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30 results about "Sodium complex" patented technology

Synthesis method of hydroquinone

The invention relates to a synthesis method of hydroquinone. The method is characterized by comprising the following steps: carrying out catalytic oxidation on phenol and oxygen to generate a mixture of p-benzoquinone and o-benzoquinone, wherein a catalyst is copper and sodium complex salt; distilling to remove solvent, adding water in residual materials, and separating p-benzoquinone and o-benzoquinone by distillation; reducing separated p-benzoquinone with a reducing agent to obtain hydroquinone, filtering out hydroquinone crude product and recrystallizing so as to obtain hydroquinone crystal; and concentrating a mother liquid obtained by filtering out hydroquinone or catechol crude product to obtain an ammonium sulfate fertilizer. The synthesis method has simple process, mild reaction conditions and short reaction period, and the yield of hydroquinone in the product is larger than that of catechol.
Owner:NANJING UNIV OF INFORMATION SCI & TECH

Production process for synthetizing EDDHA (Ethylenediamine-N,N'-bis(2-hydroxyphenylacetic acid) ferric-sodium complex) Ferrochel with one-step method

The invention provides a production process for synthetizing EDDHA Ferrochel with a one-step method, comprising the following process steps of: weighing the following raw material components in the molar ratio: 1.0% of phenol, 0.4-0.6% of quadrol, 2.0-4.0% of sodium hydroxide, 0.8-1.2% of glyoxylic acid, 0.5% of iron ion and 20% of water; firstly, synthetizing EDDHA aqueous solution; then reacting with ferric salt to synthetizing EDDHA Ferrochel solution; and drying to finally obtain the EDDHA Ferrochel. The production process has the advantages of short process flow, high yield, low production cost, no pollution and low energy consumption and does not need organic solvent. The iron content of the EDDHA Ferrochel is more than 7%, when the EDDHA Ferrochel is dissolved in water, the content of the water insoluble is less than 0.1%, and EDDHA Ferrochel is stable when PH is between 3 and 10. The EDDHA Ferrochel is mainly used as fertilizer.
Owner:SICHUAN TONGFENG TECH

Preparation method of polyamide reverse osmosis membrane containing amphoteric carboxymethylcellulose sodium complex

The invention discloses a preparation method of a polyamide reverse osmosis membrane containing an amphoteric carboxymethylcellulose sodium complex. The preparation method comprises the steps: firstly, preparing an amphoteric cationic polymer by a free radical polymerization method, then preparing an amphoteric carboxymethylcellulose sodium complex by an ionic crosslinking method, adding the amphoteric carboxymethylcellulose sodium complex into an aqueous phase monomer solution for preparing a polyamide membrane, and thus obtaining the polyamide reverse osmosis membrane containing the amphoteric carboxymethylcellulose sodium complex through an interfacial polymerization method. With utilization of good hydrophilicity, contamination resistance and a unique nanoparticle structure of the amphoteric carboxymethylcellulose sodium complex, the water permeation flux and contamination resistance of the membrane are greatly improved while the high salt interception rate of the polyamide membrane on an inorganic salt is kept. Under an operating pressure of 1.5 MPa at the temperature of 25 DEG C, the interception rate of the reverse osmosis membrane on NaCl is more than 97%, and the water permeation flux is more than 30 L.m<-2>.h<-1>. Therefore, the prepared polyamide reverse osmosis membrane containing the amphoteric carboxymethylcellulose sodium complex has high salt interception rate, water permeability and contamination resistance.
Owner:ZHEJIANG UNIV

Preparation method of iron-tartaric acid-sodium complex

The invention discloses a preparation method of an iron-tartaric acid-sodium complex. The preparation method comprises following steps: (1) water and dextrotartaric acid are added into a high-pressure reaction vessel, wherein the dextrotartaric acid concentration of the solution is more than 5 wt%; the solution is stirred, heated to 155 to 175 DEG C, and reacted for 8 to 48h at the temperature of 155 to 175 DEG C; (2) the contents of the ingredients in the high-pressure reaction vessel are determined, and the reaction is stopped when more than 30 wt% of dextrotartaric acid is converted to mesotartaric acid; (3) the ingredients in the high-pressure reaction vessel are cooled to room temperature, and then the solution is discharged; (4) a solution containing Fe3<+> is added into the solution with stirring; and (5) a solution containing Na<+> is added into the solution with stirring, the mixture is stirred until appearance is clear, color is uniform, no precipitate is generated and no stratification is causes, and then the iron-tartaric acid-sodium complex is obtained. Reaction conditions of the preparation method are mild; the preparation method is simple; consumption of raw materials is less; no pollution is caused; the preparation method is suitable for industrial production; and the stability of the iron-tartaric acid-sodium complex is much higher than that of complex prepared by existing methods.
Owner:HUNAN XUETIAN FINE CHEM IND

