Patents
Literature
Hiro is an intelligent assistant for R&D personnel, combined with Patent DNA, to facilitate innovative research.
Hiro

63 results about "Tenax" patented technology

Tenax is the brandname of Toho Tenax owned by Teijin for a carbon fiber. Tenax-7R is an adhesive particularly suited for welding plastics .

Method for simultaneously detecting plurality of volatile trace carbonyl compounds in atmosphere

The invention relates to a method for simultaneously detecting a plurality of volatile trace carbonyl compounds in the atmosphere. According to the method, a pentafluorobenzyl hydroxylamine (PFBHA) derivative standard sample of 18 carbonyl compounds (16 mono-carbonyl compounds and 2 dicarbonyl compounds) with a certain concentration is prepared. A sample is collected by a self-made glass sampling pipe of a Tenax-TA adsorbent coated by a suitable amount of the PFBHA and a sampling condition is determined; under the condition that the loading amount of the adsorbent is 50mg, the sampling effect is optimal when the coating amount of a derivation agent is 260nmol, the collection flow speed is 50mL / min and the sampling time is 3-5 hours. The method has good separation degree, high sensitivity and low detection limit; the variety of the detected carbonyl compounds is more; the thermal stability of an oxime derivative with the weak polarity, which is generated by reaction, is good; the method is applicable to GC / MS (Gas Chromatograph-Mass Spectrometer) analysis. Furthermore, the method is simple and feasible and can be used for detecting and analyzing atmosphere samples.
Owner:SHANGHAI UNIV

Systems and methods for detecting contaminants

The present invention relates to a system and method for sampling a gas flow to measure one or more contaminants within a semiconductor processing tool. The system includes a portable unit containing one or more dry traps, Tenax traps and, if desired, wet impingers. The unit is coupled to a gas flow in a clean room and the dry traps. Tenax traps and wet impingers measure contaminants contained in the gas supply for a determined sampling interval. When the sampling interval is done, the unit is sent to an analysis facility for processing.
Owner:ENTEGRIS INC

Systems and methods for detecting contaminants

The present invention relates to a system and method for sampling a gas flow to measure one or more contaminants within a semiconductor processing tool. The system includes a portable unit containing one or more dry traps, Tenax traps and, if desired, wet impingers. The unit is coupled to a gas flow in a clean room and the dry traps. Tenax traps and wet impingers measure contaminants contained in the gas supply for a determined sampling interval. When the sampling interval is done, the unit is sent to an analysis facility for processing.
Owner:ENTEGRIS INC

Plant source volatile organic matter test method

The invention relates to the technical field of the analysis testing method, in particular to a testing method for a plant source volatile organic matter; a sampling tube uses Tenax-TA, Carboxed 1000 and Carbosieve SIII as filling materials for filling; the volatile organic matter is absorbed in the sampling tube and carries out thermal desorption by two times through a secondary thermal desorption instrument; the desorption gas enters a gas chromatograph for separation and measurement with the carrier gas by being coupled on-line from the thermal desorption instrument; the invention adopts three different filling materials, expands the absorbing range of the sample, guarantees the complete collection of the sample, holds high separation capacity for chromatographic peak by adopting a capillary chromatographic column and can not cause the widening of the chromatographic peak; in the process of collecting and analyzing samples, the water disturbance is eliminated and the analysis capacity to the compound is strengthened; low temperature or cooling equipment is not needed, the analysis cost is reduced, the sensitivity of the sample analysis is improved, and the analysis requirement of the plant source volatile organic matter is met, thus reaching the T0-17 standard of an EPA method.
Owner:SHENYANG INST OF APPL ECOLOGY CHINESE ACAD OF SCI

