409 results about "Elemental composition" patented technology

A precursor source mixture useful for CVD or ALD of a film comprising: at least one precursor composed of an element selected from the group consisting of Li, Na, K, Rb, Cs, Fr, Be, Mg, Ti, Zr, Hf, Sc, Y, La, V, Nb, Ta, Cr, Mo, W, Mn, Re, Fe, Ru, Os, Co, Rh, Ir, Ni, Pd, Pt, Cu, Ag, Au, Zn, Cd, Hg, B, Al, Ga, In, Tl, Si, Ge, Sn, Pb, As, P, Sb and Bi, to which is bound at least one ligand selected from the group consisting of hydride, alkyl, alkenyl, cycloalkenyl, aryl, alkyne, carbonyl, amido, imido, hydrazido, phosphido, nitrosyl, nitryl, nitrate, nitrile, halide, azide, alkoxy, siloxy, silyl, and halogenated, sulfonated or silyated derivatives thereof, which is dissolved, emulsified or suspended in an inert liquid selected from the group consisting of aliphatic hydrocarbons, aromatic hydrocarbons, alcohols, ethers, aldehydes, ketones, acids, phenols, esters, amines, alkylnitrile, halogenated hydrocarbons, silyated hydrocarbons, thioethers, amines, cyanates, isocyanates, thiocyanates, silicone oils, nitroalkyl, alkylnitrate, and mixtures thereof. The precursor source mixture may be a solution, emulsion or suspension and may consist of a mixture of solid, liquid and gas phases which are distributed throughout the mixture.

Compositions, apparatus incorporating a composition, and methods of use are described, one composition embodiment consisting essentially of one or more reactive metals in major proportion, and one or more alloying elements in minor proportion, with the provisos that the composition is high-strength, controllably reactive, and degradable under defined conditions. Compositions of the invention may exist in a variety of morphologies, including a reactive metal or degradable alloy processed into an alloy of crystalline, amorphous or mixed structure that may constitute the matrix of other composition, for instance a composite. Methods of using apparatus comprising a composition, particularly in oilfield operations are also described (e.g. flow and displacement control, sensors, actuators). This abstract allows a searcher or other reader to quickly ascertain the subject matter of the disclosure. It will not be used to interpret or limit the scope or meaning of the claims. 37 CFR 1.72(b).

A method comprising the following steps: (a) providing a turbine component comprising a metal substrate having an external surface; and (b) analyzing the external surface by laser plasma spectroscopy to determine whether a metallic coating is present on or absent from the external surface. If a metallic coating is determined to be present on the external surface, the elemental composition, elemental concentration and / or thickness of the metallic coating present on the external surface may be determined (qualitatively and / or quantitatively) by laser plasma spectroscopy. Another method comprises the following steps: (a) providing a turbine component comprising a metal substrate having an external surface which has been subjected to treatment to remove a metallic coating applied to the external surface; and (b) analyzing the treated external surface by laser plasma spectroscopy to determine the degree of removal of the metallic coating from the treated external surface.

A process for the partial catalytic oxidation of a hydrocarbon containing feed comprising contacting the feed with an oxygen-containing gas in the presence of a catalyst retained within a reaction zone in a fixed arrangement, wherein the catalyst comprises at least one catalytically active metal selected from the group consisting of silver and Group VIII elements supported on a porous ceramic carrier. The porous ceramic carrier has a distribution of total pores wherein about 70% of the total pores (1) have a volume-to-surface area (V / S) ration that is within about 20% of the mean V / S value for the total pores and no pores have a V / S ration that is greater than twice the mean V / S value for the total pores; (2) have a pore-to-pore distance between neighboring pores that is within about 25% of the mean pore-to-pore distance between neighboring pores; and (3) have a pore throat area that is within about 50% of the mean pore throat are for the pores. Additionally, about 50% of the total pores have a coordination number between neighboring pores that is within about 25% of the mean coordination number between neighboring pores. Preferably, the oxidation process comprises a multistage, staged oxygen, catalytic partial oxidation process having fewer than or equal to about five stages and including a first stage preheat temperature of greater than about 550° C., and wherein the temperature of the product mixture in each stage following the first stage is at least about 700° C.

