The invention discloses a metallographic preparation method of a
tungsten-
zirconium alloy. The metallographic preparation method is characterized by comprising the following steps of: 1) sampling, intercepting a small block sample, and enabling a
cutting surface to be an inspection surface, 2)
grinding,
grinding the inspection surface with
abrasive paper to remove surface scratches, and after
grinding is finished, putting the sample into
alcohol for ultrasonic cleaning, and then taking out and blow-
drying the sample, (3) rough
polishing, specifically, conducting rough
polishing through
a diamond spray
polishing agent, and enabling the rotating speed to range from 300 r / min to 500 r / min, and after rough polishing is finished, putting the sample into
alcohol, ultrasonically cleaning, takingout and blow-
drying, (4) conducting fine polishin, specifically, conducting fine polishing through a
chromium sesquioxide polishing agent, and enabling the rotating speed to range from 100 r / min to 150 r / min, and after the fine polishing is finished, putting the sample into
alcohol, ultrasonically cleaning, taking out and blow-
drying, and (5) final polishing, specifically, conducting final polishing through
silicon latex suspension liquid, enabling the rotating speed to be 100-150 r / min, after final polishing is completed, putting the sample into alcohol to be subjected to ultrasonic cleaningand then taken out to be blow-dried to be observed. The metallographic preparation method has the advantages that the
sample preparation time is shortened, and the microscopic structure is clear and visible.