452 results about "Solid film" patented technology

Methods and devices are provided for forming an absorber layer. In one embodiment, a method is provided comprising of depositing a solution on a substrate to form a precursor layer. The solution comprises of at least one polar solvent, at least one binder, and at least one Group IB and / or IIIA hydroxide. The precursor layer is processed in one or more steps to form a photovoltaic absorber layer. In one embodiment, the absorber layer may be created by processing the precursor layer into a solid film and then thermally reacting the solid film in an atmosphere containing at least an element of Group VIA of the Periodic Table to form the photovoltaic absorber layer. Optionally, the absorber layer may be processed by thermal reaction of the precursor layer in an atmosphere containing at least an element of Group VIA of the Periodic Table to form the photovoltaic absorber layer.

A specific embodiment of the present invention is a process for continuously producing a porous solid film of spacer-modified nano graphene platelets for supercapacitor electrode applications. This process comprises: (a) dissolving a precursor material in a solvent to form a precursor solution and dispersing multiple nano graphene platelets into the solution to form a suspension; (b) continuously delivering and forming the suspension into a layer of solid film composed of precursor material-coated graphene platelets overlapping one another, and removing the solvent from the solid film (e.g., analogous to a paper-making, mat-making, or web-making procedure); (c) continuously converting the precursor material into nodules bonded to surfaces of graphene platelets to form a porous solid film composed of spacer-modified graphene platelets; and (d) continuously collecting the porous solid film on a collector (e.g., a winding roller). The roll of porous solid film (mat, paper, or web) can then be cut into pieces for used as supercapacitor electrodes.

Consistent with the present invention, tissue adhesive compositions and an associated laser exposure system are provided for bonding or sealing biological tissues. The compositions are comprised of chemically derivatized soluble collagen which is formulated to concentrations ranging from 300 mg / ml (30%) to 800 mg / ml (80%) collagen protein. In particular, Type I collagen, for example, is first prepared by extraction from bovine or porcine hide and purified. The collagen preparations are then chemically derivatized with sulfhydryl reagents to improve cohesive strength and with secondary derivatizing agents, such as carboxyl groups, to improve the adhesive strength of the solder to the tissue. The compositions are then formed into viscous solutions, gels or solid films, which when exposed to energy generated from an infrared laser, for example, undergo thermally induced phase transitions. Solid or semi-solid protein compositions become less viscous enabling the high concentration protein to penetrate the interstices of treated biological tissue or to fill voids in tissue. As thermal energy is released into the surrounding environment, the protein compositions again become solid or semi-solid, adhering to the treated tissue or tissue space.

The present invention relates to electrochromic polymeric solid films, manufacturing electrochromic devices using such solid films and processes for making such solid films and devices. The electrochromic polymeric solid films of the present invention exhibit beneficial properties and characteristics, especially when compared to known electrochromic media. The electrochromic polymeric solid films are transformed in situ from a low viscosity electrochromic monomer composition by exposure to electromagnetic radiation, and in so doing minimum shrinkage occurs. The electrochromic polymeric solid films of the present invention also perform well under prolonged coloration, outdoor weathering and all-climate exposure, and provide an inherent safety aspect not known to electrochromic media heretofore.

A fingerprint input device capable of obtaining a fingerprint image presenting sufficient contrast is provided. The fingerprint input device includes: a two-dimensional image sensor for picking up a fingerprint image from a fingerprint measured portion of a measurement target finger; and a transparent solid film mounted on an image pickup surface of the two-dimensional image sensor, the fingerprint measured portion being mounted on the transparent solid film when the two-dimensional image sensor picks up the fingerprint image, wherein the fingerprint input device picks up an image of a fingerprint ridgeline portion in the fingerprint measured portion as a light portion, and picks up an image of a fingerprint valley portion in the fingerprint measured portion as a dark portion through an air layer, and a refractive index of the transparent solid film satisfies that contrast of the image is more than a given value.

