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296 results about "Methyl carbamate" patented technology

Methyl carbamate (also called methylurethane, or urethylane) is an organic compound and the simplest ester of carbamic acid (H₂NCO₂H). It is a colourless solid.

Pymetrozine-containing ultralow volume liquid agent

The invention provides a pymetrozine-containing ultralow volume liquid agent, and belongs to the field of pesticides. The ultralow volume liquid agent consists of pymetrozine or active ingredient compounded by using the pymetrozine and an active ingredient II, and the balance of aids and solvent; and the active ingredient II is any one of bifenthrin, beta-cypermethrin, lambda-cyhalothrin, cyfluthrin, fenpropathrin, deltamethrin, etofenprox, triazamate, tolfenpyrad, chlorantraniliprole, flubendiamide, ethiprole, abamectin, emamectin benzoate, ivermectin, sec-butyl phenyl-N-methyl carbamate, buprofezin, hexaflumuron, flufenoxuron, chlorbenzuron, diafenthiuron, indoxacarb, 1,2-Dibenzoyl-1-tert-butylhydrazine and tebufenozide. The ultralow volume liquid agent is used for preventing and controlling multiple pests on paddy, wheat, corn, vegetables, tobacco, tea trees, fruit trees and sugarcane by ultralow volume spraying, low volume spraying or ultralow volume electrostatic spraying. The ultralow volume liquid agent has the advantages of low water consumption, high effect, long acting time, synergy and the like.
Owner:GAUNGXI TIANYUAN BIOCHEM

Mesoporous ZSM-5 zeolite, mesoporous ZSM-5 zeolite-loaded metal sulfide catalyst and application

The invention discloses mesoporous ZSM-5 zeolite, a mesoporous ZSM-5 zeolite-loaded metal sulfide catalyst and an application. The synthesizing method of the mesoporous ZSM-5 zeolite comprises the following steps: (1) after uniformly mixing diallylamine and concentrated hydrochloric acid, adding dimethyl diallyl ammonium chloride, uniformly stirring and reacting for 1-6 hours at 60-120 DEG C, and cooling to obtain a template agent DMMC (Dimethylol Methyl Carbamate); (2) preparing acidified aluminum sulfate liquor by aluminum sulfate, concentrated sulfuric acid and water; (3) adding water into water glass, uniformly stirring, adding NaOH, adding the template agent DMMC after cooling to room temperature, continuously stirring for 2-5 hours, then adding the acidified aluminum sulfate liquor under stirring, and stirring for 2-8 hours to obtain a gel in a final state; (4) crystallizing the gel in the final state obtained in the step (3), filtering, drying and calcining to obtain the mesoporous ZSM-5 zeolite. The mesoporous ZSM-5 zeolite-loaded metal sulfide catalyst prepared by taking the mesoporous ZSM-5 zeolite as a carrier is applied to hydrodesulfurization of 4, 6-dimethyl dibenzothiophene and hydrocracking reaction of n-decane, thereby greatly improving the raw material conversion ratio.
Owner:WENZHOU UNIVERSITY

Metaflumizone synthesis method

The invention relates to a metaflumizone synthesis method, in particular to a metaflumizone pesticide synthesis method, belonging to the field of agricultural insecticides. The method is formed by the following steps: synthesis of p-trifluoromethoxybenzene methyl carhamate, synthesis of p-trifluoromethoxybenzene aminooxamide and synthesis of metaflumizone. The invention has the advantages that the preparation method is simple and practical, the efficiency is high and the yield of products at each step is more than 85 percent; the toxicity of the reagent used during the synthesis processes is low, the solvent can be recycled, the side reaction is less, the corrosion to the device is low and the environmental pollution is low; and since the price of the raw materials is cheap, the production cost is reduced, the economy is good and the application prospect is good.
Owner:NANKAI UNIV

Color-developing method for rapid detection of residual organophosphorus and N-methyl carbamate pesticides

