The invention relates to a preparation method of
boron nitride /
sialon composite material by adopting
boron-rich
slag. The preparation method comprises two steps: the first step is that synthesis
sialon powder BN / (Ca, Mg) Alpha' : 1. crushing, 2. ball milling, 3. screening, 4. magnetic separating, 5. proportioning according to
mass percent: 7.94 to 45.79 portions of
boron-rich
slag, 12.19 to 58.78 portions of
silicon fume, 3.82 to 19.78 portions of
bauxite, 21.70 to 35.41 portions of
carbon black, 6. wet mixing with
anhydrous ethanol as the medium, 7.
drying with the temperature 60 DEG C; 8.
dry mixing, 9. molding forming, 10. high-temperature
sintering under one
atmospheric pressure, temperature of 1450 to 1500 DEG C, insulation for 6 to 10 hours and protection of
nitrogen; 11. eliminating carbon residual by burning; the second step is that mixing the
powder obtained by the first step and additive CaCO3, and after the molding forming, the final product
sialon ceramic composite material BN / (Ca, Mg) Alpha' is made by
sintering through burying
powder in furnace under temperature 1600 to 1700 DEG C; all properties of the product are good. The invention has simple process, low production cost, and starts a new way for boron-rich
slag integrating utilization and decreases environment
pollution.