Methods and devices are provided for forming an absorber layer. In one embodiment, a method is provided comprising of depositing a solution on a substrate to form a precursor layer. The solution comprises of at least one equilibrium and / or near equilibrium material. The precursor layer is processed in one or more steps to form a photovoltaic absorber layer. In one embodiment, the absorber layer may be created by processing the precursor layer into a solid film and then thermally reacting the solid film in an atmosphere containing at least an element of Group VIA of the Periodic Table to form the photovoltaic absorber layer. Optionally, the absorber layer may be processed by thermal reaction of the precursor layer in an atmosphere containing at least an element of Group VIA of the Periodic Table to form the photovoltaic absorber layer.

A method of depositing a solid film on a substrate in which a stream comprising particles suspended in a transport gas is moved through a heating zone. The particles are combined with the transport gas from a powder feeder operatively coupled to a gas flow tube. The particle stream is directed toward the heating zone by ejecting the powder stream from a nozzle connected to a distal end of the gas flow tube. A radiation source is directed at the suspended particles as they move through the heating zone so that the particles heated to a molten state. The droplets are undercooled in a cooling zone before impact with the substrate.

Atomic layer deposition is used to provide a solid film on a plurality of disc shaped substrates. The substrates are entered spaced apart in a boat, in a furnace and heated to deposition temperature. In the furnace the substrate is exposed to alternating and sequential pulses of at least two mutually reactive reactants, in such way that the deposition temperature is high enough to prevent condensation of the at least two reactants on the surface but not high enough to result in significant thermal decomposition of each of the at least two reactants individually.

The invention discloses a nitrogen-doped carbon nanometer particle as well as a preparation method and application thereof, belongs to the field of nanometer material science and is used for solving the technical problems that fluorescence quenching is easily caused to the aggregative state of the carbon nanometer particle due to surface passivation modifier which is added for the preparation of existing carbon nanometer particles. The nitrogen-doped carbon nanometer particle is prepared through a microwave method by using organic compounds containing polycarboxyl or polyhydroxy as materials and using ammonia water as a solvent and a nitrogen doping source. The invention further provides the application of the nitrogen-doped carbon nanometer particle as fluorescent ink and fluorescent glue. The preparation method disclosed by the invention is simple, low in cost, and convenient to realize large-scale production; the maximal fluorescent quantum efficiency of the solid film formed by the prepared fluorescent glue is as high as 84%; the prepared fluorescent ink is non-toxic, generates no precipitates after being placed for a long time, is strong in fluorescence characteristic and can be applied to various fields such as bio-imaging, biological product identification, information storage, information encryption, counterfeiting prevention, illumination and display, sensing and photovoltaic devices.

There are disclosed an organic electroluminescent (EL) device composition that includes a compound (A) having a perylene ring and a compound (B) having a diketopyrrolopyrrole skeleton, and an organic EL device that includes a pair of electrodes consisting of an anode and a cathode, and one or more organic layers including a light-emitting layer formed between the electrodes, at least one of the organic layers being a layer formed from the organic EL device composition. Furthermore, there are disclosed an organic EL device composition that includes a compound (C) having, as a solid film, a fluorescence spectrum peak wavelength of 550 nm or longer, and a compound (D) having, as a solid film in which Compound (D) is contained at 5 wt % in Compound (C), an area at a wavelength of 600 nm or shorter in a fluorescence spectrum region of 500 to 800 nm of 20% or less of the entire area, and an organic EL device including a light-emitting layer formed from this composition.

The invention discloses a novel perfluoropolyether alkoxy silane compound and a synthesis method thereof. The structure of the compound is shown as formula (1). The synthesis method includes: reacting hydroxyl terminated perfluoropolyether (PFPE), 3-(2-aminoethyl)aminopropyltrimethoxysilane, 3-(2, 3-epoxypropoxy)propyltrimethoxysilane (KH560), and an HDI trimer in a molar ratio of 1:2:2:1, during reaction, employing a certain amount of a solvent to dilute the mixed hydroxyl terminated perfluoropolyether and 3-(2-aminoethyl)aminopropyltrimethoxysilane, then adding the HDI trimer dropwise, carrying out reaction for 6h at certain temperature, then adding KH560 dropwise, and carrying out reaction for 6h again at certain temperature then reducing pressure and removing the solvent, thus obtaining the perfluoropolyether alkoxy silane compound. The compound can be coated on glass, plastic, film, and other substrate surfaces, and after crosslinking and curing, a layer of solid film can be formed, and the substrate is endowed with excellent anti-fingerprint and antifouling performance and abrasion resistance.