Preparation method of novel silicane fire retardant

The invention relates to a preparation method of novel silicane fire retardant. The method includes the following steps of firstly, dissolving siloxane in organic solvent with the siloxane as raw materials, adding a potassium hydroxide catalyst, and conducting heating reflux for 15-30 minutes after the mixture is stirred to be uniform so that sodium complex can be obtained; secondly, adding phosphorus trichloride for substitution after the phosphorus trichloride is slightly cooled, conducting reflux again for 25-40 minutes, and converting the phosphorus trichloride into phosphorus complex; thirdly, conducting filtering after cooling, cooling filtrate to -5 DEG C after the filtrate is concentrated, and generating white crystals; fourthly, flushing the white crystals obtained in the third step through methyl alcohol, placing the white crystals in a room-temperature vacuum oven to be dried for 0.6-1.5 hours, and obtaining the silicane fire retardant. Compared with the prior art, the reaction condition is gentle, the reaction temperature is moderate, the obtained finished product can be quite easily separated from a reaction system, the flame retardant property and the oxidation resistance can be effectively improved, and meanwhile the mechanics performance, the insulating performance and the heat resistance are not influenced.
Owner:SHANGHAI PUYANG NEW MATERIAL TECH CO LTD

Asphalt aging inhibitor applied to northeast coastal areas, and preparation method thereof

The invention discloses an asphalt aging inhibitor applied to northeast coastal areas. The common action of propylene glycol, nano-scale spinel powder, raw vermiculite powder and flame-retardant polyamide 66 composite fibers achieves excellent flame retardation and smoke suppression effects in the combustion process, so the flammability of asphalt is effectively reduced, and the use safety and theconstruction safety of an asphalt pavement are improved; the addition of propylene glycol can improve the low temperature resistance of the aging inhibitor, and an added iron-sodium diethylenetriaminepentaacetate complex can resist the corrosion of chloride ions and other inorganic salts in seawater to the asphalt pavement; and the aging inhibitor is mainly prepared by grinding natural minerals,is free from phosphorus and halogen, has no adverse effects on the environment, and has a remarkable environmental protection benefit.
Owner:山西云度知识产权服务有限公司

A detergent for toilet disinfection

A detergent for toilet disinfection is disclosed. The detergent comprises following components by mass: 5-7 parts of sodium metasilicate pentahydrate, 2-4 parts of oxalic acid, 3-4 parts of sodium hexametaphosphate, 5-7 parts of a sodium complex, 6-7 parts of sodium silicate, 9-11 parts of tea dregs, 4-8 parts of tri(propylene glycol) butyl ether, 6-10 parts of linseed oil, 6-8 parts of tri(propylene glycol) methyl ether, 4-6 parts of urea, and 1-2 parts of a brightening agent. The detergent is used for toilet cleaning, deodorizing and disinfection.
Owner:孙静

Ceramic tile detergent

The invention relates to the field of detergents, in particular to a ceramic tile detergent which consists of the following substances in parts by weight: 6-12 parts of nitrilotriacetic acid trisodium salt, 15-20 parts of turpentine, 8-12 parts of propylene glycol monomethyl ether, 15-25 parts of a lacquer thinner, 15-25 parts of oxalic acid, 4-6 parts of 2-amino-2-methyl-1-propyl alcohol, 1-3 parts of lauryl sodium sulfate, 15-25 parts of citric acid, 5-10 parts of glycolic acid, 2-3 parts of coconut fatty acid diethanol amine, 2-5 parts of polyoxyethylene fatty acid, 15-20 parts of hydroxyethyl cellulose, 1-2 parts of a diethylenetriamine pentaacetic acid iron-sodium complex, 5-8 parts of a waterproof agent, 3-5 parts of a corrosion inhibitor, 5-8 parts of perfume and 50-60 parts of water. The ceramic tile detergent provided by the invention is thorough in washing, the original feature of a ceramic tile can be rapidly recovered, a surface protection agent is available, a layer of a protection membrane is generated on the surface of the ceramic tile, due to addition of the waterproof agent, the phenomenon of slipping can be effectively avoided after the ceramic tile is washed, and due to addition of the corrosion inhibitor, the service life of the ceramic tile can be prolonged.
Owner:QINGDAO HUANAN SHENGYUAN FRUIT IND CO LTD

