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40results about How to "Increase chlorine content" patented technology

Method for treating hazardous wastes through cooperation of metallurgical furnace

The invention discloses a method for treating hazardous wastes through the cooperation of a metallurgical furnace. The method comprises the steps of sintering for agglomerating the hazardous wastes containing heavy metal, or condensing for agglomeratingthe hazardous wastes containing the heavy metal, and smelting the combustible hazardous wastes to form a finished product block so as to obtain analloy crude product containing the heavy metal. According to the method for treating the hazardous wastes through the cooperation of the metallurgical furnace provided by the invention, the hazardouswastes containing the heavy metal are treated through a melting furnace, valuable metal in the hazardous wastes containing the heavy metal is recycled, meanwhile, organic matters inthe combustible hazardous wastes are decomposed by high temperature of the melting furnace, and heat values in the organic matters are utilized, so that inthe smelting process of the hazardous wastes containing the heavy metal, the harmful element of the combustible hazardous wastes, and fly ash used as a first slag former or furnace slags produced by residue incineration is reduced to be below 0.1 percent, the wastes can be directly used as building materials and used for preparing rock wool and the like, and the metal recovery rate reaches to more than 90 percent.
Owner:唐山市丰润区明营再生资源有限公司

Fluid purification media and systems and methods of using same

A fluid purification system capable of removing lead from significant volumes of fluids also containing at least one of TOC and TTHM under low pressure conditions and at reasonable flow rates is provided. The system comprises a first fluid purification media comprising a rigid porous purification block. The rigid purification block includes a longitudinal first surface; a longitudinal second surface disposed inside the longitudinal first surface; and a porous high density polymer disposed between the longitudinal first surface and the longitudinal second surface. The system further includes a second fluid purification media, comprising a fibrous, nonwoven fabric disposed adjacent to the first surface of the first fluid purification media, the second surface of the first purification media, or both.
Owner:KINETICO

Ultrafiltration membrane for wastewater treatment and preparation method thereof

The invention discloses an ultrafiltration membrane for wastewater treatment and a preparation method of the ultrafiltration membrane. The ultrafiltration membrane is prepared from the following components: chlorinated polyvinyl chloride, modified polyacrylonitrile, polyethylene glycol, polyoxyethylene fatty alcohol ether and dimethylformamide. The ultrafiltration membrane is subjected to hydrophilic modification, so that the infiltration rate of the ultrafiltration membrane is high, the water flux of the ultrafiltration membrane is increased, and the rejection rate of the ultrafiltration membrane is increased; after the polyvinyl chloride is subjected to chlorination modification, the chlorine content of the material is improved, so that the molecular bond polarity of the material is increased, the intermolecular force is enhanced, the chemical stability is improved, and the mechanical property, the chemical corrosion resistance and the heat resistance of the material are greatly improved; polyacrylonitrile is modified, so that precious metal ions and rare metal ions have high adsorption capacity; and the ultrafiltration membrane is good in wastewater treatment effect, good in physical property and mechanical property and not prone to loss, and the wastewater treatment cost is reduced.
Owner:广德华东电子电路发展有限公司

Novel high effective noble metal adsorbent and its preparing method

The present invention relates to the design and synthesis method of adsorbing resin, and by means of special polymerization method, small crosslinked polystyrene ball is made to possess proper geometric features and maximized function. By means of proper design, the synthesis steps are reduced, and functional radical contains special reactive functional groups capable of adsorbing noble metal. One functional molecule contains four adsorbing groups. The obtained adsorbent has excellent noble metal adsorbing performance and selectivity under different pH conditions, and may be used in the adsorption and recovery of noble metal in different fields.
Owner:SUZHOU UNIV

Method for preparing oxygen-enriched super-crosslinked resin based on Friedel-Crafts alkylation reaction and application of oxygen-enriched super-crosslinked resin

The invention relates to a method for preparing oxygen-enriched super-crosslinked resin based on a Friedel-Crafts alkylation reaction and application of the oxygen-enriched super-crosslinked resin, and the method for preparing the oxygen-enriched super-crosslinked resin based on the Friedel-Crafts alkylation reaction comprises the following steps: (1) swelling chloromethylated crosslinked polystyrene; (2) preparing oxygen-enriched precursor resin, namely carrying out a Friedel-Crafts reaction on the chloromethylated crosslinked polystyrene treated in the step (1) and oxygen-containing small molecules at 40-50 DEG C under the catalysis of a Lewis acid for a preset time; and (3) preparing the oxygen-enriched super-crosslinked resin, namely carrying out a Friedel-Crafts reaction on the oxygen-enriched precursor resin prepared in the step (2) and rigid small molecules at 80-90 DEG C for a preset time, and weaving the oxygen-enriched precursor resin skeleton. The oxygen-enriched super-crosslinked resin is easy to elute after adsorption, can be repeatedly used, has a good repeated use effect, can be widely applied to the fields of chemical analysis, drug separation and purification, environmental pollution treatment and the like, and has a great development prospect.
Owner:CENT SOUTH UNIV

A method for separating and purifying desulfurized gypsum and a device for realizing the method