Preparation method of metal carrier Tenax coating stirring and extracting rod

The invention relates to a preparation method of a metal carrier Tenax coating stirring and extracting rod, which comprises the following steps of: a, selecting and preprocessing a metal rod; b, synthesizing heat-resistant epoxy resin; c, manufacturing a stirring rod coating; d, curing the coating; and e, removing impurities of the extracting rod body, wherein the extracting rod is used in a stirring manner, and the metal is iron, nickel, cobalt, stainless steel or alloy; and when the extracting rod is used in a headspace or ultrasonic manner, the metal is stainless steel, copper, aluminum or alloy. Tenax is fixed on the surface of the metal rod by using the synthesized heat-resistant epoxy resin or organic silicon resin to form a coating material with heat stability and solvent washing resistance, thus the extracting rod realizes the enrichment of trace organic matters. The invention is especially suitable for processing samples of soil, air, essence and spice, indoor air, alcohol, phenol, amine-aldehyde, ketone, aryl halides and the like.
Owner:TIANJIN CHUNFA BIO TECH GRP

Method for analyzing contents of three different occurrence forms of organic pollutants in soil

ActiveCN105548389ASolve the problem that the degree of pollution is not scientific enoughComponent separationTenaxPretreatment method
The invention relates to a soil contaminant detection method in the field of environment analysis, specifically to a method for analyzing the contents of three different occurrence forms of organic pollutants in soil. Directed at the problem that conventional methods which usually evaluate the contamination degree of soil on the basis of the total concentration of organic pollutants is not scientific enough, the method provided by the invention employs a pretreatment method consisting of Tenax resin adsorption, extraction with an organic solvent, alkaline and thermal hydrolysis and re-extraction with the organic solvent for graded extraction and cooperatively uses gas chromatography, combined gas chromatography and mass spectrometry, liquid chromatography and liquid chromatographic-gas chromatographic apparatus detection and analysis technology, so the contents of three different occurrence forms, including a soluble form, an adsorption form and a bound form, of organic pollutants in soil are detected. The method provided by the invention can accurately and quantitatively analyze the contents of the three different occurrence forms of organic pollutants in soil and has good application value in soil contamination risk evaluation and pollution abatement and restoration.
Owner:NANJING UNIV

Method of taking Tenax as simulant to measure migration amount from paper and volatile and semi-volatile organic matter in paperboard by TD-GC/MS

The invention relates to a method of taking Tenax as a simulant to directly measure a migration amount from paper and volatile and semi-volatile organic matter in a paperboard by TD-GC / MS, belongs to the technical field of analytic chemistry, and specifically relates to a volatile and semi-volatile compound of taking modified polyphenylene oxide (MPPO, Tenax) as the simulant to directly measure the migration amount by thermal desorption-gas chromatography / mass spectrometry(TD-GC / MS). The method comprises the following steps of: 1, preparing and packing simulated samples; 2, performing simulation test to the samples under testing conditions; 3, weighting the simulant and placing it into a sample hose, directly analyzing it by the TD-GC / MS method to gain the migration amount. Through the method, the special migration amount of the volatile and semi-volatile matter in the paper and the paperboard can be precisely measured so that the paper and the paperboard are improved in quality security. The method has the advantages of effectiveness, feasibility and convenient operation, the simulant can be directly analyzed and sampled without being in advance treated, thus it has the characteristics of high sensitivity, high recycling rate, excellent repeatability and promotion application value.
Owner:CHINA TOBACCO YUNNAN IND

Heat purge and trap instrument and heat purge and trap method

The invention relates to a heat purge and trap instrument, comprising a heating furnace, a sample furnace, a high-purity nitrogen gas cylinder, a transmission pipe sealably connected with the air outlet of the sample furnace, a trapping pipe sealably connected with the other end of the transmission pipe and a cooling cold trap with the trapping pipe sleeved therein. The invention also relates to a heat purge and trap method. The method successively comprises the following steps of 1. putting a to-be-tested sample in the sample furnace; 2. adsorbing materials with 80-mesh granular Tenax TA; 3. heating the sample furnace to a temperature of 180 DEG C-600 DEG C; 4. opening the high-purity nitrogen gas cylinder and the cooling cold trap, wherein the flow rate of the high-purity nitrogen gas is 20 mL / 80 min; the collecting time lasts for 30-60 minutes; and the cooling cold trap is kept at a temperature of -1.0 DEG C-15.0 DEG C. The heat purge and trap instrument and the heat purge and trap method are in no need of organic reagents and post-enrichment processes, and are suitable for the determination of volatile organic components in solid samples such as rocks, soils, coals and the like. Combined with GC / MS, the sensitivity for detecting alkane organic components is superior to 0.1 ng / g.
Owner:BEIJING RES INST OF URANIUM GEOLOGY

