The invention provides an
ammonia recycling method and a
system in APT production process. The
ammonia recycling method comprises following steps: 1, APT
crystallization steam is discharged using a
centrifugation blower fan, is introduced into a rectifying
tower for rectification and condensation of
ammonia tail gas to remove most water, and is introduced into a
heat exchanger; 2, a
three stage solution obtained via
ion exchange is directly used for preparing a
desorption agent, the rest
ammonia nitrogen wastewater is pumped into a stirring tank, an alkali is added for ammonia activation, andgenerated ammonia
tail gas is introduced into the
heat exchanger;
wastewater obtained via ammonia activation is pumped into an
air stripping tower, and ammonia
tail gas obtained via
air stripping is introduced into the
heat exchanger; when the ammonia-
nitrogen value of obtained
air stripping wastewater is detected to be qualified, discharging through a
branch pipe is carried out, otherwise, the wastewater is pumped into the air stripping
tower for air stripping; and 3, the temperature of the ammonia tail gas is reduced to be lower than 45 DEG C
after treatment using the heat exchanger, the ammonia tail gas is introduced into a
hydrochloric acid absorbing tower for circulating absorption, and an obtained solution is sent back to the main treatment
stream directly for preparation of the
desorption agent. The ammonia recycling method and the
system are used for comprehensive treatment of
ammonia nitrogen wastewater
waste gas obtained in
tungsten smelting, waste is changed into valuables,the method flow is simple, operation is convenient, the method is easy to control, and cost is low.