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47 results about "Scanning tunnel microscopy" patented technology

Low-temperature scanning tunneling microscope using closed-cycle refrigerator to achieve refrigeration

ActiveCN103901232ASolve the scarcity of consumption reservesSettle the priceScanning probe microscopyControl systemEngineering
The invention discloses a low-temperature scanning tunneling microscope using a closed-cycle refrigerator to achieve refrigeration. The low-temperature scanning tunneling microscope comprises a closed-cycle refrigerator system, a helium heat exchange gas refrigeration vibration isolation interface system, a low-temperature scanning tunneling microscope scanning head system, a vacuum system, a vibration reduction platform and a scanning tunnel microscope control system. According to the low-temperature scanning tunneling microscope, under the condition that no liquid helium is consumed, atomic-scale resolution low-temperature ultrahigh-vacuum scanning tunnel microscopy space imaging and high-energy resolution scanning tunnel spectrum accurate measurement can be achieved like a liquid helium refrigeration system. The technical scheme of closed-cycle refrigeration can also be used for other applications needing lower temperature and low-vibration environments like other members of scanning probe microscope families. Large-range temperature changes can also be achieved through feedback combination of heating elements and temperature measuring elements.
Owner:FUDAN UNIV

Preparation method for scanning probe of scanning tunneling microscope and control circuit

The invention provides a preparation method for a scanning probe of a scanning tunneling microscope and a control circuit. The method comprises: oxidation film removing processing is carried out on a probe; a rubber gasket sleeve the probe of the probe with the diameter of 0.5mm, wherein the distance between the bottom of the rubber gasket and the bottom of the probe is 2mm; a metal filament loop is placed into a KOH solution with the concentration of 2 to 3 mol/L and the bottom of the probe is inserted into the liquid surface at the depth of 1mm; the probe serves as an anode and the metal filament loop serves as a cathode and voltages of 5 to 12 V are applied to the two ends; and when a first voltage of the anode is equal to a second voltage on a fixed resistor of a control circuit, the control circuit cuts off the circuit and thus the point of a needle is formed at the bottom of the probe. Besides, the control circuit consists of a relay, a fixed resistor, a cathode, and an anode, wherein the relay and the fixed resistor are connected with a single-chip microcomputer in series and the cathode and the anode are connected by using an electrolyte. According to the invention, the aspect ratio is controlled and the gravity is increased by using the rubber gasket and the control circuit cuts off the power supply automatically and detects the voltages in real time, so that the ideal probe point with the proper aspect ratio and the clear scanning pattern can be prepared by using a one-step corrosion method.
Owner:CENT SOUTH UNIV

Controllable preparation method for realizing self-assembled nano-flowers of p-type laminar gallium telluride nano-sheets

InactiveCN107021784AAchieve high-quality self-assembly synthesisOvercome the shortcoming of easy compoundingPhysical/chemical process catalystsZinc oxides/hydroxidesHeterojunctionPhotoluminescence
The invention discloses a method for controllably preparing self-assembled nano-flowers of p-type laminar gallium telluride nano-sheets under normal pressure. The method comprises the following process steps: a) preparing one layer of ZnO thin film with a nano-flower shape on a sapphire substrate and taking the ZnO thin film as a seed layer in a growth process of GaTe; b) putting a prepared precursor sample into a tubular furnace and forming the GaTe in a normal-pressure and high-purity argon gas environment; c) testing a synthesized material by utilizing characterization methods including a scanning tunneling microscope, Raman, photoluminescence, an atomic force microscope, a transmission electron microscope and the like. The shape of the GaTe gallium is controlled through the shape and growth conditions including time length, argon gas flow, temperature and the like of ZnO; the preparation of ZnO nano-flowers is controlled through adjusting conditions including gas flow, temperature and the like. The method is efficient and the synthesis is controllable; a heterojunction structure of the prepared GaTe/ZnO nano-flowers has a remarkable pn junction rectifying effect and can be used for producing hydrogen through photoelectric catalysis and the like; furthermore, the reference is also provided for the growth of a novel two-dimensional material GaTe.
Owner:SUN YAT SEN UNIV