An apparatus (100) for sequentially analyzing particles such as single cells or single beads, by spectrometry. The apparatus, an elemental flow cytometer, includes means (102) for sequential particle introduction, means (104) to vaporize, atomize and excite or ionize the particles, or an elemental tag associated with an analyte on the particles, and means (106) to analyze the elemental composition of the vaporized, atomized and excited or ionized particles, or an elemental tag associated with the particles. Methods for sequentially analyzing particles such as singe cells or single beads by spectrometry are also described.

An article made of constituent elements is prepared by furnishing at least one nonmetallic precursor compound, wherein all of the nonmetallic precursor compounds collectively contain the constituent elements. The constituent elements include a titanium-base metallic composition, boron present at a level greater than its room-temperature solid solubility limit, and, optionally, a stable-oxide-forming additive element present at a level greater than its room-temperature solid solubility limit. The precursor compounds are chemically reduced to produce a material comprising a titanium-base metallic composition having titanium boride particles therein, without melting the titanium-base metallic composition. The titanium-base metallic composition having the titanium boride particles therein is consolidated without melting.

The present invention provides a method and apparatus for performing elemental analysis of a formation fluid downhole. The present invention provides elemental analysis of a formation fluid downhole using breakdown spectroscopy. In one aspect of the invention, a method and apparatus are provided for performing laser induced breakdown on a formation fluid sample is provided. In another aspect of the invention a method and apparatus are provided for performing spark induced breakdown spectroscopy. Plasma is induced in a fluid under test downhole. Emissions from the plasma are analyzed to determine the elemental composition of the fluid under test. Emissions include but are not limited to light in the ultraviolet, visible, and near infrared regions of the spectrum. A spectrometer is provided for elemental analysis of a fluid downhole. Elemental analysis yields information about the fluid and the formation from which the fluid originated.

An apparatus (100) for sequentially analyzing particles such as single cells or single beads, by spectrometry. The apparatus, an elemental flow cytometer, includes means (102) for sequential particle introduction, means (104) to vaporize, atomize and excite or ionize the particles, or an elemental tag associated with an analyte on the particles, and means (106) to analyze the elemental composition of the vaporized, atomized and excited or ionized particles, or an elemental tag associated with the particles. Methods for sequentially analyzing particles such as singe cells or single beads by spectrometry are also described.

A sputter target material which is of a sintered material, wherein the sputter target material consists of 0.5 to 50 atomic % in total of at least one metal element (M) selected from the group of Ti, Zr, V, Nb and Cr, and the balance of Mo and unavoidable impurities, and has a microstructure seen at a perpendicular cross section to a sputtering surface, in which microstructure oxide particles exist near a boundary of each island of the metal element (M), and wherein the maximum area of the island, which is defined by connecting the oxide particles with linear lines so as to form a closed zone, is not more than 1.0 mm2.

A method for calibrating and analyzing data from a mass spectrometer, comprising the steps of acquiring raw profile mode data containing mass spectral responses of ions with or without isotopes; calculating theoretical isotope distributions for each of at least one calibration ion based on elemental composition; convoluting the theoretical isotope distributions with an initial peak shape function to obtain theoretical isotope profiles for each ion; constructing a peak component matrix including the theoretical isotope profiles for calibration ions as peak components; performing a regression analysis between the raw profile mode mass spectral data and the peak component matrix; and reporting the regression coefficients as the relative concentrations for each of the components. A mass spectrometry system operated in accordance with the method and a computer readable medium having program code thereon for performing the method.

A battery has a positive electrode active material containing an olivine lithium phosphate-based compound having an elemental composition represented as LiMPO4, where M is a transition metal including at least Fe. The product of a separator thickness x (μm) and a separator porosity y (%) is controlled to be equal to or less than 1500 (μm·%). A porous layer containing inorganic particles and a binder is disposed between the separator and the positive electrode and / or between the separator and the negative electrode.