Preparation method of iron-tartaric acid-sodium complex

The invention discloses a preparation method of an iron-tartaric acid-sodium complex. The preparation method comprises following steps: (1) water and dextrotartaric acid are added into a high-pressure reaction vessel, wherein the dextrotartaric acid concentration of the solution is more than 5 wt%; the solution is stirred, heated to 155 to 175 DEG C, and reacted for 8 to 48h at the temperature of 155 to 175 DEG C; (2) the contents of the ingredients in the high-pressure reaction vessel are determined, and the reaction is stopped when more than 30 wt% of dextrotartaric acid is converted to mesotartaric acid; (3) the ingredients in the high-pressure reaction vessel are cooled to room temperature, and then the solution is discharged; (4) a solution containing Fe3<+> is added into the solution with stirring; and (5) a solution containing Na<+> is added into the solution with stirring, the mixture is stirred until appearance is clear, color is uniform, no precipitate is generated and no stratification is causes, and then the iron-tartaric acid-sodium complex is obtained. Reaction conditions of the preparation method are mild; the preparation method is simple; consumption of raw materials is less; no pollution is caused; the preparation method is suitable for industrial production; and the stability of the iron-tartaric acid-sodium complex is much higher than that of complex prepared by existing methods.
Owner:HUNAN XUETIAN FINE CHEM IND

Sodium complex fertilizer, uses and employing method thereof

The invention relates to sodium composite fertilizer which can promote the growth of desert plants and increase the drought resistance performance of the desert plants, as well as the application and the fertilizing method thereof. The sodium composite fertilizer is characterized in that the fertilizer consists of the raw materials as follow in weight percent: 0 to 85 percent of sodium nitrate, 0to 22 percent of monobasic sodium phosphate, 0 to 99 percent of sodium silicate, and 0 to 90 percent of sodium chloride. The application of sodium composite fertilizer is that the sodium composite fertilizer can be directly fertilized in plants grown in desert areas or can be used for seeding the desert plants or can be used in the sand cultivation or water cultivation of the desert plants. The sodium composite fertilizer has the fertilizing method that the sodium composite fertilizer is fertilized into the desert soil with 6 kg to 60 kg for one acre, or 0.2 to 3 g of fertilizer is directly fertilized into 1 kg of the soil, or 0.2 to 3 g fertilizer is firstly dissolved with water, and the water-fertilizer mixed solution is fertilized into 1 kg of the soil. The invention has the advantagesof further expanding the vegetation-covered areas of desert areas by providing the sodium composite fertilizer which can promote the growth of the desert plants and increase the drought resistance performance of the desert plants, as well as the application thereof, thereby solving the problem of continuously expanding desertification, and promoting the recovery of the plants and the reestablishment of the ecological system.
Owner:LANZHOU UNIVERSITY

A kind of glycerin-carboxymethylcellulose sodium composite type hydrogen peroxide bleaching stabilizer and its application

ActiveCN106120295BStrong heat and alkali resistance and oxidation resistanceEasy to useLiquid/gas/vapor fibres/slivers/rovings treatmentFiberCarboxymethyl cellulose
The invention discloses a glycerinum-carboxymethylcellulose compound hydrogen peroxide bleaching stabilizer and an application thereof. The compound hydrogen peroxide bleaching stabilizer is prepared from the following components in parts by weight, 1-1.5 parts of glycerinum, 0.1-2 parts of carboxymethylcellulose, 2-2.7 parts of soluble starch and 10-14 parts of water. A preparation method of the compound hydrogen peroxide bleaching stabilizer includes the steps: mixing the water with the glycerinum and heating the water and the glycerinum to 100 DEG C; adding the soluble starch into mixed boiling solution and uniformly stirring the solution; slowly dripping carboxymethylcellulose solution and then performing low-temperature standing. The compound hydrogen peroxide bleaching stabilizer is applied to the bleaching process of linen rove and a fabric thereof. The hydrogen peroxide bleaching stabilizer has the function of efficiently stabilizing hydrogen peroxide, is low in fiber material damage, high in heat resistance, alkali resistance and oxidation resistance, easy to use, good in compatibility with other auxiliaries, low in cost and ideal, and reduces environmental pollution.
Owner:绍兴市荣士达衬布有限公司