An integrated adsorption tube for benzene and total volatile organic compounds in indoor air and its detection method

The invention relates to an integrated adsorption tube for benzene and total volatile organic compounds in indoor air and a detection method thereof, comprising an adsorption tube capable of simultaneously collecting samples of benzene and total volatile organic compounds, and Tenax-TA Adsorbent, coconut shell activated carbon adsorbent and Tenax-TA adsorbent, the adsorption tube of the present invention can simultaneously sample benzene and total volatile organic compounds in indoor air, and can use the benzene data in the analysis results of total volatile organic compounds As the structure of benzene analyzed separately, the detection result has good reproducibility, the recovery rate of benzene and total volatile organic compounds is high, the detection cost is reduced, and the experiment is convenient.
Owner:CHANGZHOU ARCHITECTUAL RES INST GRP CO LTD

Method for testing content of 16 types of polycyclic aromatic hydrocarbon content in incense combustion smoke by thermal desorption/gas chromatography-mass spectrometry

The invention discloses a method for testing the contents of 16 types of polycyclic aromatic hydrocarbons in incense combustion smoke by a thermal desorption / gas chromatography-mass spectrometry. An incense combustion sample combusts in a space being 1.8 m*1.8 m*1.8 m; smoke is collected into a heat desorption pipe containing Tenax-TA filler through a sampling pump; after the heat desorption, GC-MS is used for detection in a selective ion mode (SIM); an external standard method is used for quantification. The result shows that the concentration of 16 types of polycyclic aromatic hydrocarbons shows a good linear relationship in a concentration range of 0.05 to 1.0 mg / L; the relative coefficient r is greater than 0.995; the method detection limit is 0.06 to 1.10 ng / m<3>; the average adding standard recovery rate is 89.2 to 100.7 percent; the relative standard deviation (RSD, n being equal to 6) is 1.7 percent to 5.0 percent. The method has the advantages that the 16 types of polycyclic aromatic hydrocarbons in the incense combustion smoke can be effectively subjected to qualitative and quantitative analysis; the characteristics of simplicity, high speed, high reliability and the likeare realized; the experiment requirements can be met.
Owner:广东省江门市质量计量监督检测所

Sampling device of gaseous contaminant in material crushing process

InactiveCN102103043AEffective monitoringEffectively monitor and obtainWithdrawing sample devicesHydrogenTenax
The invention discloses a sampling device of gaseous contaminant in the material crushing process, which comprises a crusher. The feeding hole of the crusher extends into a rotary barrel, and the discharge hole of the rotary barrel extends into a storing box. The storing box is communicated with a dust collecting cylinder, and the dust collecting cylinder is communicated with a draught fan through a dust removing bag. A draught fan is connected with a gas buffer pipe, and four sampling rubber pipes are fixed in the gas buffer pipe. The first sampling rubber pipe is connected with a first sampler through phenolic absorbing liquid, the second sampling rubber pipe is connected with the first sampler through brominated hydrogen absorbing liquid, the third sampling rubber pipe is connected with a second sampler through an activated charcoal absorbing pipe, and the fourth sampling rubber pipe is connected with the second sampler through a Tenax-GC pipe. Excess gas is exhausted from a gas diversion port. Aiming at gaseous contaminant possibly produced during crushing, the gas samplers are used for respectively sampling different materials at an exhaust port. The sampling device can ensure that the contaminant is effectively monitored and data information is obtained and has the advantage of simple structure.
Owner:TSINGHUA UNIV