Differing from traditional alloys often containing one primary elemental composition, the present invention reforms a conventional superalloy to a high-entropy superalloy by redesigning the elemental compositions of the conventional superalloy based on a mixing entropy formula. Particularly, this high-entropy superalloy shows advantages of light weight and low cost under the premise of containing a low amount of expensive metal composition. The proposed high-entropy superalloy of the present invention comprises a primary elemental composition and at least one principal strengthening elemental composition, wherein the primary elemental composition has a first element content of at least 35 at % and each of the principal strengthening elemental compositions have a second element content of over 5 at %. Moreover, a variety of experimental results have proved that the high-entropy superalloy simultaneously possesses a variety of excellent high-temperature mechanical properties, such as high mechanical strength, high corrosion resistance, high oxidation resistance, and high creep resistance.

Structural parameters of a specimen are determined by fitting models of the response of the specimen to measurements collected by different measurement techniques in a combined analysis. X-ray measurement data of a specimen is analyzed to determine at least one specimen parameter value that is treated as a constant in a combined analysis of both optical measurements and x-ray measurements of the specimen. For example, a particular structural property or a particular material property, such as an elemental composition of the specimen, is determined based on x-ray measurement data. The parameter(s) determined from the x-ray measurement data are treated as constants in a subsequent, combined analysis of both optical measurements and x-ray measurements of the specimen. In a further aspect, the structure of the response models is altered based on the quality of the fit between the models and the corresponding measurement data.

A system and method for measuring elemental concentrations of a material from a sample containing several elements by LIBS analysis. The material is heated to generate plasma and its chemical composition is determined from spectral analysis of its radiation. The spectral lines of interest are identified among those emitted by the constituents of each element composing sample. The intensities of the spectral lined identified are measured. From an estimate of temperature, electron density and relative concentration values, the chemical composition of the plasma is calculated. The absorption coefficient according to wavelength is calculated for the spectral zones of the lines of interest. From an estimate of the plasma width, the spectral radiance of the plasma is calculated for the same spectral zones and then a comparison of the intensity and shape of the spectrum thus calculated with those of the spectrum measured is performed. These calculations and this comparison are repeated iteratively in order to adjust the temperature, electron density, relative values of the elemental concentrations and width of the plasma.

A material sorting system sorts materials, such as scrap pieces composed of unknown metal alloys, as a function of their detected x-ray fluorescence. The x-ray fluorescence may be converted into an elemental composition signature that is then compared to an elemental composition signature of a reference material in order to identify and / or classify each of the materials, which are then sorted into separate groups based on such an identification / classification. The material sorting system may include an in-line x-ray tube having a plurality of separate x-ray sources, each of which can irradiate a separate stream of materials to be sorted.

The present invention provides a novel organic compound capable of simultaneously emitting fluorescence and phosphorescence. The organic compound according to the present invention is an organic compound consisting of only elemental hydrogen and at least two kinds of elements selected from the group consisting of elements belonging to the thirteenth group to the seventeenth group of the second period to the fifth period of the periodic table, and being capable of simultaneously emitting fluorescence and phosphorescence at a temperature of from −30° C. or more and 100° C. or less.

The invention discloses a high-strength and high-conductivity CuAg alloy material with a continuous fiber tissue and a preparation method thereof. The material consists of Cu, Ag, etc. Cu and Ag alloyingot with a columnar structure is obtained by a directional solidification technology, and continuous fibrous tissue structure is obtained by the technologies of extruding, drawing, etc. The components of the alloy material are as follows: 5-10wt% of Ag and balance of Cu. The preparation method of the CuAg alloy comprises the following steps: (1) preparing chemical composition; (2) vacuumizing asmelting room and a directional solidification room; (3) smelting the alloy; (4) directionally solidifying; (5) hot extruding; (6) hot processing; and (7) drawing wire or rolling. The material is applicable to slide contact material such as a middle-load and low-load switch, a breaker, a contactor, a micromotor slip ring, a commutating sheet, and the like, high-pulse magnetic field conductor material, an integrated circuit lead wire frame, a fish torpedo lead wire, an electric conduction reed, etc.