Automated atomic scale fabrication

A method for autonomously applying a dangling bond pattern to a substrate for atom scale device fabrication includes inputting the pattern, initiating a patterning process, scanning the substrate using a scanning probe microscope (SPM) to generate an SPM image of the substrate, feeding the SPM image into a trained convolution neural network (CNN), analyzing the SPM image using the CNN to identify substrate defects, determining a defect free substrate area for pattern application; and applying the pattern to the substrate in that area. An atom scale electronic component includes functional patches on a substrate and wires electrically connecting the functional patches. Training a CNN includes recording a Scanning Tunneling Microscope (STM) image of the substrate, extracting images of defects from the STM image, labeling pixel-wise the defect images, and feeding the extracted and labeled images of defects into a CNN to train the CNN for semantic segmentation.
Owner:QUANTUM SILICON INC

Method and device for realizing atomic-scale laser pumping detection

The invention discloses a method and device for realizing atomic-scale laser pumping detection. The method comprises the steps of triggering a first laser to emit a first laser pulse and a second laser to emit a second laser pulse based on an electric pulse, and adjusting the delay time between the first laser pulse and the second laser pulse; editing the waveform of the electric pulse to modulatethe delay time; combining and collimating the first laser pulse and the second laser pulse and irradiating an object to be detected; detecting the tunneling current signals of the irradiated object to be detected; and extracting a signal related to the delay time in the tunneling current signals. According to the invention, while signal modulation is realized, the laser average power in unit timeis ensured to be constant; therefore, the influence of the heat effect on a scanning tunneling microscope can be eliminated; the combination of the laser pumping detection technology and the scanningtunneling microscope technology is realized; and the atomic-scale spatial resolution and the nanosecond-scale time resolution can be obtained at the same time.
Owner:PEKING UNIV

Tube-type approximation and imaging unit mechanical tandem type scanning tunneling microscope body

The invention relates to a tube-type approximation and imaging unit mechanical tandem type scanning tunneling microscope body. The tube-type approximation and imaging unit mechanical tandem type scanning tunneling microscope body comprises a base, a sliding rod, a sleeve and a spring piece, and is characterized by further comprising a first piezoelectric tube, a second piezoelectric tube and a probe bracket, wherein one end of the first piezoelectric tube is fixed on the base, and the other end is connected and fixed to the second piezoelectric tube in a tandem manner in the axial direction; the sleeve is concentrically and coaxially fixed to the deformation free end of the second piezoelectric tube; the spring piece exerts pressure in the radial direction of the sleeve to clamp the sliding rod to the inner wall of the guide rail; the sliding direction of the sliding rod is in the axial direction of the sleeve; and the probe bracket and the second piezoelectric tube are concentricallyand coaxially arranged, and one end of the probe bracket is fixed to a tandem connection position of the first piezoelectric tube and the second piezoelectric tube. The tube-type approximation and imaging unit mechanical tandem type scanning tunneling microscope body is highly compact in radial and axial structures, the second piezoelectric tube is further used for approximating low starting voltage capable of realizing a needle sample approximation step, high rigidity of the scanning unit is ensured, the main body is made of an insulating material, the cross section of the structure is free of a conductive loop, and the tube-type approximation and imaging unit mechanical tandem type scanning tunneling microscope body is particularly suitable for extreme physical conditions of extremely low temperature, strong / fast changing magnetic field and strong vibration.
Owner:HEFEI INSTITUTES OF PHYSICAL SCIENCE - CHINESE ACAD OF SCI

Transfer vacuum sample holder and vacuum interconnection system

PendingCN113884698AAchieve deliveryRealize vacuum interconnectionMaterial analysisSmall sampleEngineering
The invention discloses a transfer vacuum sample holder. The sample holder comprises a second holder body assembly and a thermocouple, wherein the second holder body assembly is provided with a containing groove and a pair of second inserting grooves formed in the two opposite sides of the containing groove, and the two second inserting grooves are the same in extending direction and communicate with the containing groove; the thermocouple is fixed on the second holder body assembly and is positioned at a first end of an accommodating groove; the thermocouple extends to a lower part of the accommodating groove and is used for being in contact with a small sample holder when the two sides of the small sample holder in the width direction are inserted into second inserting grooves from second ends of the accommodating groove. The invention further discloses a vacuum interconnection system. The transfer vacuum sample holder has the function of allowing the small sample holder to be inserted and fixed, can be applied to a near-normal-pressure scanning tunneling microscope and a low-temperature scanning tunneling microscope at the same time, and can enable the thermocouple to be in automatic contact with the small sample holder after the small sample holder is inserted into the transfer vacuum sample holder, so detection of the temperature of a sample is achieved; transfer and vacuum interconnection of samples between two different scanning tunneling microscopes are realized.
Owner:SUZHOU INST OF NANO TECH & NANO BIONICS CHINESE ACEDEMY OF SCI

