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52 results about "Petroleum processor" patented technology

The crude oil distillation unit (CDU) is the first processing unit in virtually all petroleum refineries. The CDU distills the incoming crude oil into various fractions of different boiling ranges, each of which are then processed further in the other refinery processing units.

Deep desulfurization method for diesel by coupling of oxidation and extraction

The invention relates to a deep desulfurization method for diesel by coupling of oxidation and extraction, that is a catalyzed oxidation desulfurization method for diesel in petroleum refining technologies. The method comprises the following steps of crushing and fine grinding a zirconium hydroxide carrier, dipping into impregnation liquid formed by aqueous ammonium meta-tungstate solution, placing the impregnation liquid in an ultrasonic generator to carry out ultrasonic facilitating impregnation, boiling off water after the impregnation is finished, drying and baking at high temperature to obtain a WO3 / ZrO2 super solid acidic catalyst; adding aqueous hydrogen peroxide solution, extraction solvent and the WO3 / ZrO2 super solid acidic catalyst in diesel containing sulfur, carrying out catalyzed oxidation desulfurization reaction under the action of power ultrasonics, cooling to the room temperature after the reaction is finished, separating and recycling the solid catalyst, standing and layering, wherein the upper layer is desulfurized diesel and the lower layer can be reused after regeneration. The invention has simple process, mild condition, high desulfurization degree and gasoline recovery, low cost and no pollution to environment and can obtain ultra-low sulfur clean diesel products.
Owner:YANGZHOU UNIV

Pseudomonas sp. XQ23 capable of efficiently degrading multiple phenolic compounds

The invention discloses a pseudomonas sp. XQ23 capable of efficiently degrading multiple phenolic compounds. The strain of the pseudomonas sp. XQ23 is separated and purified from sludge which is seriously polluted by phenols. The strain has been preserved in China Center for Type Culture Collection since August 8th, 2009, and the preservation No. is CCTCC M 209175. The invention belongs to the technical field of environmental protection, and especially aims to the degradation problem of phenolic compounds in phenol-containing sewage generated in the petroleum refining process. Ten phenolic compounds, such as phenol, methyl phenol and the like, generally account for more than 97% of the total phenol content in the phenol-containing sewage. The strain is inoculated to the water body which contains one, or some or all of the ten phenolic compounds, and necessary inorganic salts are added; and while controlling the reaction temperature at 30+ / -2 DEG C and the controlling initial pH value to 7.0+ / -0.2 during degrading, the strain can completely degrade the phenolic compounds within shorter time under aerobic conditions.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Complex sulfurization and denitrification method for distillate

The invention discloses a complex sulfurization and denitrification method for distillate in petrochemical industry and petroleum refining technology. Through the method, sulfides and nitrides are removed from gasoline, diesel oil and other light oil distillate and the oil quality is improved. The technical scheme comprises the following steps of: filling a complexing agent anhydrous AlCl3 and the distillate in a reactor according to a mass ratio of sulfur and nitrogen elements in the distillate to AlCl3 of 0.012-0.120; adding water serving as a complexing aid, wherein the mass ratio of the water to the AlCl3 is 0.08-0.12; carrying out complex reaction at the temperature of between 50 and 80 DEG C for 50 to 70 minutes; after the reaction is finished, making the distillate stand to split phase, wherein the standing time is 10 to 20 minutes; and finally, taking an upper oil phase out, and adding 0.5 to 2.0 volume percent of water to clean residual complex in the oil so as to prepare the refined distillate. The method has the advantages of mild reaction condition, low operating cost, simple technical flow, low equipment investment, good sulfurization and denitrification effects, and use for removing sulfides and nitrides from the distillate in the petroleum refining technology.
Owner:SOUTHWEST PETROLEUM UNIV

Fractionating tower liquid level adaptive control method in petroleum refining process

The invention discloses a fractionating tower liquid level adaptive control method in a petroleum refining process. In the method, a reverse error neural network and an extreme value optimization method are adopted as adaptive tools, and the input and output quantities of an actual operation process are combined to design a predictive PI control strategy. A data acquisition device is firstly usedto collect the past input and output quantities of the system, and then an extreme value optimization algorithm is designed as a solver to adjust a neural network weight in an online mode so as to train the neural network high-efficiently and accurately. After a set error constraint is satisfied, the trained neural network weight is taken as the identification parameter of the system, a system model that is close to an actual situation is established, and finally, predictive PI control is designed to control the fractionating tower liquid level of in the petroleum refining process. By using the method, the interference of a model mismatch system can be effectively alleviated, control performance is increased, and simultaneously, the application of advanced control in industrial process control is promoted.
Owner:DONGHUA UNIV

