33results about How to "Uniform network structure" patented technology

The invention relates to a hydrophobic silica aerogel heat-insulation composite material. The composite material consists of silica aerogel and an inorganic fiber product, wherein the silica aerogel is doped with a flame retardant and an infrared blocking agent; the inorganic fiber product comprises one or more of glass fibers, quartz glass fibers, aluminium silicate fibers, ceramic fibers, alumina fibers, zirconia fibers, rock wool fibers and basalt fibers, and the porosity of the inorganic fiber product is higher than 50%. The composite material has the overall waterproof performance, the extremely low heat conductivity coefficient and the excellent high-temperature heat-insulation performance, can pass an incombustibility test under the condition that the material is ensured to be hydrophobic as a whole, and reaches level A1 according to the incombustibility test; the preparation process is simple, the production cycle is short, the cost is lower, the equipment requirement is low, and reaction conditions are controllable.

The invention relates to a method for preparing ceramic foams with pore gradient. The method comprises the following steps: arranging polymers or organic matter spheres to form a template in gradient distribution according to the design requirement, carrying out heating and pressurizing to ensure the spheres to adhere to each other to form a whole, filling the whole into a moulding mould and then injecting slurry for gel casting and removing the mould after drying the spheres to obtain a moulded green body integrating the spheres and solidifying slurry, immersing the green body after removing the mould into a solvent or warming the green body, removing the spheres to obtain a network-shaped body only with the solidifying slurry and obtaining the ceramic foams with pore gradient after binder removal and high-temperature sintering. The ceramic foams prepared according to the technical scheme adopted by the invention have the following advantages: the pore diameters are in gradient distribution; the pore gradient can be designed and controlled; the moulded green body has high strength and can be processed and cut into needed shapes; the sizes and shapes of the products are controllable; the problem that the shapes and sizes of the products as well as the sizes of the pores are usually limited by organic carriers in the process of preparing the ceramic foams is solved; and the shortcomings of less slurry absorbed for moulding, more blind pores and low product strength in the impregnation method are overcome.

The invention discloses a preparation method of a CuW70 contact material, comprising the steps of: adding inducing copper powder into tungsten powder in certain proportion and mixing them well, putting the mixed powder into a rubber sheath which is then placed in the high pressure cylinder of a cold isostatic pressing machine so as to be pressed into a skeleton green body, and then preparing the CuW70 contact material through copper infiltration of the sintered skeleton. Due to disappeared copper-rich area and uniform two-phase distribution of the prepared CuW70 contact material by the methodof the invention, the material has rapidly moving cathode spot on the surface, effectively dispersed electric arc, less copper phase splashing, and improved ablation resistance.

The invention discloses an aquatic biological source medical collagen with high purity and activity, and is capable of solving the problems of a natural collagen dressing that the mechanical strength is bad, the degradation resistance ability is weak and the wound is easily infected by microorganisms. An acid extraction method and a method of removing telopeptide by pepsase are used for extracting the collagen, the extraction ratio is improved by the ultrahigh pressure treatment and a tissue mashing method, and through a series of purification operations, such as decellularization, protein elimination, degreasing, repeated salting out, dialysis, degerming, decoloration and heat source removal, the medical collagen with the high purity and activity is prepared. A netlike collagen sponge with uniform pores is prepared by a vacuum freeze-drying technology, and the collagen sponge is modified by a physical crosslinking and chemical crosslinking mode so as to prepare the inner layer, and is compounded with a chitosan outer layer film and a medical non-woven fabric base cloth layer, finally a compound multilayer medical dressing finished product is obtained by Co-60 sterilization.

The invention discloses a preparation method of a cellulose based conductive hydrogel. The preparation method comprises the following steps: (1) dissolving microcrystalline cellulose (MCC) with 1-Butyl-3-methylimidazolium chloride, reacting in a N2 protective atmosphere, and adding N,N-methylenebisacrylamide and benzoyl peroxide to prepare a pure microcrystalline cellulose hydrogel; and (2) soaking the pure microcrystalline cellulose hydrogel obtained in the step (1) in a mixed solution of FeCl3 and sodium p-benzenesulfonate, and immersing in a pyrrole water solution to prepare the cellulose based conductive hydrogel. The cellulose based conductive hydrogel prepared by the method has the advantages of uniform stable network structure, excellent conductivity, swelling property and heat stability, favorable electric conductivity and favorable swelling property; and the equilibrium swelling rate can be up to about 500%.