Low-temperature gathering device and low-temperature gathering method capable of realizing synchronous gathering of H2/CH4/CO2/H2S

The invention relates to a low-temperature gathering device and a low-temperature gathering method capable of realizing synchronous gathering of H2 / CH4 / CO2 / H2S. The device comprises a liquid nitrogenpump, a sleeve pipe, a temperature probe, heating rods, adsorbing hydrazine and adsorbents, wherein the liquid nitrogen pump can pump liquid nitrogen into the sleeve pipe; the adsorbing hydrazine is inserted into the sleeve pipe; the heating rods are positioned at both sides of the adsorbing hydrazine; the temperature probe is connected with the adsorbing hydrazine; the adsorbents are filled in the adsorbing hydrazine and are divided into three layers; silica wool is arranged among all layers of the adsorbents; and the adsorbents are sequentially a glass bead, a Tenax adsorbent and active carbon from top to bottom. The adsorbing hydrazine is reduced to -145+ / -5 DEG C by the liquid nitrogen pump, so that four gases are respectively absorbed by the three adsorbents synchronously; and the adsorbing hydrazine is heated to 190+ / -5 DEG C, so that the synchronous desorption of the four gases. The invention has simple structure, is easy to realize and can synchronously gather and preconcentrate the four tracing gases in the ocean and provide convenience for the following online analysis work.
Owner:TONGJI UNIV

In-vehicle odor source detection method

PendingCN111766328ARealize odor traceabilityComponent separationOdor sourceTenax
The invention relates to the technical field of odor testing, and provides an in-vehicle odor source detection method. The method comprises the steps that a Tenax sampling tube is used for collectingan in-vehicle gas sample of a target vehicle, a first corresponding relation between a gas substance peak and retention time is obtained through a gas chromatograph-mass spectrometer for one part, anda second corresponding relation among odor intensity, odor types and retention time is determined through an olfactory discriminator for the other part; a first target gas substance in the in-vehiclegas sample is determined according to the first corresponding relationship and the second corresponding relationship; all the parts are put into a polyvinyl fluoride sampling bag, an experiment is carried out in an environment test cabin, a gas sample of each part is collected by using a Tenax sampling tube, and a second target gas substance of the gas sample of each part is determined; and the odor source part in the vehicle is determined according to the target gas substance of each part gas sample. According to the method, odor tracing of the target gas substance between the target vehicleand the internal parts can be achieved.
Owner:CRRC TANGSHAN CO LTD

Thermal desorption and sampling device for methyl mercury

InactiveCN104713966ASimplified thermal analysisSimplify operabilityComponent separationMethylmercuryTenax
The invention discloses a thermal desorption and sampling device for methyl mercury. The thermal desorption and sampling device comprises a flow meter and a thermal desorption device, wherein the thermal desorption device comprises a heating coil, a heating power supply, a heating switch and a heating power supply and voltage regulator; when an experiment for determining the content of the methyl mercury is carried out, an argon bottle is firstly opened; argon enters the lower end of the flow meter through a PFA gas pipeline, then flows out from the upper end of the flow meter, and enters a methyl mercury-enriched Tenax adsorption pipe through the PFA gas pipeline; and the heating coil sleeves the adsorption pipe. According to the thermal desorption and sampling device, carrier gas flow control and heating desorption devices are integrated; the thermal desorption and sampling device is simple in structure and convenient to operate; thermal desorption and sampling operation on the methyl mercury are greatly simplified; experiment efficiency is improved; and compared with devices with the similar functions, the thermal desorption and sampling device is extremely low in construction cost.
Owner:HENAN POLYTECHNIC UNIV

Method of utilizing Tenax as simulant with GCMS (Gas Chromatography Mass Spectrometry) to determine transfer volume of aromatic amine in paper and paperboard