Method and device of heavy oil two stage catalytic cracking reforming and gasoline upgrade coupling

The invention is a two-stage heavy oil catalytic cracking conversion method and device, belonging to petroleum refining process and device technical field, separating heavy oil reaction course into top and bottom reacting regions, making raw oil and regenerated catalyst firstly contact and react with each other in the bottom reacting region and successively separating the carbon deposit deactivated catalyst from reacting oil; making the oil gas go up into the second reacting region to mix with the catalyst used in gasoline reaction and continue reaction; a heavy oil reactor is connected in parallel with gasoline reacting part; the gasoline and catalyst complete reaction in the gasoline reactor and then make gas-solid separation in gasoline settler, where the oil gas is discharged through pipeline and the extracted catalyst is fed into pre-rising stages below the first and second heavy oil reacting regions to continue taking part in heavy reaction; a catalyst return pipe is arranged between the pre-rising stages of the gasoline settler and gasoline reactor to make a part of catalyst used in gasoline reaction return to the bottom of the gasoline reactor, so as to take part in gasoline reaction. And it can obviously raise efficiency of heavy oil reactor, improve product quality and need not consume energy because of catalyst change.
Owner:石宝珍

Apparatus and method for producing road petroleum asphalt from ultra heavy oil

The invention discloses an apparatus and a method for producing road petroleum asphalt from ultra heavy oil, and belongs to the field of petroleum refining process. The apparatus comprises a first heat exchanger, wherein one end of the first heat exchanger is connected with a raw-material pump; the other end of the first heat exchanger is connected with a flashing tower, wherein the tower bottom of the flash tower is connected with a flash bottom pump; the flash bottom pump is connected with a second heat exchanger; the second heat exchanger is connected with a heating furnace; the heating furnace is connected with the bottom of a reaction tower; the top of the reaction tower is connected with a fractionating tower; the bottom of the fractionating tower is connected with a tower bottom pump; the tower bottom pump is connected with the heating furnace; the heating furnace is connected with a vacuum tower; and the vacuum tower is connected with a residual oil pump. Visbreaking of the ultra heavy oil can be realized and heavy traffic paving asphalt with good performance can be produced through process combination of visbreaking and vacuum distillation.
Owner:PETROCHINA CO LTD

High-temperature corrosion inhibitor for oilfield exploitation and petroleum refining process and preparation method of high-temperature corrosion inhibitor

ActiveCN106433781ASafe and Reliable ProductivitySafe and reliable operabilityDrilling compositionBorehole/well accessoriesPetrochemicalStearic acid
The invention belongs to the technical field of petrochemical equipment and particularly provides a high-temperature corrosion inhibitor for oilfield exploitation and a petroleum refining process. The high-temperature corrosion inhibitor is prepared from raw materials in parts by weight as follows: a raw material group A: 6-8 parts of ricinolic acid and 2-4 parts of stearic acid; a raw material group B: N-methyldiethanolamine, triethanolamine and industrial white oil, wherein the weight of N-methyldiethanolamine is 0.18-0.2 times that of the raw material group A, the weight of triethanolamine is 0.06-0.08 times that of the raw material group A, and the weight of the industrial white oil is 0.35-0.4 times that of the raw material group A. The high-temperature corrosion inhibitor has the corrosion inhibition rate of about 97% and has the advantages of being good in corrosion inhibiting effect, non-irritant, safe, reliable, safe and stable in the production use operation process, environment-friendly and the like. According to the preparation method, performance of the raw materials is comprehensively considered, and the high-temperature corrosion inhibitor with more stable performance and more excellent corrosion inhibition effects can be obtained.
Owner:徐文忠 +1

System for solving ultrahigh gas temperature of dynamic wave furnace of waste acid recycling device

The invention relates to the field of alkylation assorted waste acid recycling devices in the petroleum refining process and in particular relates to a system for solving ultrahigh gas temperature of a dynamic wave furnace of a waste acid recycling device. The system comprises a dynamic wave gas-liquid separator, a filler washing tower and an electric defogger which are connected through a pipeline; the system is characterized in that furnace gas firstly enter a dynamic wave exchange column; the dynamic wave exchange column is connected with one or more reversed injection pipes; a nozzle control valve is arranged on each reversed injection pipe and used for controlling the pressure of the reversed injection pipe; the reversed injection pipes are connected with the dynamic wave gas-liquid separator through a dynamic wave dilute acid pump; the furnace gas enters the dynamic wave gas-liquid separator and carries out gas-liquid separation, then the furnace gas enters the filler washing tower to be washed and cooled, finally the furnace gas enters the electric defogger and removes the residual acid fog. The system is capable of reducing the temperature of a furnace gas outlet of a dynamic wave scrubber, facilitating long-period and safe operation of the device, improving the treatment capacity of the device, reducing the dilute acid treatment capacity and reducing sewage treatment load and cost.
Owner:SHANDONG JINCHENG HEAVY OIL RES INST OFCHEM TECH