InactiveCN102455295ANegative and positive color development results are obviousEasy to operateMaterial analysis by observing effect on chemical indicatorMethyl carbamatePesticide residue
The invention relates to a rapid detection method for residual pesticides. The invention reveals an acetylcholinesterase-based color-developing method for the first time, and in the method, a special color-developing agent is adopted, so that negative and positive color-developing results are extremely obvious, and can be directly judged by naked eyes without using a spectrophotometer, therefore, the method has a good application prospect in the field of rapid detection on residual pesticides.
Owner:上海福盈资产管理有限公司

Raw bamboo protective agent and processing technology thereof

InactiveCN102687729APlay a role in long-term protectionMoth proofBiocidePest repellentsPunchingMethyl carbamate
The invention discloses an insect-resistant, corrosion-resistant, and mildew-resistant raw bamboo protective agent which comprises the following components: ammoniacal copper quaternary, N-2-benzimidazolyl methyl carbamate, and a penetrating agent, and also discloses processing technology of the raw bamboo protective agent, which comprises the following steps: performing bamboo joint punching processing of a fresh felled raw bamboo, naturally drying; putting the raw bamboo into a pressure impregnation tank, closing the tank door, turning on a vacuum pump to vacuumizing the impregnation tank; adding the raw bamboo protective agent till the impregnation tank is filled up with the vacuum pump being turned on; turning off the vacuum pump, turning on a pressure pump till the raw bamboo protective agent becomes saturated in the raw bamboo; releasing the pressure, discharging the protective agent in the impregnation tank. The purpose of the invention is to provide the raw bamboo protective agent which can simultaneously provide insect-resistant, corrosion-resistant, and mildew-resistant effects for raw bamboos, and also to provide the processing technology of the raw bamboo protective agent, which allows the protective agent to completely penetrate into the raw bamboo and thus to reach the effect of long-term raw bamboo protection without environment problems.
Owner:SOUTHWEST FORESTRY UNIVERSITY +1

Technology for synthesizing pyraclostrobin by six-step method

The invention provides a technology for synthesizing pyraclostrobin by a six-step method. The synthesis technology comprises the following steps: 1) performing a reduction reaction of ortho-nitrotoluene; 2) performing an acylation reaction of hydroxylamine; 3) performing a methylation reaction; 4) obtaining N-methoxyl-N-2-bromomethyl phenyl methyl carbamate through a bromination reaction; and 5) performing synthesis of 1-(4-chlorophenyl)pyrazolidine-3-ketone; and 6) performing synthesis of pyraclostrobin. Compared with the prior art, the preparation method has the advantages of simple process, easily available raw materials with low cost, and mild reaction condition, and the purity and yield of the target products are high.
Owner:ANHUI GUANGXIN AGROCHEM

Method for preparing 5-(4- fluobenzene sulphonyloxy) benzimidazole-2-amido methyl formate

The invention relates to a preparation method for 5-(4-fluorophenyl-sulfonyl)-benzimidazole-2-methyl carbamate. The method includes (1) using p-aminophenol as raw materials, and preparing a number of new 3-nitro-4-substituted aminophenol intermediates through acylation and denitrification; (2) carrying out a condensation reaction of 3-nitro-4-substituted aminophenol intermediates with the 4-fluorophenylsulfonyl chloride in the alkaline solution, and hydrolyzing to obtain 2-nitro-4-(4-fluorophenyl-sulfonyl)-aniline intermediates; (3) carrying out a reduction reaction of 2-nitro-4-(4-fluorophenyl-sulfonyl)-aniline intermediates to obtain 4-(4-fluorophenyl-sulfonyl)-o-phenylenediamine intermediates; and (4) carrying out a closed loop reaction of closed-loop agents and 4-(4-fluorophenyl-sulfonyl)-o-phenylenediamine to obtain 5-(4-fluorophenyl-sulfonyl)-benzimidazole-2-methyl carbamate. This invention has the advantages of high yield, small unit consumption, and low cost. The raw materials are cheap and the method is easy for industrialized production.
Owner:CHANGZHOU YABANG QH PHARMACHEM +1
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