The invention discloses a method for determining a transfer volume of aromatic amine in paper and a paperboard. The method comprises the following steps: taking the modified polyphenyl ether as a simulant, conducting solvent extraction on the simulant, concentrating the extract liquor, and carrying out the GC / MS method to determine the transfer volume. The steps and the method provided by the invention can be effectively used for determining the transfer volume of the specific aromatic amine which is transferred from the paper and the paperboard to the dry food simulant; the method is feasible, simple to operate, accurate in method, high in sensitivity, and of value for popularization and application.
Owner:CHINA TOBACCO YUNNAN IND

Medical electronic nose gas concentrating system, and method

The invention discloses a medical electronic nose gas concentrating system, and a method. The medical electronic nose gas concentrating system comprises a flow rate control unit, a temperature control unit, and an adsorption tube containing a mixed adsorbent. The mixed adsorbent is selected from CarbopackTMB and Tenax GR based on the adsorption capacity of gases; OD1 / 4inch, 7inch Length standard adsorption tube is adopted; and the adsorption tube contains the mixed adsorbent with a thickness ranging from 120 to 150mm; and a first grade Peltier cooling system is adopted by the mixed adsorbent. A gas concentration system is adopted by the medical electronic nose gas concentrating system, so that the detection capacity and capacity of resisting disturbance of the medical electronic nose with the gas concentrating system are both improved, a problem of the prior art that electronic noses can not be directly applied to respiratory gas disease diagnosis because of poor gas sensor detectability is solved, development of olfactory analogue technology of the state is promoted, the gap between the prior art and international advanced level is narrowed, disease early diagnosis is realized, and great practical significance is achieved.
Owner:胥勋涛

Measuring method of low-concentration odorous gas

The invention relates to a measuring method of low-concentration odorous gas, comprising the following steps: adsorption treatment: at the normal temperature of 20-25 DEG C, filling 100L of odorous gas into a glass tube filled with solid Tenax poly 2,6-diphenyl-p-phenvlene and activated carbon to completely adsorb odorous substances in the odorous gas; heat resolution treatment: heating the glass tube in the first step to a specific temperature, and resolving the adsorbed odorous substances again; blowing treatment: carrying out desorption on the odorous substances by 10L of carrier gas N2; mixing the odorous substances with N2; flowing out and collecting from the other end to obtain the odorous gas which is condensed by 10 times; measuring the concentration of the odorous gas concentrated by 10 times with a GB / T14675-93 three-point comparative smelly bag method; calculating to obtain the concentration of the odorous gas of the original odorous gas. By using the method of the invention, the low-concentration odorous gas is condensed to reach the range which can be measured by the existing three-point comparative smelly bag method. The measuring method of the invention has the advantages of no pollution, low cost, good deodorization effect and the like, is economic, convenient, quick and easy to realize, and is more suitable for measuring the concentration of the odorous gas under low-concentration environment.
Owner:TIANJIN ACADEMY OF ENVIRONMENTAL SCI

Method for detecting benzene and total volatile organic compounds in indoor air and sampling device

The invention discloses a method for detecting benzene and total volatile organic compounds in indoor air and a sampling device. The method comprises the following steps: 1) using an adsorption tube for air sampling, and controlling the temperature of the adsorption tube to be below 28DEG C by a temperature adjusting device, wherein an adsorbent filled in the adsorption tube comprises 60 to 80 mesh-Tenax-TA adsorbent; 2) resolving the adsorption tube in a resolver, and directly sending an analytical gas to a chromatograph for analysis; and 3) respectively calculating the content of the benzeneand the total volatile organic compounds by peak area quantification, retention time qualification, and area external standard method. The method can simultaneously detect the benzene and the total volatile organic compounds, overcomes the influence of ambient temperature, avoids a penetrating phenomenon, has high recovery rate, and is simple in operation, thereby effectively saving workload andcost.
Owner:广州市赛特检测有限公司