Process for improving absorption stability in petroleum refining process

The invention discloses a process based on improving absorption stability in the petroleum refining process, comprising the following steps: compressed rich gas cooling process, absorption process, reabsorption process, desorption process, gasoline stabilization process, and light and heavy gasoline separation process. This process can efficiently absorb the fractionated components, avoid the reaction caused by contact with each other, make the components stable and convenient for subsequent use, and solve the unreasonable design of the absorption process for the fractionated components in the existing refining process. The absorption effect is poor, and it is extremely unstable, which can easily lead to reactions between components, resulting in the problem of composition confusion.
Owner:陈飞

Treatment method for spent caustic soda

An embodiment of the present invention relates to a method for treating spent caustic soda generated from an oil refinery process, a petrochemical process, etc. through a process in which a series of treatment steps are integrated, wherein the method can constitute a process under a mild condition excluding high temperature and / or high pressure conditions and can be advantageous to a post treatment process since the amount of by-products is small.
Owner:SK ENERGY CO LTD (KR)

Quick-dry fog sealing layer material, and preparation method and application thereof

ActiveCN105542487AClosed maintenance time is shortenedIn situ pavingsOil processingOrganic solvent
The invention relates to a quick-dry fog sealing layer material, which is formed by the following components: 20wt percent to 40wt percent of asphalt-recycling agent, and 5wt percent to 25wt percent of complex solubilizer, wherein the asphalt-recycling agent is formed by deasphalted oil, heavy aromatic oil and additives; the additives are selected from at least one of the following compounds: dibutyl phthalate, epoxidized soybean oil, chlorinated methoxy fatty acid ester and parabens; the mass ratio of the deasphalted oil to the heavy aromatic oil to the additives is 1:0.1 to 1:0.05 to 0.5. The invention also relates to a preparation method and application of the quick-dry fog sealing layer material. According to the quick-dry fog sealing layer material, the heavy aromatic oil and the like during the petroleum refining process are utilized to form the asphalt-recycling agent so as to obtain the fog sealing layer material with high additional value, so that the quick-dry fog sealing layer material can play a role in preventing aging and regenerating on aged asphalt pavements. In addition, according to the quick-dry fog sealing layer material provided by the invention, the maintenance time at low temperature is only 2 to 4h, which is shortened by over half the time for sealing and maintaining of the existing fog sealing layer material.
Owner:EAST CHINA UNIV OF SCI & TECH

Circulating pump sealing oil and application thereof

The invention relates to a circulating pump sealing oil and application thereof. The circulating pump sealing oil comprises base oil and low-density blend oil, wherein the base oil is selected from at least one of hydrogenated coal-liquefaction solvent oil, hydrogenated heavy aromatic hydrocarbon oil and hydrogenated anthracene oil. The invention also relates to application of the circulating pump sealing oil for sealing pumps in the processes of making oil from coal and refining petroleum. The sealing oil in the invention has the advantages of simple production process, low processing cost, excellent quality and low production cost.
Owner:CHNA ENERGY INVESTMENT CORP LTD +1

Manganese, zirconium and titanium ternary composite catalytic wet oxidation catalyst for alkaline residue wastewater as well as preparation method and application of catalyst

The invention discloses a manganese, zirconium and titanium ternary composite catalytic wet oxidation catalyst for alkaline residue wastewater as well as a preparation method and an application of thecatalyst. The ternary composite catalyst is formed by supporting ruthenium, zirconium and titanium ternary composite metal on nano aluminosilicate crystals as a carrier. The preparation method of themanganese, zirconium and titanium ternary composite catalytic wet oxidation catalyst for alkaline residue wastewater is simple and easy to implement, the obtained manganese, zirconium and titanium ternary composite catalytic material has good catalytic action on catalytic wet oxidation treatment of high-concentration and refractory alkaline residue wastewater produced in the petroleum refining process, tests prove that the degradation efficiency is remarkably improved, the CODcr removal rate of the alkaline residue wastewater is increased by 41% or above as compared with the wet oxidation degradation effect without the catalyst under the same condition, and the catalyst has very good practicability.
Owner:JIANGSU OPEN UNIV