The invention discloses a making technology of potato noodles. The making technology comprises the following steps of taking potato whole powder and wheat flour in a proportion of the potato whole powder to the wheat flour being (0.5-2) to 1, and performing uniform stirring to obtain mixed powder; adding vital wheat gluten of which the percentage by weight is 1-3%, alginic acid of which the percentage by weight is 0.2-0.4% and table salt of which the percentage by weight is 3-5% to the mixed powder, performing uniform stirring, adding water, and performing dough mixing; leavening the mixed dough for 15-60min; and putting the leavened dough in a machine, and performing extrusion and shaping. The vital wheat gluten is added during dough mixing, so that the moldability of dough sheets can beimproved, the chewiness is improved, the loss rate of the noodles is reduced, and the expansivity of the noodles is increased; the table salt is added during dough mixing, so that the flavor, the color and the texture characteristics of the noodles can be improved; through addition of an appropriate amount of the table salt, the plump mouth feel of the noodles can be improved, the peculiar smell is concealed, the balanced flavor is increased, and the flexibility of the noodles can be improved. According to the leavening time, the condition that starch and protein can sufficiently absorb moisture is facilitated, so that a uniform network structure is formed, and the quality of the made noodles is good.

The invention provides a production method for a fish oil microcapsule product with ultrafine edible fungus powder as a main wall material. Main materials for microcapsule encapsulation are ultrafine mushroom and tremella powder and perilla oil used as a deodorization substance for fish oil. The production method comprises the following steps: preparation of the ultrafine mushroom and tremella powder; preparation of composite fish oil; and preparation of a fish oil microcapsule. The prepared fish oil microcapsule product has a pure white color and good appearance and can effectively encapsulate a core material. The product has strong antibacterial activity, effectively inhibits fishy smell of the fish oil, supplements and reinforces the function of unsaturated fatty acid of the fish oil and has the excellent characteristics of water solubility, thickening performance, gelatinization, film formation, etc. The wall material of the fish oil microcapsule becomes a nutrition component for the product and enriches nutritional functions of the fish oil product.

The invention relates to a hyperbranched polyether functionalized graphene / epoxy resin nano composite coating as well as a preparation method and application thereof. The nano composite coating is composed of a component A and a component B, wherein the component A comprises a mixed resin, an antirust pigment, an inorganic pigment, mineral substance powder and an organic solvent; the component B is an epoxy resin curing agent; the mixed resin is composed of an epoxy resin and hyperbranched polyether functionalized graphene; and the hyperbranched polyether functionalized graphene is 2-10% of the mass of the epoxy resin. A coating prepared from the hyperbranched polyether functionalized graphene / epoxy resin nano composite coating can effectively shield corrosive substances, and shows excellent corrosion resistance, and especially the acid resistance of the nano composite coating is obviously improved and is improved by 50% compared with that of a pure epoxy resin coating.

The invention discloses a preparation method of an anti-notch-sensitivity graphene-type nano composite aquagel. By using the graphene-oxide-carried supported microgel as a crosslinking agent, the nano composite aquagel has the two crosslinking modes (physical crosslinking and chemical crosslinking), and thus, has favorable ductility and mechanical strength. The inside of the nano composite aquagel has high crosslinking density and complex crosslinking mode, and thus, the material can have favorable energy dissipation mechanism in case of cracking, and can still keep favorable ductility and mechanical strength when a notch appears in the aquagel.

The invention discloses a Ce,V and Er co-doped dental microcrystalline glass, and a preparation method and application thereof. The raw materials of the microcrystalline glass consist of SiO2, Li2O, K2O, P2O5, Al2O3, ZrO2, Na2O, CeO2, V2O52 and Er2O3. A glass block is obtained through a melt casting method, and microcrystalline glass easy for machining is obtained after crystallization treatment,and then secondary crystallization is carried out to obtain the finished product of the microcrystalline glass which takes Li2Si2O5 as a main crystalline phase. The microcrystalline glass has excellent bending strength, good semi-permeability, fluorescent property, uniform and full coloring and excellent stability. The color and the aesthetic effect of the microcrystalline glass reach the color and the aesthetic effect of A2 in a VITA-Classical colourimetric card and are consistent with the fluorescent characteristic and the semi-permeability of natural teeth, and the microcrystalline glass can be applied to dental whole-porcelain repair materials.