Fire coal combustion source discharged carbonyl compound sampling device

The invention discloses a fire coal combustion source discharged carbonyl compound sampling device. The sampling device comprises an air inlet part, a first-grade dilution system, a second-grade dilution system, a staying chamber and a sampling part. A combustion temperature can influence carbonyl compound gas-particle distribution and thus in order to simulate cooling, dilution and coagulation of flue gas discharged into air, the staying chamber is built and used after flue gas dilution. The sampling part adopts a self-made sampling tube coated with a pentafluorophenyl hydrazine (PFPH) Tenax-TA adsorbent to acquire a sample and utilizes a steam coating process and an introduction port thermal desorption analysis method so that solvent-caused influence on a detection result is avoided. The device is simple and easy, utilizes a dilution system to adjust a dilution ratio and is suitable for acquisition of other high-flue gas concentration gas substances.
Owner:SHANGHAI UNIV

Thermal desorption-gas phase separation-thermal pyrolysis system based on phenylated derived organic mercury

The invention discloses a thermal desorption-gas phase separation-thermal pyrolysis system based on phenylated derived organic mercury. The thermal desorption-gas phase separation-thermal pyrolysis system comprises a column box and a pressure-regulation and temperature-control switch box, wherein the pressure-regulation and temperature-control switch box is arranged at one end of the column box; the column box and the pressure-regulation and temperature-control switch box are provided with a thermal desorption assembly, a gas phase separation assembly, a thermal pyrolysis assembly and an assisting assembly; the thermal desorption assembly comprises a thermal desorption heating wire switch, a thermal desorption heating wire time control switch, a thermal desorption heating wire pressure regulator, a thermal analysis heating wire pressure regulator pressure-regulation knob, a thermal desorption heating wire and a Tenax adsorption pipe; the Tenax adsorption pipe is transversely mounted at the top of the column box; the thermal desorption heating wire is mounted at the outer part of the Tenax adsorption pipe. According to the thermal desorption-gas phase separation-thermal pyrolysis system disclosed by the invention, thermal desorption, gas phase separation and thermal pyrolysis parts are integrated, and methyl mercury and ethyl mercury in a sample can be effectively determined; compared with a traditional gas chromatograph, a programed temperature rising device has a smaller size, so that an experiment space is saved; meanwhile, programed temperature control can be realized, and temperature can be increased section by section.
Owner:OCEAN UNIV OF CHINA

Analysis method for reaction products of preparing ethylene glycol by ethylene oxide catalytic hydration

The invention relates to an analysis method for reaction products of preparing ethylene glycol by ethylene oxide catalytic hydration, which is mainly used for solving the problems of overlapped peak and furcation of chromatographic peak in the presence of a large amount of water as well as poor analysis result repeatability in the existing glycol, diethylene glycol and triethylene glycol analysistechnology. The technical scheme of the analysis method of the invention is as follows: a gas chromatograph is used to perform the analysis, wherein the reaction product passes through Tenax TA polymeric adsorbent before entering into the chromatographic column, and then the follow-up analysis is carried out; and the internal standard substance is a butyl cellosolve aqueous solution, thus the problems in the prior art can be preferably solved, and the analysis method can be used for tracking and analyzing the technological products for preparation of ethylene glycol by ethylene oxide catalytic hydration.
Owner:CHINA PETROLEUM & CHEM CORP +1

Two-section type gas sampling tube as well as preparation method and application thereof

The invention provides a two-section type gas sampling tube as well as a preparation method and application thereof. Tenax TA and a Carboxen 1000 carbon molecular sieve are selected as adsorbents to prepare the two-section type gas sampling tube, and the preparation method comprises the following steps: adding a copper net into a hollow tube of an adsorption tube, then adding glass wool, adding a Tenax TA adsorbent, adding glass wool for separation, then adding a Carboxen 1000 carbon molecular sieve, and finally adding glass wool and a copper net in sequence to fix the adsorbents in the tube, so as to obtain a finished product, wherein Tenax TA has relatively good adsorption performance on VOCs (Volatile Organic Compounds) with six or more carbon atoms. The Carboxen 1000 carbon molecular sieve has good adsorbability on VOCs with six or less carbon atoms, and the Carboxen 1000 carbon molecular sieve and the Tenax TA are combined for application, so that various volatile organic compounds released by plastics can be better collected, and the accuracy of qualitative and quantitative analysis of VOCs is improved.
Owner:JINAN UNIVERSITY