Vapor phase heat transfer oil and its preparation process

The invention discloses a gas-phase heat-conducting oil and a preparation process thereof. The gas-phase heat-conducting oil contains alkyl diphenyl and its isomer compounds. The preparation process of gas-phase heat transfer oil includes the following steps: 1. Raw material selection. The raw material selected in this step is the tower bottom material after the catalytic reforming unit in the petroleum refining process or the polyester production raw material p-xylene plant tower bottom material or pyrolysis production Hydrogenation feedstock for ethylene by-products. 2. Extraction of aromatics. In this step, chemical products such as benzene and xylene are obtained, and the remaining products are the primary raw materials for gas-phase heat transfer oil. 3. Precision rectification and purification. In this step, the preliminary raw materials obtained in step 2 are purified, and the fraction at 240°C-270°C is selected, and then the above fraction is sent to a high-efficiency precision rectification tower for further rectification, and the fraction at 252°C-258°C is cut. Narrow cut, ie the final vapor phase heat transfer oil product. This vapor phase heat transfer oil product can completely replace the existing but biphenyl-diphenyl ether products (for example: vp-1, DowthermA, ThermS, ThermS-300 and other foreign vapor phase heat transfer oils).
Owner:北京燕通石油化工有限公司

Wet-type purification equipment for petroleum refining

The invention relates to the technical field of petrochemical production equipment, and discloses wet purification equipment for petroleum refining. According to the technical scheme, the wet-type purification equipment for petroleum refining comprises a bottom plate and a fixing plate fixedly installed on the bottom plate, and a transverse plate parallel to the bottom plate is fixedly installed on the fixing plate. The wet-type purification equipment for petroleum refining further comprises: a spray head, wherein the spray head is movably arranged on the bottom plate; a reciprocating mechanism which is movably arranged on the bottom plate and is connected with the spray head; a lifting assembly which is connected with the reciprocating mechanism and is movably mounted on the bottom plate; and a driving mechanism which is connected with the reciprocating mechanism. Polluted gas generated in the petroleum refining process is efficiently purified, purification liquid and dust in the purification process can be automatically screened, the purification liquid can be recycled, the cost is greatly reduced, and safety and environment friendliness are achieved.
Owner:东营思达石油化工有限公司

Method and device of heavy oil two stage catalytic cracking reforming and gasoline upgrade coupling

The invention is a two-stage heavy oil catalytic cracking conversion method and device, belonging to petroleum refining process and device technical field, separating heavy oil reaction course into top and bottom reacting regions, making raw oil and regenerated catalyst firstly contact and react with each other in the bottom reacting region and successively separating the carbon deposit deactivated catalyst from reacting oil; making the oil gas go up into the second reacting region to mix with the catalyst used in gasoline reaction and continue reaction; a heavy oil reactor is connected in parallel with gasoline reacting part; the gasoline and catalyst complete reaction in the gasoline reactor and then make gas-solid separation in gasoline settler, where the oil gas is discharged through pipeline and the extracted catalyst is fed into pre-rising stages below the first and second heavy oil reacting regions to continue taking part in heavy reaction; a catalyst return pipe is arranged between the pre-rising stages of the gasoline settler and gasoline reactor to make a part of catalyst used in gasoline reaction return to the bottom of the gasoline reactor, so as to take part in gasoline reaction. And it can obviously raise efficiency of heavy oil reactor, improve product quality and need not consume energy because of catalyst change.
Owner:石宝珍

High-temperature corrosion inhibitor used in oil field exploitation and petroleum refining process and preparation method thereof

The invention belongs to the technical field of petrochemical equipment and particularly provides a high-temperature corrosion inhibitor for oilfield exploitation and a petroleum refining process. The high-temperature corrosion inhibitor is prepared from raw materials in parts by weight as follows: a raw material group A: 6-8 parts of ricinolic acid and 2-4 parts of stearic acid; a raw material group B: N-methyldiethanolamine, triethanolamine and industrial white oil, wherein the weight of N-methyldiethanolamine is 0.18-0.2 times that of the raw material group A, the weight of triethanolamine is 0.06-0.08 times that of the raw material group A, and the weight of the industrial white oil is 0.35-0.4 times that of the raw material group A. The high-temperature corrosion inhibitor has the corrosion inhibition rate of about 97% and has the advantages of being good in corrosion inhibiting effect, non-irritant, safe, reliable, safe and stable in the production use operation process, environment-friendly and the like. According to the preparation method, performance of the raw materials is comprehensively considered, and the high-temperature corrosion inhibitor with more stable performance and more excellent corrosion inhibition effects can be obtained.
Owner:徐文忠 +1