The invention relates to a method for preparing a hydrophobic silica airgel thermal insulation composite material, comprising the following steps: (1) Preparation of silica sol: using siloxane as a precursor, adding an organic solvent, water and an acid catalyst , to obtain silica sol; (2) Preparation of composite gel: add flame retardant and infrared blocking agent to silica sol, stir evenly; add alkali catalyst, immerse inorganic fiber products in silica sol, Stand still; (3) solvent replacement: replace the composite gel with an organic solvent; (4) dry: dry the composite gel. The invention has the advantages of simple process, short production cycle, low cost, low equipment requirements, controllable reaction conditions, and excellent product performance, and the prepared silica airgel composite material has overall waterproof performance, extremely low thermal conductivity, and excellent high temperature Thermal insulation performance, under the condition of ensuring the overall hydrophobicity of the material, it can pass the non-combustibility test, and its non-combustibility test can reach A1 level.

The invention discloses a preparation method of a CNT-GO / Cu composite material with a hierarchical structure and belongs to the field of metal-based composite material preparation. According to the preparation method, CNTs, GO, sodium hydroxide and copper acetate serve as raw materials, and the CNT-GO / Cu composite material with the hierarchical structure is prepared by adopting a molecule level blending method. The method has the beneficial effects that the process is simple, time is short, and energy consumption is low. Besides, due to the large specific surface area of GO and a high length-diameter ratio of CNTs, after the two are mixed, a mixed reinforced body with a net-shaped structure can be obtained, and the dispersion uniformity of a single reinforced body is improved. In addition,by continuously adjusting a pH value of a solution, the CNT-GO / Cu composite material with the hierarchical structure can be made. The composite material is composed of an enriched area (carbon-rich area) and a depleted area (carbon-poor area) of a carbon nanometer reinforced body, the carbon-rich area can effectively improve the strength of the composite material, and the carbon-poor area can effectively improve the toughness of the composite material, so that the composite material obtains good comprehensive performance.

The invention discloses a preparation method of a CuW70 contact material, comprising the steps of: adding inducing copper powder into tungsten powder in certain proportion and mixing them well, putting the mixed powder into a rubber sheath which is then placed in the high pressure cylinder of a cold isostatic pressing machine so as to be pressed into a skeleton green body, and then preparing the CuW70 contact material through copper infiltration of the sintered skeleton. Due to disappeared copper-rich area and uniform two-phase distribution of the prepared CuW70 contact material by the methodof the invention, the material has rapidly moving cathode spot on the surface, effectively dispersed electric arc, less copper phase splashing, and improved ablation resistance.

The invention relates to a high-permeability and high-selectivity PVA / GA / CS-M<+> pervaporation film for dewatering an organic solution and a preparation method of the high-permeability and high-selectivity PVA / GA / CS-M<+> pervaporation film. The preparation method includes: heavy metal ions (M<+>) such as Ag<+>, Cu<2+> and Fe<3+> are used to chelate with CS (chitosan) to serve as the precursor, mixing the precursor with PVA (polyvinyl alcohol), and adding GA (glutaraldehyde) to serve as the crosslinking agent to obtain the high-permeability and high-selectivity PVA / GA / CS-M<+> pervaporation filmwhich is high in mechanical strength and heat stability and excellent in permeability and selectivity to the organic solution.

The invention discloses a preparation method of a CNT-GO / Cu composite material with a hierarchical structure and belongs to the field of metal-based composite material preparation. According to the preparation method, CNTs, GO, sodium hydroxide and copper acetate serve as raw materials, and the CNT-GO / Cu composite material with the hierarchical structure is prepared by adopting a molecule level blending method. The method has the beneficial effects that the process is simple, time is short, and energy consumption is low. Besides, due to the large specific surface area of GO and a high length-diameter ratio of CNTs, after the two are mixed, a mixed reinforced body with a net-shaped structure can be obtained, and the dispersion uniformity of a single reinforced body is improved. In addition,by continuously adjusting a pH value of a solution, the CNT-GO / Cu composite material with the hierarchical structure can be made. The composite material is composed of an enriched area (carbon-rich area) and a depleted area (carbon-poor area) of a carbon nanometer reinforced body, the carbon-rich area can effectively improve the strength of the composite material, and the carbon-poor area can effectively improve the toughness of the composite material, so that the composite material obtains good comprehensive performance.

The invention discloses a preparation method of an anti-notch-sensitivity graphene-type nano composite aquagel. By using the graphene-oxide-carried supported microgel as a crosslinking agent, the nano composite aquagel has the two crosslinking modes (physical crosslinking and chemical crosslinking), and thus, has favorable ductility and mechanical strength. The inside of the nano composite aquagel has high crosslinking density and complex crosslinking mode, and thus, the material can have favorable energy dissipation mechanism in case of cracking, and can still keep favorable ductility and mechanical strength when a notch appears in the aquagel.