Method for measuring volatile organic compounds released by bag

InactiveCN108828083AAccurate determination of contentAvoid flaws that do not reflect the real situationComponent separationTenaxChemical compound
The invention relates to a method for measuring volatile organic compounds released by a bag. The method comprises sampling: putting a bag sample to be detected into a sampling bag, carrying out heating at 70+ / -10 DEG C for 3-6h so that the volatile organic compounds in the bag sample to be detected are released into the sampling bag and taking volatile organic compound samples from the sampling bag through a Tenax-TA sampling pipe, and detection: detecting TDS / GC / MS of the Tenax-TA sampling pipe after sampling. The method can accurately determine the content of the releasable volatile organiccompounds in the bag without destroying the samples to be tested, can greatly reduce the detection cost and is economical and environmentally friendly.
Owner:GUANGZHOU FIBER PROD TESTING & RES INST

Metal carrier stirring and extracting rod

The invention relates to a metal carrier Tenax coating stirring and extracting rod which uses metal as a carrier, wherein a coating contains a Tenax adsorbing agent, the extracting rod is used in a stirring manner, the metal is selected from iron, nickel, cobalt, stainless steel or alloy; and the extracting rod is used in a head space or ultrasonic manner, the metal is selected from stainless steel, copper, aluminum or alloy. The extracting rod is used for fixing the Tenax on the surface of the metal rod by using synthetic high-temperature epoxy resin or organic silicon resin to form a coating material with good heat stability and solvent rinsing resistance, thus trace organic matters are enriched. The invention is especially suitable for processing samples, such as soil, atmosphere, essence perfume, indoor air, alcohol, phenol, amine and aldehyde, ketone, aryl halides and the like.
Owner:TIANJIN CHUNFA BIO TECH GRP

Thermal desorption, gas-phase separation and thermal cracking system based on ethylation derivation of methyl mercury

The invention discloses a thermal desorption, gas-phase separation and thermal cracking system based on ethylation derivation of methyl mercury, comprising a thermal desorption part, a gas-phase separation part, a thermal cracking part, a gas flowmeter, a Teflon FEP pipeline and a pressure regulating and temperature control switch chamber, wherein the thermal desorption part comprises a thermal desorption heater strip switch, a thermal desorption heater strip time control switch, a thermal desorption heater strip pressure regulator, a pressure regulating knob of the thermal desorption heater strip pressure regulator, a thermal desorption heater strip and a Tenax adsorption pipe; the gas-phase separation part comprises a heater jacket, a heater jacket switch, an OV-3 packed column and a heater jacket temperature control plate; and the thermal cracking part comprises a thermal cracking heater strip switch, a thermal cracking heater strip time control switch, a thermal cracking heater strip pressure regulator, a pressure regulating knob of the thermal cracking heater strip pressure regulator, a thermal cracking heater strip and a quartz pipe. The system realizes the aim of integration of thermal desorption, gas-phase separation and thermal cracking devices, and simultaneously, each part can be individually operated, thereby saving the analysis time, having low manufacturing cost and greatly reducing experiment cost.
Owner:OCEAN UNIV OF CHINA

Method for testing harmful volatile matters of non-metallic material of passenger vehicle

