Hydrophobic silica aerogel heat-insulation composite material
A technology of silica and composite materials, which is applied in the field of airgel thermal insulation materials, can solve the problems of limiting the application range and market of airgel products, the impact on human health and production safety, and the use of airgel products, so as to reduce the The number of times of solvent replacement, the effect of improving high-temperature heat insulation performance and convenient operation
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
preparation example Construction
[0030] The preparation method of the hydrophobic silica airgel thermal insulation composite material of the present invention comprises the following steps:
[0031] (1) Preparation of silica sol: use siloxane as the precursor, mix and stir various siloxanes evenly, then add organic solvent and water, stir evenly, keep stirring, then add acidic catalyst drop by drop to adjust the pH of the solution value to 1-6, preferably 1-5, at 0°C-70°C constant temperature for more than 6 hours, preferably at 30-70°C constant temperature for more than 8 hours, to obtain a clear silica sol; the siloxane, organic solvent , The molar ratio of water is 1:1-80:2-40, preferably 1:1-70:2-30. By optimizing the molar ratio of siloxane, organic solvent, and water, the porosity, specific surface area, density, and organic matter content of the airgel can be adjusted to obtain a silica airgel with better performance.
[0032] The organic solvent is one or more of methanol, ethanol, ethylene glycol, p...
Embodiment 1
[0041] Mix and stir methyl orthosilicate and vinyltrimethoxysilane at a molar ratio of 1:8, then fully mix and stir this mixture with propanol and water at a molar ratio of 1:40:3, and use 3mol / L of H 2 SO 4 Slowly drop the solution into the uniformly mixed solution, and change the dropwise addition while stirring, adjust the pH value of the solution to 1, and then keep stirring the prepared solution at 50°C for 10 hours to prepare a silica sol. According to the proportion of doping 5g zinc borate, 5g ammonium polyphosphate, and 5g nickel oxide per 1L of silica sol, dope the flame retardant and infrared blocking agent into the sol, mix thoroughly and evenly, and then adjust the pH value with ammonia solution to 6. The ceramic fiber felt was immersed in the doped silica sol, placed in a water bath at 40°C, and a silica composite gel was formed after 30 hours. Continue aging for 20 hours in a 60°C water bath. Take out the composite gel and replace it with propanol. The rati...
Embodiment 2
[0043] Mix and stir ethyl orthosilicate and diethyldiethoxysilane at a molar ratio of 1:6, then fully mix and stir the mixture, absolute ethanol and water at a molar ratio of 1:50:8 Uniformly, use 2mol / L HOOC-COOH solution to slowly drop into the uniformly mixed solution, add dropwise while stirring, adjust the pH value of the solution to 5, and then keep stirring the prepared solution at 50°C for 12 hours to obtain the Silica sol. According to the ratio of doping 10g of antimony oxide, 10g of melamine phosphate, and 10g of indium tin oxide per 1L of silica sol, dope the flame retardant and infrared blocking agent into the sol, mix thoroughly and evenly, and then adjust the pH value with ammonia solution to 6.3. The basalt fiber felt was immersed in the doped silica sol, placed in a water bath at 60°C, and a silica composite gel was formed after 8 hours. Continue aging for 24 hours in a 50°C water bath. The composite gel was taken out and replaced with absolute ethanol, th...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com