The invention relates to the technical field of
metal rust protection, in particular to a method for manufacturing water-based
metal antirust agents. The method comprises the following steps that
caprolactam and
sodium hydroxide are put into water according to the
molar ratio of 1:0.8 to 1.5, temperature rises to 60 DEG C to 100 DEG C, and the temperature is kept for three hours to ten hours; (2) the temperature is cooled to 0 DEG C to 20 DEG C, and 1 / 5 to 1 / 3 of the
molar weight of
caprolactam is put according to the step (1),
cyanuric chloride is added, heat preservation is carried out for one to three hours,
sodium hydroxide is added, and the PH value is adjusted to 7.5 to 12; (3) temperature rises to 70 DEG C to 100 DEG C, the temperature is kept for five hours, and the
sodium hydroxide is used for adjusting the PH value to 7.5 to 12; (4) the temperature is cooled to 30 DEG C to 50 DEG C, solutions are filtered, then,
hydrochloric acid is added to enable the PH value to one to three, circulating stirring is carried out, and the heat preservation is carried out for one to five hours at the temperature of 30 DEG C to 60 DEG C. The method for manufacturing the water-based
metal antirust agents has the advantages of being
environmentally friendly, high in yield, high in product purity, excellent in product performance and low in cost.