PendingCN111505136ASolve pollutionAccurately lock the sourceComponent separationTenaxHazardous substance
The invention discloses a method for testing harmful volatile matters in a non-metallic material of a passenger vehicle. The method comprises the following steps: putting a non-metal material into a sampling bag; arranging a blank sampling bag with the same specification; separating harmful volatile substances from an adsorption object to be detected through heating; collecting benzene substancesthrough a TENAX sampling tube; extracting benzene substances in the TENAX sampling tube through a thermal desorption system; introducing the benzene substances into a gas chromatography-mass spectrometer; obtaining a quantitative value of each benzene substance through a benzene substance analysis curve; and collecting aldehyde ketone substances through a DNPH sampling tube, eluting the DNPH sampling tube through acetonitrile to prepare an aldehyde ketone substance reagent, guiding the aldehyde ketone substance reagent into a high performance liquid chromatograph-diode array detector, obtaining quantitative values of the aldehyde ketone substances through an aldehyde ketone substance analysis curve, and finally obtaining the concentration of harmful volatile substances through calculation.By detecting the concentration of harmful substances volatilized from various non-metallic materials, the unqualified automotive trim assembly is locked, and targeted improvement is achieved.
Owner:FAW CAR CO LTD

Detection method for real-time continuous monitoring of release of volatile organic compounds in plastic runway and application of detection method

InactiveCN107085052ANot brokenNot affected by pollutionComponent separationTenaxAir velocity
The invention belongs to the technical field of environmental monitoring, and discloses a detection method for real-time continuous monitoring of release of volatile organic compounds in a plastic runway and application of the detection method. The method comprises the following steps: (1) putting a sample to be detected into an experimental cabin, and setting temperature and relative humidity of the experimental cabin, air velocity on the surface of the sample and an air replacement rate; (2) after putting the sample, collecting air in the cabin by a constant current sampler, and enabling the extracted air to pass through a Tenax TA adsorption tube; (3) gas chromatography-mass spectrometry detection: fixing the Tenax TA adsorption tube to a two-stage thermal desorption instrument, after thermal desorption, enabling the volatile organic compounds to enter gas chromatography-mass spectrometry for detection, and performing qualitative and semi-quantitative analysis according to an area normalization method. The detection method can be used for simultaneously performing qualitative and semi-quantitative determination on multiple volatile organic compounds, and can be applied to detection of the volatile organic compounds in fields such as plastic runway, automobile seats and furniture.
Owner:中科检测技术服务(广州)股份有限公司 +1

Novel thermal desorption adsorption tube

InactiveCN109632402AHigh recovery rate of adsorption heat desorptionEasy to makeComponent separationWithdrawing sample devicesFiberActivated carbon
The invention discloses a novel thermal desorption adsorption tube, which adopts activated carbon fibers with wide industrial application as a filler, and belongs to the technical field of atmosphericenvironment monitoring. The novel thermal desorption adsorption tube is designed according to an ambient air toxic organic compound determination method TO-17 in a VOCs (Volatile Organic Compounds) monitoring method system proposed by the United States Environmental Protection Agency, which can effectively collect volatile halogenated hydrocarbons, and is significantly higher in collection efficiency for the VHCs than a Tenax TA tube. The novel thermal desorption adsorption tube can replace the Tenax TA tube to serve as a VOCs sample collection and adsorption tube, and is used for sampling the analyzing the VHCs in the atmosphere and effectively evaluating the concentration level of the VHCs in the ambient air.
Owner:DALIAN UNIV OF TECH

Method for testing transfer volumes of volatile and semi-volatile organic matters in paper and paperboard by taking Tenax as simulant by virtue of HS-GC/MS

The invention relates to a method for testing transfer volumes of specific volatile and semi-volatile organic matters in paper and a paperboard, belongs to the technical field of analytic chemistry, and particularly relates to the method for directly testing transferred volatile and semi-volatile compounds by taking Tenax as the simulant by virtue of a headspace gas chromatography-mass spectrometry (HS-GC / MS). The method comprises the following steps: (1) preparing a simulation sample, assembling, and covering the surface of a to-be-tested object with the Tenax; (2) simulating the assembled sample in a normal drying oven under a temperature testing condition for required time; (3) directly analyzing a simulant by virtue of the HS-GC / MS, so as to obtain the transfer volumes. The method can be used for effectively testing the transfer volumes of the specific volatile and semi-volatile organic matters in the paper and the paperboard, is feasible, easy to operate, accurate and sensitive and has popularization and application values.
Owner:CHINA TOBACCO YUNNAN IND
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products