The invention discloses a high-entropy
alloy fiber as well as a preparation method and application thereof, relates to an electrochemical catalyst and a preparation method thereof, and aims to solve the problems that an existing
platinum catalyst is high in price and low in
platinum reserve, and the electrochemical
catalysis performance and the stability need to be improved. The preparation method comprises the steps: 1, weighing
metal raw materials; 2,
smelting the
mixed metal raw materials into a
metal button
ingot by adopting a high-vacuum
electric arc smelting furnace, and then melting the button
ingot to form a master
alloy rod by suction
casting; 3, performing drawing treatment on the master
alloy rod by adopting melt drawing equipment to obtain alloy fibers; and 4, carrying out free dealloying treatment on the alloy fibers. After the high-entropy alloy
fiber is subjected to dealloying treatment, a porous structure is formed on the surface, the
overpotential of 230 mV can be achieved on electrochemical
oxygen evolution
catalysis, the Tafel slope is about 40, a good
catalysis effect is achieved, meanwhile, a good electrochemical
hydrogen evolution catalysis effect is achieved, and the
overpotential of
hydrogen evolution catalysis is about 180 mV.