Anti-coking reaction kettle for petroleum refining

The invention relates to the technical field of reaction kettles, in particular to an anti-coking reaction kettle for petroleum refining, which comprises a bottom plate, and the top of the bottom plate is fixedly connected with two vertical plates for supporting and fixing; the reaction kettle body is used for refining petroleum; the motor is used for providing driving force; a shaking mechanism for improving the mobility of petroleum is mounted on the outer side of the reaction kettle body. When the reaction kettle works, the reaction kettle moves left and right to shake, so that the mobility of petroleum can be effectively improved; when the reaction kettle works, the reaction kettle rotates, so that petroleum in the reaction kettle can be uniformly refined; when the reaction kettle works, cokes on the inner wall of the reaction kettle can be cleaned in the petroleum refining process of the reaction kettle, so that normal petroleum refining can be effectively ensured.
Owner:姬雅妮

A method for self-adaptive control of fractionation tower liquid level in petroleum refining process

The invention discloses an adaptive control method for the liquid level of a fractionation tower in the petroleum refining process. In this method, the reverse error neural network and extreme value optimization method are used as adaptive tools, and the predictive PI control strategy is designed in combination with the input and output of the actual operation process. The present invention first uses the data acquisition device to collect the past input and output of the system, and then designs an extreme value optimization algorithm as a solver to adjust the weight of the neural network online, thereby efficiently and accurately training the neural network; after satisfying the set error constraints, The trained neural network weight is used as the identification parameter of the system, and a system model close to the actual situation is established. Finally, the predictive PI control is designed to control the liquid level of the fractionation tower in the process of petroleum refining. By adopting the method of the invention, the interference of model mismatch to the system can be effectively relieved, the control performance is improved, and the application of advanced control in industrial process control is also promoted.
Owner:DONGHUA UNIV

A kind of quick-drying mist sealing layer material and its preparation method and application

ActiveCN105542487BClosed maintenance time is shortenedIn situ pavingsOil processingOrganic solvent
The invention relates to a quick-dry fog sealing layer material, which is formed by the following components: 20wt percent to 40wt percent of asphalt-recycling agent, and 5wt percent to 25wt percent of complex solubilizer, wherein the asphalt-recycling agent is formed by deasphalted oil, heavy aromatic oil and additives; the additives are selected from at least one of the following compounds: dibutyl phthalate, epoxidized soybean oil, chlorinated methoxy fatty acid ester and parabens; the mass ratio of the deasphalted oil to the heavy aromatic oil to the additives is 1:0.1 to 1:0.05 to 0.5. The invention also relates to a preparation method and application of the quick-dry fog sealing layer material. According to the quick-dry fog sealing layer material, the heavy aromatic oil and the like during the petroleum refining process are utilized to form the asphalt-recycling agent so as to obtain the fog sealing layer material with high additional value, so that the quick-dry fog sealing layer material can play a role in preventing aging and regenerating on aged asphalt pavements. In addition, according to the quick-dry fog sealing layer material provided by the invention, the maintenance time at low temperature is only 2 to 4h, which is shortened by over half the time for sealing and maintaining of the existing fog sealing layer material.
Owner:EAST CHINA UNIV OF SCI & TECH

Smoke dust purification device for petroleum refining process

InactiveCN108526181ATo achieve the effect of adjusting the air intakeAvoid enteringDirt cleaningAir volumePetroleum
The invention discloses a smoke dust purification device for a petroleum refining process. A structure of the smoke dust purification device for the petroleum refining process comprises an air suctioncover, a device sealing cover, a smoke dust purification chassis, a control panel, anti-slip supporting legs, a control button, a power indicator light, a purification device shell, a fixing flange,a universal suction arm, and an air volume adjusting valve. The smoke dust purification device for the petroleum refining process realizes that the smoke dust purification device for the petroleum refining process is provided with the air volume adjusting valve, and smoke dust purification device for the petroleum refining process can adjust air inlet amount of the suction arm when being used, avoids excessive smoke entering the device to reduce purification quality, avoid impurities entering the inside of the device through the suction arm when not in use, effectively prolongs the service life of the device, and improves the practicality of the device.
Owner:谢云琼
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