The invention belongs to the field of active pharmaceutical ingredient screening, and particularly relates to a lipid raft@organic-inorganic hybrid monolithic column as well as a preparation method and application thereof. According to the invention, an organic-inorganic hybrid monolithic column is used as a matrix, and the permeability and the specific surface area of the organic-inorganic hybrid monolithic column are superior to the permeability and the specific surface area of a traditional silica gel packed column; a lipid raft well modifies the surface of the organic-inorganic hybrid monolithic column; the prepared lipid raft@organic-inorganic hybrid monolithic column has a uniform net structure; and different screening requirements can be met by adjustment of the aperture and permeability of the organic-inorganic hybrid monolithic column and modification with lipid rafts from different sources. The lipid raft@organic-inorganic hybrid monolithic column can be applied as an affinity screening model to lipid raft chromatography stationary phase research and online drug screening research.

The invention discloses an antibacterial dressing for chemotherapy of skin cancer and a preparation method thereof. The preparation method comprises the steps of (1) dissolving an amino-modified Pluronic F127 drug-carried micelle in water to prepare a solution with the concentration of 2-6 wt%, and uniformly stirring the solution; (2) adding water to dissolve quaternized polyglutamic acid and adding tyramine hydrochloride to prepare a polyglutamic acid solution with the concentration of 15-20 wt%; (3) uniformly mixing the solutions obtained in steps (1) and (2), and then adding 1-ethyl-(3-dimethylaminopropyl) carbodiimide hydrochloride and N-hydroxysuccinimide, stirring the mixture, pouring the mixture into a mold, and conducting demolding 2-5 minutes later to obtain the antibacterial dressing for the chemotherapy of skin cancer. The prepared antibacterial dressing for the chemotherapy of skin cancer has an ideal uniform network structure, high self-healing efficiency, great broad-spectrum antibacterial property and good wound infection prevention performance and can be used for repairing wounds after a physical resection operation of skin cancer, inhibiting infiltrating tumor tissues which cannot be resected and preventing relapse.

The invention relates to the technical field of polyamide material modification, in particular to an electromagnetic shielding polyamide material and a preparation method thereof. The electromagneticshielding polyamide material is prepared from the following raw materials in parts by weight: 75-85 parts of polyamide resin, 3-5 parts of PEDOT-g-MAH:PSS conductive powder, 10-15 parts of carbon fiber, 0.5-2 parts of a silane coupling agent, 0.1-0.5 part of an antioxidant and 2-3 parts of other auxiliary agents; the PEDOT-g-MAH:PSS conductive powder is prepared from 3,4-dioxyethylene thiophene, 3-thiophene acetic acid and sodium polystyrene sulfonate. The electromagnetic shielding polyamide material provided by the invention has excellent electromagnetic shielding performance and can effectively reduce the percolation threshold of carbon fiber in a composite material, and meanwhile, the material has excellent mechanical properties; a preparation process of the material is simple and easyto operate, and has an important practical application value.

The invention provides a carbon fiber reinforced plastic-thermoplastic laser thermal fusion welding technology. Laser surface pretreatment is conducted on carbon fiber reinforced plastic firstly, and a uniform net-shaped structure is obtained; then the laser welding work procedure is conducted, the carbon fiber reinforced plastic and thermoplastic are overlaid and positioned through pressure; and positioning laser welding is conducted on the thermoplastic and pretreated thermoplastic. According to the carbon fiber reinforced plastic-thermoplastic laser thermal fusion welding technology, the technical defect that an existing carbon fiber reinforced plastic-thermoplastic connecting technology is poor in manufacturability is overcome, the technical effects that after the carbon fiber reinforced plastic is pretreated, an extra adhesive does not need to be used, and subsequent clearing is not needed are achieved, the mechanical performance of obtained weld joints is excellent, the welding efficiency is high, and manufacturing cost is reduced.

The invention discloses hydrogel synergistically constructed by macromolecular self-assembly and metal coordination, and relates to the field of biomedical high polymer materials, and the hydrogel is prepared by the following steps: firstly, preparing nano-scale spherical casein micelles with negative charges on the surface by utilizing the characteristic that casein can be self-assembled into micelles in an aqueous solution; secondly, metal ions are added and reassembled with the casein micelles to form a spherical aggregate with the metal ions on the surface; and then adding an organic small molecule compound containing disulfide bonds to generate dynamic coordination bonds with metal ions, thereby preparing the nanoscale micelle cross-linking agent. And finally, introducing the nano-micelle cross-linking agent into a monomer solution, and constructing the high-strength multifunctional hydrogel with a uniform internal structure under the induction of ultraviolet light. The hydrogel obtained in the invention has excellent biocompatibility and relatively high adaptability, and is a multifunctional hydrogel with great medical potential.

