

An undercoating layer material for lithography, containing polysiloxane and an organotitanium compound having no alkoxy group; and a method for forming a wiring including a step of applying the undercoating layer material onto a substrate and curing to form an undercoating layer and forming a photoresist layer thereon; a step of removing by dry etching the exposed portion of the undercoating layer which is not covered with the photoresist pattern; a step of forming a predetermined wiring pattern using the photoresist pattern and the patterned undercoating layer as masks; and a step of removing the undercoating layer and photoresist pattern remaining on the substrate. The undercoating layer material is advantageous that the storage stability, the form of the lower portion of the resist pattern, and the burying properties are excellent and no voids are found.
Owner:TOKYO OHKA KOGYO CO LTD

Preparation method of catalyst component for ethylene polymerization or copolymerization and catalyst thereof

The invention relates to a preparation method of a catalyst component for ethylene polymerization or copolymerization and a catalyst thereof. The method comprises the following steps: (1) at a temperature of 50-90DEG, dissolving magnesium halide in a solvent system containing an organic epoxy compound and an organic phosphorus compound to form a uniform solution; adding an organic alcohol compound during or after the solution formation and leaving them to react for certain time so as to obtain a reaction solution; (2) in the presence of an organic titanium compound and at a temperature of -30DEG C-0DEG C, subjecting the solution and a titanium compound to a contact reaction, or adding the organic titanium compound after the contact reaction of the solution obtained in step (1) and the titanium compound, and raising the temperature of the mixture slowly to 50-120DEG C, leaving solids to precipitate gradually and form particles, after certain period of reaction, removing the unreacted material and the solvent, and conducting washing with an inert diluent so as to obtain a solid component; and (3) suspending the solid component in certain amount of the inert diluent, performing a contact reaction with an organic aluminium compound under a temperature of 0DEG C-50DEG C, and after certain reaction time, removing the inert diluent, thus obtaining the catalyst component. The catalyst provided in the invention has high catalytic activity and good hydrogen response.
Owner:CHINA PETROLEUM & CHEM CORP +1

Preparation method of PBS (poly butylenes succinate)

The invention relates to a preparation method of PBS (poly butylenes succinate). The preparation method comprises the following steps: adopting succinic acid and butanediol with the molar ratio of (1.2-2.2): 1 as the raw materials; carrying out negative pressure esterification reaction for about 3.5 hours at the pressure of 40-80 kPaA and the temperature of 135-160 DEG C; afterwards, carrying out polycondensation reaction for about 2.5 hours at the pressure of 2-4 kPaA and the temperature of 170-210 DEG C to prepare the PBS with high molecular weight, wherein the whole reaction is carried out under the condition of catalyst existence; the catalyst is a titanium-phosphorus coordination composite catalyst generated through carrying out coordination reaction on raw materials, namely, organic phosphorus compounds and organic titanium compounds; the molar ratio of the catalyst dosage to the succinic acid dosage is 0.03%-3%. According to the PBS with high molecular weight prepared through the preparation method, the number-average molecular weight is 100 thousand or above, the tensile strength is 36 MPa or above, and the elongation at rupture is 250% or above.
Owner:BC P INC CHINA NAT PETROLEUM CORP +1

Micro/nano-scale sheet type titanium polyester catalyst and application thereof

The invention belongs to the technical field of titanium polyester catalysts and in particular relates to a micro / nano-scale sheet type titanium polyester catalyst and the application thereof. The micro / nano-scale sheet type titanium polyester catalyst provided by the invention comprises an organic titanium compound and a dispersing medium, wherein the structural formula of the organic titanium compound is Tix(OR1O)y(OOCC6H4COO)zH4. The invention further provides the titanium polyester catalyst for esterification reaction, transesterification and / or polycondensation reaction in catalytic polyester synthesis. Compared with the traditional polyester catalyst antimony acetate, the titanium polyester catalyst provided by the invention has the advantage that the reaction speed in the polycondensation stage is increased by more than 60%; compared with the titanium or titanium composite polyester catalyst, the titanium polyester catalyst provided by the invention has the advantage of good compatibility with the polyester; the micro / nano-scale sheet type titanium polyester catalyst provided by the invention has the advantages of low agglomeration, hydrolysis resistance, high temperature resistance and the like and is an efficient and stable polyester catalyst with low toxicity.
Owner:上海慧翌新材料科技有限公司

Biodegradable polyester composite catalyst, as well as preparation method and using method thereof

The invention relates to the technical field of catalysts for biodegradable polyester and discloses a biodegradable polyester composite catalyst, as well as a preparation method and a using method thereof. The biodegradable polyester composite catalyst comprises the following raw materials in parts by weight: 50-98 parts of organic titanium compound, 1-30 parts of organic silicon compound and 0-10 parts of cocatalyst, and the biodegradable polyester composite catalyst is obtained through the following method: firstly stirring and uniformly mixing the organic titanium compound in the required quantity with the organic silicon compound in the required quantity, and then continuously stirring and uniformly mixing the cocatalyst in the required quality with the organic titanium compound in the required quantity and the organic silicon compound in the required quantity to get the biodegradable polyester composite catalyst. The biodegradable polyester composite catalyst disclosed by the invention has the characteristics of simple preparation process, simplicity and convenience in operation, lower preparation cost and easiness in industrial production, and by adopting the biodegradable polyester composite catalyst obtained in the invention, the reaction time is shortened, and the polyester with good color phase and high molecular weight can be prepared.
Owner:XINJIANG BLUE RIDGE TUNHE CHEM IND JOINTSTOCK +1

Surface-treated zinc oxide powder, anti-bacterial agent, and anti-bacterial composition

Provided is a zinc oxide powder having an average particle diameter of 1.1 mum or more and having an anti-bacterial activity; an anti-bacterial agent comprising the zinc oxide powder; and an anti-bacterial composition containing the anti-bacterial agent. A surface-treated zinc oxide powder which has an average particle diameter of 1.1 mum or more and of which the surface is treated with at least one compound selected from silicon oxide, a silicone oil, an organosilicon compound and an organotitanium compound.
Owner:SAKAI CHEM IND CO LTD
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