The invention discloses a preparation method of a nanometer soft magnetic
manganese zinc ferrite preparation method, belonging to the ferrite magnetic
material technology field. The method comprises: a first step of preparing
manganese zinc ferrite nanometer power; a second step of pressing to form a circular blank; a third step of
sintering the prepared product, i.e., putting the formed blank in the second step into a tube electric resistance furnace, rising the temperature from the
room temperature to 900-1100 DEG C at a speed of 5 DEG C / minute under
nitrogen protection, free-cooling the temperature to 850 DEG C, insulating heat under the temperature in two hours, then free-cooling to the
room temperature, and finally obtaining the soft magnetic
manganese zinc ferrite sinter, i.e., the nanometer soft magnetic
manganese zinc ferrite product. The method of the invention adopts a low-temperature two-step
sintering process, has low
sintering temperature, short sintering time and no high-temperature
solid-phase
chemical reaction process, thereby realizing energy-saving, consumption reduction, low production cost and high yield.