Surface modification method of anti-oxidation nano-calcium carbonate for silicone sealant

The invention discloses a surface modification method of anti-oxidation nanometer calcium carbonate used for a silicone sealant. The method comprises the following steps: 1, preparing a material: preparing a nanometer calcium carbonate slurry; 2, carrying out surface treatment: adding fatty acid and diethylenetriaminepentaacetic acid ferric-sodium complex mixed saponification liquor to the nanometer calcium carbonate slurry, and stirring to prepare a modified nanometer calcium carbonate slurry; 3, dehydrating and drying: carrying out dehydrating and drying treatment on the modified nanometer calcium carbonate slurry; and 4, crushing the obtained material to obtain a nanometer calcium carbonate product. The nanometer calcium carbonate product modified through the method has good compatibility to a silicone adhesive system, and a filled sealant has good mechanical strength and very good anti-oxidation characteristic. The product has the advantages of good dispersibility, less agglomeration, good thixotropy and processability, and effective increase of the tensile strength and the elongation at break of the silicone sealant. The above preparation method has the advantages of simplicity, low production cost and good economic benefit.
Owner:GUANGXI HUANA NEW MATERIALS TECH CO LTD

Cleaning wet tissue for liquid crystal screen

The invention discloses cleaning wet tissue for a liquid crystal screen. The cleaning wet tissue comprises spunlaced nonwoven cloth and cleaning liquid, and the cleaning liquid is composed of 6-15% of dodecyl glucoside, 5-10% of tripropylene glycol monomethyl ether, 5-10% of ethylene glycol monoethyl ether, 3-5% of N-methyl-2-pyrrolidone, 0.2-0.4% of DTPA iron-sodium complex, 0.2-0.4% of trisodium N-iminodiacetate and the balance of deionized water. The cleaning wet tissue is convenient to use, capable of quickly cleaning oil stain and dirty marks on the screen, free of residue and free of damage to the screen.
Owner:HEFEI HUIKE PRECISION DIE CO LTD

Easy-to-clean floor detergent

The invention discloses an easy-to-clean floor detergent which is prepared from, by weight, 6-11 parts of lauryl alcohol polyoxyethylene ether, 7-10 parts of sodium xylene sulfonate, 1.5-2.3 parts of dimethoxybenzene, 4-6 parts of o-methylphenyl acetic acid, 1-4 parts of ethylparaben, 12-17 parts of dimethyl silicon oil, 2.4-5 parts of oleic acid, 8-11 parts of potassium silicate, 3-5 parts of diethyltriaminepentaacetate iron-sodium complex, 0.5-1.2 parts of methylisothiazolinone, 8-13 parts of lauramidopropyl betaine, 3-8 parts of triethanolamine, 2.3-5 parts of 45% methanol, 3.2-5.4 parts of citric acid and 1.3-2.7 parts of ethylene glycol butyl ether. The easy-to-clean floor detergent has the advantages of being capable of deeply cleaning various stains in floors, low in foam, easy to clean, good in aromatic smell and free of irritation.
Owner:青岛千帆高新技术有限公司

Formula of automobile windscreen cleaning agent

The invention discloses a formula of an automobile windscreen cleaning agent. The formula of the automobile windscreen cleaning agent is prepared from the following raw materials in parts by weight: 4-13 parts of C8-10 fatty alcohol polyoxyethylene ether phosphate monoester, 6-12 parts of a diethylenetriamine pentaacetic acid iron-sodium complex, 5-8 parts of sodium dodecyl benzene sulfonate, 6-10parts of tripolyphosphate, 4-6 parts of alcohol, 8-12 parts of potassium sorbate, 2-4 parts of ethyecellulose, 3-6 parts of 3-phosphoglyceric acid, 1-2 parts of an anionic surfactant I, 5-9 parts ofsodium tripolyphosphate, 2-3 parts of an anionic surfactant II, 1-3 parts of isopropanol and 1-2 parts of nano-titanium sol. The formula of the automobile windscreen cleaning agent has the beneficialeffects that the cleaning agent is capable of effectively cleaning stains on the windscreen, the cleaning agent has the advantages of high cleaning capability, short washing time, no corrosion to substrate, no irritation to human body and no trace after being used, a protection layer can be formed on the outer surface of the windscreen, and the cleaning agent is capable of preventing dust accumulation in a certain time and preventing water stain residue.
Owner:成都凯斯恩科技有限公司
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