This invention discloses a novel multicomponent system or a single compound that is capable of performing triplet-triplet annihilation up conversion process. (TTA-UC) A solution or solid film that comprises this TTA-UC system or compound is provided. This system or compound can be used in an optical or optoelectronic device.

The invention discloses a method for extracting tungsten from scheelite, comprising the following steps of: mixing the scheelite with a mixed solution of phosphoric acid and sulfuric acid for reaction, adding dihydrate gypsum as seed crystals, and controlling the concentration of SO4<2->, the content of P2O5 and the reaction temperature to obtain the dihydrate gypsum with good filtering and washing properties. The invention has the advantages that one-step efficient normal pressure leaching of the scheelite is achieved, thus resources and energy consumption are saved, and the resolution ratio of the scheelite is up to above 98%; the problems of Cl<-> corrosion and serious HCl volatilization are overcome; the cyclic utilization of phosphoric acid is basically achieved, and the leaching cost and waste water discharge are greatly reduced; leaching equipment is simple, is convenient for operation and is easy to realize industrialization; the single and stable dihydrate gypsum is obtained, the filter efficiency of the dihydrate gypsum is high, the washing property of the dihydrate gypsum is good, and the P2O5 content in the washed dihydrate gypsum is reduced to be below 2%, thereby reducing the loss of phosphoric acid; and the passivation phenomenon of calcium sulfate solid film when the tungsten ore is leached is avoided.

The invention discloses a solar energy sea water desalinization device based on reflection and total reflection, and belongs to the technical field of solar energy heat collection and water treatment. The device is composed of an upper surface transparent film, a total reflection solid film with a gradually-varied wall thickness and hydrophilic capillary tubes; the plurality of devices can be arranged and combined to form multiple solar energy sea water desalinization films; the combined devices are floated on the sea surface for use. According to the invention, a capillary phenomenon is utilized to enable sea water to go up to the upper ends of the capillary tubes, sunlight enters through the upper surface layer transparent film, and is subjected to reflection or total reflection when being in contact with an inner surface, and finally the sunlight is gathered on the black hydrophilic fiber capillary tubes to generate heat energy to realize sea water evaporation. The convection and heat exchange of the raised water vapor and external air is realized through the upper surface layer transparent film, the water vapor is condensed to generate fresh water on the inner side of the transparent film, the fresh water slips through the inner wall of a reflecting surface, and flows into the lower part of a housing through water outlet holes in the wall of a supporting cylinder to be stored. The fresh water is conveyed to users after accumulation, and meanwhile, small-sized plant can be planted at sea.

Consistent with the present invention, tissue adhesive compositions and an associated laser exposure system are provided for bonding or sealing biological tissues. The compositions are comprised of chemically derivatized soluble collagen which is formulated to concentrations ranging from 300 mg / ml (30%) to 800 mg / ml (80%) collagen protein. In particular, Type I collagen, for example, is first prepared by extraction from bovine or porcine hide and purified. The collagen preparations are then chemically derivatized with sulfhydryl reagents to improve cohesive strength and with secondary derivatizing agents, such as carboxyl groups, to improve the adhesive strength of the solder to the tissue. The compositions are then formed into viscous solutions, gels or solid films, which when exposed to energy generated from an infrared laser, for example, undergo thermally induced phase transitions. Solid or semi-solid protein compositions become less viscous enabling the high concentration protein to penetrate the interstices of treated biological tissue or to fill voids in tissue. As thermal energy is released into the surrounding environment, the protein compositions again become solid or semi-solid, adhering to the treated tissue or tissue space.