The invention provides high-toughness hydrogel based on PHEMA as well as a preparation method and application of the high-toughness hydrogel, and belongs to the technical field of high polymer materials. The structure of the hydrogel is shown as a formula I, and x is 100-200; y is from 50 to 100; and z is in a range of 200 to 300. The hydrogel with a uniform cross-linked network structure and hydrogen-bond interaction is obtained by copolymerization of hydroxyethyl methylacrylate and maleic anhydride. The hydrogel has relatively high fracture toughness and can meet the requirements of being used as a substitute material for breasts and the like; meanwhile, thehydrogel has low elastic modulus, and stem cell adipogenic differentiation can be induced easily; in addition, the hydrogel is good in biocompatibility and has the effect of promoting growth of breast related cells. The hydrogel has excellent mechanical properties and biocompatibility, and can promote growth of breast related cells, so that the hydrogel can overcome the defects of existing breast substitute materials and the like, a breast substitute material with more excellent performance is prepared, and the hydrogel has a good application prospect.

The invention provides a hydrothermal preparation method of conductive polyaniline film. The raw materials such as aniline monomer and oxidant are pre-reacted at low temperature, and the FTO glass that has been hydroxylated beforehand is put into the hydrothermal reaction kettle with the conductive side facing down. , and then transfer the pre-reacted mixed solution into a hydrothermal reactor to react at a certain temperature for 3-4 hours; the polymer prepared by the method of the present invention can self-assemble and grow on FTO conductive glass, and the results of characterization and testing prove that polyaniline The thin film has good electrical conductivity and electrochromic performance, and can be used in electrochromic materials and the like.

The invention relates to organosiloxane compositions which can be crosslinked by hydrosilylation reaction and contain: (A) cyclosiloxanes of formula (I): [RaR1 bR2 cSiO2 / 2]m wherein the radicals and indices have the meaning given in claim 1, with the proviso that a + b + c is equal to 2, at least 3 radicals R1 are present per siloxane molecule (A) and at least m-3 radicals R2 are present per siloxane molecule (A), (B) organosilicon compounds having two Si-bonded hydrogen atoms and at least one aromatic radical and (C) catalysts that promote the addition of Si-bonded hydrogen to aliphatic multiple bonds. The invention also relates to a method for the production thereof and to the use thereof and vulcanizates obtainable therefrom.

The invention discloses edible soluble fish oil granules with the effect of improving immunity and a preparation method thereof. The edible soluble fish oil granules are prepared from fish oil as a base material, mixed fine powder as a wall material, xanthan gum and isomaltooligosaccharides according to a weight ratio of the mixed fine powder, xanthan gum, isomaltooligosaccharides to fish oil of 2.5-3: 0.5-1: 0.3-0.6: 1.1-1.6. The mixed fine powder comprises radix astragali powder, wolfberry powder, pitted red date powder and walnut kernel powder according to a ratio of 1-3: 1-2: 2-3: 1-3. The xanthan gum and isomaltooligosaccharides are edible additives approved by the FDA and have wide sources. Radix astragali, wolfberry, red dates and walnuts are common Chinese medicinal materials, are rich in polysaccharides, have a high nutritional value and can improve immunity. The preparation method can be operated simply and has stable processes. The edible soluble fish oil granules have smooth surfaces and uniform sizes, are easy to convey and store and have a good development and application prospect in the field of foods and medicines.

The invention discloses an antimony sulfide-based heterojunction photocathode and its preparation method and application. The structure consists of conductive glass, antimony sulfide light-absorbing layer, ultra-thin titanium dioxide layer and promoter layer from bottom to top. The antimony sulfide light-absorbing layer has a network structure; the thickness of the ultra-thin titanium dioxide layer is 5-10nm. The preparation method is as follows: sequentially depositing an antimony sulfide light-absorbing layer, an evenly covered ultra-thin titanium dioxide layer, and a co-catalyst layer on the conductive glass. In the present invention, the antimony sulfide material with nano-morphology is used as the light-absorbing material of the photocathode for the first time, and a photoelectrode with strong light absorption in the visible spectrum and high photoresponse characteristics is obtained through structural design. The equipment used in the invention is simple, easy to operate, and the preparation process is green and non-toxic. The photoelectrode film grows uniformly and has good crystal quality, which is conducive to large-scale production and application, and has broad development prospects.