The invention discloses a method for extracting and separating volatile oil, flavone and
polysaccharide of
abelmoschus manihot flowers. The method comprises the following steps: (1) smashing the
abelmoschus manihot flowers dried in the shade into 10-80 mesh
powder, adding an
organic solvent into the
powder, and carrying out
reflux extraction, thus obtaining an extracting solution and
drug dregs; (2) preparing volatile oil, namely, carrying out water
distillation on the extracting solution to prepare the volatile oil of the
abelmoschus manihot flowers; (3) carrying out extraction on the
drug dregs by adopting
warm water, and adding
ethanol into the liquid obtained after extraction for separation, thus obtaining a supernate and a precipitate; (4) preparing general flavone, namely, concentrating and
drying the supernate to obtain the general flavone; and (5) preparing total
polysaccharide, namely,
drying the precipitate, thus obtaining the total
polysaccharide. According to the method for extracting and separating the volatile oil, the flavone and the polysaccharide of
abelmoschus manihot flowers, the three-component extraction
separation method is adopted, and the three active materials, including the volatile oil, the flavone and the polysaccharide of the
abelmoschus manihot flowers are extracted and separated, the active materials of the
abelmoschus manihot flower medicinal material are sufficiently utilized, and a foundation is laid for the comprehensive development and application of the
abelmoschus manihot flower medicinal material.