A method of making an anti-reflective film comprises preparing a liquid composition with specific amounts of tetraethyl orthosilicate, polyethylene glycol, HCl, ethanol and at least one alcohol having a higher boiling point than ethanol and miscibility with both ethanol and water; applying the liquid composition onto a surface of a substrate to form a liquid film; evaporating the ethanol and the at least one alcohol from the liquid film to form a solid film; and heating the solid film to form a silica film.

An apparatus for depositing a solid film onto a substrate from a reagent solution includes reservoirs of reagent solutions maintained at a sufficiently low temperature to inhibit homogeneous reactions within the reagent solutions. The chilled solutions are dispensed through showerheads, one at a time, onto a substrate. One of the showerheads includes a nebulizer so that the reagent solution is delivered as a fine mist, whereas the other showerhead delivers reagent as a flowing stream. A heater disposed beneath the substrate maintains the substrate at an elevated temperature at which the deposition of a desired solid phase from the reagent solutions may be initiated. Each reagent solution contains at least one metal and either S or Se, or both. At least one of the reagent solutions contains Cu. The apparatus and its associated method of use are particularly suited to forming films of Cu-containing compound semiconductors.

A process for making a diffusely reflecting polarizer comprises the steps of arranging polymeric fibers containing certain fibrils and forming a solid film. A diffusely-reflective polarizer employs the film to effect polarization.

The invention relates to a multi-field coupled loading micro nanometer press-in testing system and a multi-field coupled loading micro nanometer press-in testing method. The system comprises a mechanical loading and measurement sub system, a magnetic field loading and measurement sub system, an electric field loading and measurement sub system, and a circulating oil bath heating field loading and measurement sub system; a variable magnetic field is applied by controlling the magnitude of current flowing through an electromagnet; a variable electric field is applied by a high-precision voltage-stabilizing power supply, and the electric field is applied in different directions of a test sample by adjusting the position distribution of positive and negative electrodes on the test sample; and silicone oil is heated in a heating area, and flows to an oil bath cavity through an oil path, and the test sample is heated by a test sample platform through heat conduction. The multi-field coupled loading micro nanometer press-in testing system has a compact structure, has high practical value, and can detect micro and nano scalephysico-mechanical properties of an electromagnetic solid film material accurately; and the principle is reliable.

In present ivnention the aliphatic acid which is easy to be adsorbed on the solid surface is used as raw material, with the chemical adsorption property of active group being in solution on some solids (silver and aluminium oxide) and sol-gel method to prepare solid film and self-assemble stable and ordered unimolecular aliphatic acid extra-thin film with low surface energy on it. It is characterized by that toxicity of raw material is low, film is compact and uniform, its preparation process is simple, said film possesses good abrasion-resistance, anti-friction property and antisticking property, and said ivnented aliphatic acid unimolecular film and solid film also have good combination property.

A piezoelectric thin film element includes a vibration plate, a lower electrode provided on the vibration plate and made of a conductive oxide, a piezoelectric thin film provided on the lower electrode and made of a polycrystalline substance, and an upper electrode provided on the piezoelectric thin film, wherein the lower electrode includes a titanium oxide film formed on the vibration plate, a platinum film formed on the titanium oxide film, and a conductive oxide film formed on the platinum film and, the platinum film and the conductive oxide film being a solid film with no holes.

A method for depositing a solid film of ZnO onto a substrate from a reagent solution includes a reservoir of reagent solution maintained at a sufficiently low temperature to inhibit homogeneous reactions within the reagent solution. The reagent solution contains a source of Zn, a source of O, and multiple ligands to further control solution stability and shelf life. The chilled solution is dispensed through a showerhead onto a substrate. The substrate is positioned in a holder that has a raised structure peripheral to the substrate to retain or impound a controlled volume (or depth) of reagent solution over the exposed surface of the substrate. The reagent solution is periodically or continuously replenished from the showerhead so that only the part of the solution directly adjacent to the substrate is heated. A heater is disposed beneath the substrate and maintains the substrate at an elevated temperature at which the deposition of a desired solid phase from the reagent solution may be initiated. The showerhead may also dispense excess chilled reagent solution to cool various components within the apparatus and minimize nucleation of solids in areas other than on the substrate. The deposited film may be annealed after deposition and may be doped to enhance selected characteristics. The ZnO films made by the process have distinctive electrical and optical properties and are suitable for a variety of electronic and optical devices.

