The invention discloses a preparation method of a carbon / carbon hot-pressing mold for a high-pressure hot-pressing
sintering furnace, which comprises the following steps of: 1, presetting continuous
carbon fibers along the radial direction of a hot-pressing mold paving layer, and paving the
carbon fibers along the circumferential direction and the longitudinal direction to obtain a three-dimensional structure prefabricated body; 2, high-temperature pretreatment; 3, performing
chemical vapor deposition to obtain a hot-pressing die blank; 4, dipping-carbonizing to obtain a compact hot-pressing die blank; 5,
processing to a final size; and 6, dipping-carbonizing to obtain the carbon / carbon hot-pressing mold. The continuous
carbon fibers are introduced in the radial direction in advance, then the circumferential carbon fibers and the longitudinal carbon fibers are laid, the damage effect of the radial carbon fibers is avoided, the circumferential carbon fibers and the longitudinal carbon fibers are kept complete and continuous, the reinforcing effect is achieved, the overall structural strength is improved, the radial heat
conductivity coefficient of the carbon / carbon hot-pressing die is increased, and the service life of the carbon / carbon hot-pressing die is prolonged. Therefore, the carbon / carbon hot-pressing die is stable in structure, excellent in
mechanical property, uniform in thermal field, long in service life and suitable for a high-pressure hot-pressing furnace.