Scanning probe and preparation method thereof

PendingCN111157767AImplement atomic force feedback mechanismStable outputScanning probe microscopyFeedback controlNanotechnology
The invention provides a novel scanning probe for a novel scanning tunneling microscope and a preparation method thereof. The scanning probe comprises a probe body. The probe body comprises a probe tip and a micro-cantilever bearing the probe tip, the micro-cantilever being provided with an upper surface and a lower surface corresponding to the upper surface, and the probe tip being connected to the position, close to the end, of the upper surface of the micro-cantilever; a metal conductive layer covering the upper surface of the micro-cantilever and the probe tip; an insulating layer coveringthe metal conductive layer; and a metal reflecting layer covering the lower surface of the micro-cantilever. The novel scanning probe is formed by introducing the insulating layer, feedback control over whether the scanning probe makes contact with a sample or not, the contact distance and the like can be achieved through atomic force, and the application field of the scanning tunneling microscope is widened.
Owner:上海新克信息技术咨询有限公司

United measuring system and its measuring technology for scanning channel microscope and scanning micro electrode

It relates to a scanning tunneling microscope and scanning microelectrode combined measurement system and technology, comprising a scanning tunneling microscope (STM) measurement platform, a scanning microprobe and a control / drive unit; a tunneling current signal and a micro-area potential signal measurement unit and measurement signals control and processing unit. The scanning microprobe is used to detect the surface tunnel current and the surface potential distribution simultaneously, and the scanning measurement mode is exchanged by piezoelectric microscanning and stepping motor mechanical scanning, and the tunneling current is used as an indication that the scanning microelectrode reaches the surface of the sample, and the scanning is realized. Quantitative control of the distance between the tip of the microelectrode and the surface of the sample can significantly improve the spatial resolution of the distribution measurement of the electrochemical corrosion potential of the surface micro-area. The system can simultaneously measure nanometer-resolution surface topography images and surface micro-area electrochemical activity distribution images, and realize the interrelated research on surface topography structure-chemical activity. Provide an open platform for multiple surface spatially resolved measurement technologies that combine each other, complement each other, and correlate research.
Owner:XIAMEN UNIV

Shape-controllable Scanning Tunneling Microscope Tip Preparation System

The invention relates to a scanning tunnel microscope, in particular to a morphology controllable scanning tunnel microscope needle point preparation system. The system comprises a corrosion platform,a working circuit, and control software, and can be used for preparing various needle points for STM tests. The corrosion platform comprises an electrolytic tank filled with corrosive liquid, a probepositioning mechanism used for fixing and adjusting the position of a metal wire and a monitoring platform capable of observing the change of the shape of the needle point in the corrosion process inreal time; the working circuit supplies power to the electrolytic tank, and meanwhile, acquires the voltage signals of the needle point, and feeds back to the computer control software, and a stepping motor is controlled by a motor driving circuit to complete feeding and lifting motions of the probe; the control software controls a programmable power supply to output currents in different changemodes and timely cuts off the power supply when the needle point is pulled off according to the voltage signal fed back by an acquisition card, so that the stepping motor is triggered to extract the needle point. The controllable operation of the dynamic corrosion process is realized based on real-time control, real-time observation and feedback, so that a needed needle point for the STM with different morphologies can be prepared.
Owner:XIAMEN UNIV

Method of metallic clusters fabrication with desired size using scanning tunneling microscopy tip induced reactions

A method of transferring a single metal atom from a first location to a second location on the surface of a metal oxide is disclosed. The method includes obtaining a material having a first metal atom deposited on a first oxygen atom vacancy of the metal oxide and transferring the first metal atom of the metal on the first oxygen atom vacancy to a second location on the metal oxide by applying a voltage to the first metal atom. The second location can be a second metal atom on a second oxygen atom vacancy of the metal oxide, where the first and second metal atoms form a first metal atom second metal atom species, or a metal atom of the metal oxide, where the first metal atom and the metal atom of the metal oxide forms a first metal atom metal atom of the metal oxide species.
Owner:UCL BUSINESS PLC +1