The invention relates to a high luminance, high efficiency indole 3,2-b carbazole derivatives organic electroluminescenct material, belonging to the organic electroluminescent material technical field. The general structural formula of the indole 3,2-b carbazole derivatives organic electroluminescent compound is in the picture; in which, R3, R7 is alkyl or the substitute aryl, R1, R2 or R4-R6, R8 is hydrogen atom, benzene, naphthaline, anthracene, fluorine, carbazole, triarylated amine, thiophene, pyridine, pyran, quinoline, pyrrole, furan or imidazole. The compound of the invention has high fluorescence in both solution and solid film and has high film forming ability, thermal stability and photostability.

The antiwear lubricating paint for engine piston ring is one kind of dry film lubricant. The paint consists of compoiste adhesive, antiseptic additive, antiwear additive, surfactant and dispersing medium. It is painted to the surface of piston and high temperature cured to form firm, compact and dense solid film with excellent antiwear resistance, high impact resistance and good sealing performance.

A cryogenic fuel tank assembly 10 is provided comprising a cryogenic fuel tank wall 22. A foam assembly 24 is affixed to the cryogenic fuel tank wall 22, the foam assembly 24 having an inner surface 30 and an outer surface 32. A first solid film 40 bonded to the outer surface 32 to provide a uniform outer bonding surface 42. A thermal protection system assembly 38 is bonded to the uniform outer bonding surface 42.

A hood latch mechanism having interengaging pivot elements and pins for pivotally carrying the elements, first and second parts of a frame which are placed on opposite side of the pivot elements, the parts being held together tightly by pins pivotally carrying the pivot elements on the frame parts, springs biasing the pivoting elements to predetermine positions away from the hasp catched position, the pivotal elements and pins having a coating thereon of non-conductive resin and lubricious solid film with the frame and springs having a cathodic electropainted coating thereon, the coatings permitting manual override of the springs to facilitate release of the catched position.

An apparatus for depositing a solid film onto a substrate from a reagent solution includes a reservoir of reagent solution maintained at a sufficiently low temperature to inhibit homogeneous reactions within the reagent solution. The reagent solution contains multiple ligands to further control temperature stability and shelf life. The chilled solution is dispensed through a showerhead onto a substrate. The substrate is positioned in a holder that has a raised structure peripheral to the substrate to retain or impound a controlled volume (or depth) of reagent solution over the exposed surface of the substrate. The reagent solution is periodically or continuously replenished from the showerhead so that only the part of the solution directly adjacent to the substrate is heated. A heater is disposed beneath the substrate and maintains the substrate at an elevated temperature at which the deposition of a desired solid phase from the reagent solution may be initiated. The showerhead may also dispense excess chilled reagent solution to cool various components within the apparatus and minimize nucleation of solids in areas other than on the substrate. The apparatus and its associated method of use are particularly suited to forming films of II-VI semiconductors.

The present invention provides a fingerprint input device capable of obtaining a fingerprint image presenting sufficient contrast. The fingerprint input device includes: a two-dimensional image sensor for picking up a fingerprint image from a fingerprint measured portion of a measurement target finger; and a transparent solid film mounted on an image pickup surface of the two-dimensional image sensor, the fingerprint measured portion being mounted on the transparent solid film when the two-dimensional image sensor picks up the fingerprint image, wherein the fingerprint input device picks up an image of a fingerprint ridgeline portion in the fingerprint measured portion as a light portion, and picks up an image of a fingerprint valley portion in the fingerprint measured portion as a dark portion through an air layer, and a refractive index of the transparent solid film satisfies that contrast of the image is more than a given value.