The invention discloses a preparation method of a permanent purple
pigment. The preparation method of the permanent purple
pigment comprises ball-milling, by weight part, 600 parts of permanent purplecrude products for 20-50 h to obtain pre-milled materials; adding 500-550 parts of n-butyl
alcohol and 4000-5000 parts of water into the pre-milled materials, and reflowing the mixture for 3-5 hoursto obtain
crystal-transformed pre-milled materials; washing and then
evaporation-
drying the
crystal-transformed pre-milled materials obtain dried
crystal-transformed pre-milled materials; adding diluted
hydrochloric acid into the dried crystal-transformed pre-milled materials to obtain acidified materials; filtering the acidified materials to obtain an acidified material
filter cake; at high speeddispersing the acidified material
filter cake into water to obtain a
slurry, and secondary-filtering the
slurry to obtain a finished product
filter cake;
drying the finished product filter cake to obtain the permanent purple
pigment. By adding the diluted
hydrochloric acid into the dried crystal-transformed pre-milled materials to remove impurities produced during ball milling, the preparation method of the permanent purple pigment can reduce the
conductivity of the permanent purple pigment, avoid
polymerization of the permanent purple pigment and reduce the
viscosity of the permanent purplepigment; besides, serving as
crystal transformation solvent, the n-butyl
alcohol is relatively low in
toxicity and easy to recover, thereby being beneficial to cost saving, and meanwhile, through reflowing of n-butyl
alcohol aqueous solution, the permanent purple pigment can be high in tinting strength and saturation in an water-based ink
system.