Needle tip transfer support of scanning tunneling microscope

The invention provides a needle tip transfer support of a scanning tunneling microscope; the needle tip transfer support comprises: a first unit that includes a first surface and a second surface, andthe transmission mode of the first unit comprises horizontal transmission; the base that is located on the first surface and connected with the first unit, the base comprises a first through hole anda second through hole, the diameter of the first through hole is larger than that of the second through hole, the center line of the first through hole coincides with the center line of the second through hole, and therefore a limiting step face is formed between the first through hole and the second through hole; an elastic member that comprises a top, a bottom and an elastic fixing part, wherein the top makes contact with the limiting step face, the bottom makes contact with the first surface, and the horizontal section distance of the elastic fixing part is smaller than the diameter of thesecond through hole. And the scanning tunneling microscope needle tip support is fixed through the elastic fixing part. Operations such as transmission, in-situ treatment and replacement of the needle tip in an ultrahigh vacuum combined system can be realized, and impurity pollution under the atmosphere is avoided.
Owner:SHANGHAI INST OF MICROSYSTEM & INFORMATION TECH CHINESE ACAD OF SCI

Single-layer or several-single-layer CrTe3 film and preparation method thereof

The invention discloses a single-layer or several-single-layer CrTe3 film and a preparation method thereof. The thin film is of a single structure phase and is a magnetic semiconductor two-dimensional material, and the surface of the thin film shows a characteristic zigzag structure under a scanning tunneling microscope. According to the preparation method of the single-layer CrTe3 thin film, the single-layer CrTe3 thin film is prepared in a vacuum cavity by adopting a molecular beam epitaxy method. The single-layer CrTe3 thin film is easy to prepare, high in quality, uniform in component and smooth in surface. The invention further provides application of the single-layer CrTe3 thin film in a spinning electronic device, and the single-layer CrTe3 thin film has important application on miniaturization of the electronic device.
Owner:UNIV OF SCI & TECH OF CHINA

A controllable preparation method for self-assembled nanoflowers of p-type layered GaTe nanosheets

InactiveCN107021784BAchieve high-quality self-assembly synthesisOvercome the shortcoming of easy compoundingPhysical/chemical process catalystsZinc oxides/hydroxidesHeterojunctionPhotoluminescence
The invention discloses a method for controllably preparing self-assembled nano-flowers of p-type laminar gallium telluride nano-sheets under normal pressure. The method comprises the following process steps: a) preparing one layer of ZnO thin film with a nano-flower shape on a sapphire substrate and taking the ZnO thin film as a seed layer in a growth process of GaTe; b) putting a prepared precursor sample into a tubular furnace and forming the GaTe in a normal-pressure and high-purity argon gas environment; c) testing a synthesized material by utilizing characterization methods including a scanning tunneling microscope, Raman, photoluminescence, an atomic force microscope, a transmission electron microscope and the like. The shape of the GaTe gallium is controlled through the shape and growth conditions including time length, argon gas flow, temperature and the like of ZnO; the preparation of ZnO nano-flowers is controlled through adjusting conditions including gas flow, temperature and the like. The method is efficient and the synthesis is controllable; a heterojunction structure of the prepared GaTe / ZnO nano-flowers has a remarkable pn junction rectifying effect and can be used for producing hydrogen through photoelectric catalysis and the like; furthermore, the reference is also provided for the growth of a novel two-dimensional material GaTe.
Owner:SUN YAT SEN UNIV

Preparation method of water supramolecular motor

The invention discloses a preparation method of a water supramolecular motor. The method comprises steps that S1, highly-oriented pyrolytic graphite is adhered to a conductive metal plate by using low-temperature conductive silver adhesive, degassing is performed, then water molecules are deposited on a surface of the highly-oriented pyrolytic graphite in situ by using a microleakage valve at thetemperature of 90-110K, and self-assembling is performed to form a water cluster and a water molecular chain; S2, a graphite sample adsorbed with the water molecules is moved into a scanning tunnel microscope, the working environment is ultra-high vacuum, the temperature is 77 K, a needle tip of the scanning tunnel microscope is arranged above the water cluster, a voltage pulse is applied to inject tunneling electrons into the water cluster, and a negative electricity water cluster is formed; and S3, the negative electricity water cluster attracts a water molecular chain through electrostaticinteraction, the water molecular chain rotates clockwise or anticlockwise around the negative electricity water cluster under the driving of tunneling electrons, and the water supramolecular motor with the negative electricity water cluster as a stator and the water molecular chain as a rotor is obtained. The method is advantaged in that the water supramolecular motor can be prepared on a solid surface.
Owner:SOUTHWEST UNIVERSITY
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