The invention provides a separation and purification method of desulfurized gypsum and the implementation thereof to upgrade the quality of the desulfurized gypsum. The method is to add alcoholic foaming agent and hydrophobic collector into the desulfurized gypsum slurry in the stirring condition. The equipment for the implementation comprises the collector injection unit and the foaming agent injection unit. The outlet of the collector injection unit is connected to the desulfurized slurry pond; the outlet of the foaming agent injection unit is connected to the oxidized air transmission pipe. The invention applies the principle of dissolved air floating, combines the black gel debris and hydrophobic collector, and combines the hydrophobic base of the foam generated by the foaming agent and the hydrophobic base on the surface of the black gel debris, wherein the bubble takes the black debris to the liquid top layer to make the black debris detached from the desulfurized gypsum slurry. The removal rate of the black gel debris is higher than 90%, which guarantees the dehydration effects of the desulfurized gypsum slurry and enhances the purity and whiteness of the desulfurized gypsum and improves the quality of the desulfurized gypsum.
Owner:CHINESE RES ACAD OF ENVIRONMENTAL SCI

Preparation method of cresyl diphenyl phosphate

The invention relates to a preparation method of cresyl diphenyl phosphate. The method includes the steps of: 1) esterification reaction: mixing phosphorus oxychloride with a catalyst, then adding phenol dropwise, and at the end of the reaction, conducting reduced pressure distillation to obtain diphenoxy phosphoryl chloride; 2) reduced pressure reaction: reacting the intermediate diphenoxy phosphoryl chloride obtain in step 1) with m, p-cresol under a reduced pressure, and removing the reacted hydrogen chloride gas to obtain a cresyl diphenyl phosphate crude product; and 3) refining: carryingout alkali washing, washing and reduced pressure distillation on the cresyl diphenyl phosphate crude product obtained in step 2) to obtain cresyl diphenyl phosphate. Phosphorus oxychloride and phenolare employed for reaction to prepare the diphenoxy phosphoryl chloride intermediate, the generated intermediate reacts with m, p-cresol to prepare the product, the synthetic route reduces the impurities phenyl xylylphosphate, tricresyl phosphate and triphenyl phosphate, thus improving the purity.
Owner:ZHEJIANG WANSHENG

Preparation method of setting paraffin for polyurethane foam caulk

The invention discloses a method for producing shaping paraffin serving as polyurethane foam crack filler.The method comprises the following steps of adding heavy liquid wax and light liquid wax into a reaction kettle, and stirring the materials to be uniform, so that reaction materials are obtained; introducing chlorine into the reaction kettle, and controlling the reaction temperature; after the reaction materials react with the chlorine for a while, detecting the density and viscosity of chlorinated paraffin, and then blowing off hydrogen chloride gas; then detecting the acid value, and then adding compound heat stabilizer, so that the shaping paraffin is obtained.The method has the advantages that the produced shaping paraffin is high in chlorine content, as a result of increase of the chlorine content, the viscosity of the polyurethane foam crack filler can be increased accordingly, and thereby the phenomena that when the polyurethane foam crack filler is used under the condition of low temperature and low humidity, the completely dry speed is low, obtained foam is low in viscosity and thus cannot support a framework of the foaming volume, obtained foam is made to flow out and cannot expand in a space where gluing is predicted to be conducted are avoided.
Owner:SHIJIAZHUANG DONGXIANG CHEM CO LTD

Vinyl chloride copolymer emulsion for water-based anticorrosion coating and its preparation method and application

The invention discloses a vinyl chloride copolymer emulsion for water-based anticorrosion coatings and a preparation method thereof, comprising the steps of: adding deionized water, vinyl chloride, allyl chloride, isobutyl vinyl ether, maleic anhydride, Emulsifier and reducing agent, stir and heat up to 45-60°C, then continuously drop ammonium persulfate initiator aqueous solution to start polymerization, continuously add vinyl chloride during polymerization, control the speed of vinyl chloride addition, and maintain the pressure of the polymerization system ± 0.1 kg / cm 2 , continue to polymerize until the pressure of the system drops by 0.5-2.0kg / cm after adding vinyl chloride 2 When the temperature is lowered, the polymerization is terminated, unreacted monomers are removed, and a vinyl chloride copolymer emulsion is obtained. The present invention increases the chlorine content of the copolymer by introducing the addition amount of propylene chloride monomer and isobutyl vinyl ether, and at the same time introduces maleic anhydride, the caking monomer, so that the obtained vinyl chloride copolymer can be used to prepare the vinyl chloride copolymer with good anticorrosion effect and Adhesive water-based paint.
Owner:JIANGSU LISIDE NEW MATERIAL

A modified tri-block copolymer electrolyte membrane and its preparation method

The invention provides a modified triblock copolymer electrolyte membrane and a preparation method thereof, belonging to the technical field of electrolyte. The modified triblock copolymer electrolyte membrane has a structure as shown in the specification, wherein in the formula, m, n and p are respectively integers from 50 to 3000, x is more than zero and smaller than or equal to m, and y is more than zero and smaller than or equal to n; T is monovalent anion. The preparation method comprises the following steps: adding modified triblock copolymer SEBS and excess trimethylamine and dimethylformamide into a reactor, wherein the solid content is 5-20wt%; stirring for reaction for 24 hours at 40 DEG C, then coating reaction liquid to a clean horizontal glass board to form a membrane naturally, evaporating the solvent at the temperature of 60 DEG C, and stripping the membrane, thus obtaining the modified triblock copolymer electrolyte membrane. According to the invention, the conventional route of chloromethylation is abandoned, and a chloroacetyl modification method is adopted, so that the membrane is relatively environmental-friendly and safe, and an ion exchange membrane with higher chlorine content, namely, higher ion exchange capacity, and excellent conductivity can be obtained.
Owner:NANYANG NORMAL UNIV
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