A correlative evaluation of a sample using an x-ray computed tomography (CT) x-ray fluorescence (XRF) system and the method for analyzing a sample using x-ray CT and XRF is disclosed. The CT / XRF system includes an x-ray CT subsystem for acquisition of volume information and a confocal XRF subsystem for acquisition of elemental composition information. The CT / XRF system also includes a controller for managing the acquisitions by the x-ray CT subsystem and confocal XRF subsystem. Combining sub-micrometer spatial resolution 3-D imaging with elemental composition analysis in 3-D with ppm level sensitivity is important to elemental identification of precious metal grains in crushed and ground ores and floatation tailings in the mining industry.

Disclosed is a polymer material comprised of at least one non-cyclic ceramic-forming polymer. The porosity and elemental composition of the resulting ceramic can be varied by inclusion of polymers with particular ratios of carbon, silicon, oxygen, and hydrogen and by manipulation of the conditions under which the polymer material is converted to a ceramic. The resulting ceramic may be useful in fiber-reinforced ceramic matrix composites (CMCs), semiconductor fabrication, fiber coatings, friction materials, and fire resistant coatings. A first aspect of the invention provides a compound of formula I wherein x is between about 0.75 and about 0.9, y is between about 0.05 and about 0.15, and z is between about 0.05 and about 0.20.

A titanium material of the present invention includes a base material composed of a titanium alloy containing at least one alloying element selected from the group consisting of gold, silver, and platinum group elements; and a concentrated layer integrally disposed as a layer on the surface of the base material. In the concentrated layer, the alloying elements are concentrated by elution of Ti from the surface of the base material. The average thickness of the concentrated layer is 2.5 nm or more. The total alloying element concentration in the concentrated layer is 40 to 100 atomic percent. The total content of the alloying element in the base material is 0.01 to 1.0 percent by mass. Electrodes composed of the titanium material of the present invention are suitable for use in separators of fuel cells, and can readily be produced, so that the cost can be reduced.

This invention discloses preparation and application of regulator for repairing soil polluted by heavy metals. The regulator utilizes hydroxyapatite extracted from animal bone as the main raw material, as well as commercialized Si-Ca-Mg Fertilizer at a ratio of 1:(0.5-1). Besides, solutions containing Fe, Zn, Mn, Mo, B, etc., are also added. The regulator comprises: CaO 40-50 wt.%, SiO2 10-20 wt.%, MgO 3-6 wt.%, P2O5 15-30% wt.%, Al2O3 5-10 wt.%, K2O 0.1-0.5 wt.%, Fe2O3 0.1-1.0% wt.%, ZnO 0.3-0.5 wt.%, MnO 0.1-0.5 wt.%, and impurities. Once applied, the regulator is uniformly mixed with soil according to a ratio of 0.05-1.0 wt. % of dry soil. The regulator has such advantages as abundant raw materials, simple process, low cost, good repairing effect, low addition amount, no secondary pollution, no influence on soil structure, and high nutrition, thus can partly replace chemical fertilizers.

An X-ray fluorescence measuring system and related measuring methods are disclosed, the system using X-ray energy at a level of less than 80 KeV may be directed toward a material, such as coal. The energy fluoresced may be detected (10) and used to measure the elemental composition of the material, including trace elements. The material may be moving or stationary.

A portable system for elemental analysis includes one or more neutron emitters, a chamber for containing a test sample, at least one gamma ray detector electrically connected to a data acquisition system, and software or firmware executing on the data acquisition system from a non-transitory physical medium, the software or firmware providing a first function for producing one or more gamma ray spectrums, a second function for applying correction factors to the one or more gamma ray spectrums, and a third function for analyzing the corrected gamma ray spectrum or spectrums to determine a deconvolved elemental composition of the test sample.

Disclosed are methods and apparatus for characterizing defects by using X-ray emission analysis techniques. The X-rays are emitted in response to an impinging beam, such as an electron beam, directed towards the sample surface where a defect resides. It may also be used to help determine where the void(s) are with respect to the interconnect structure. Methods disclosed are for spatially locating defects in or on integrated circuits. Also disclosed are methods for identifying the elemental composition of defects and spatially locating different elemental components of defects.

A powder raw material is prepared by mixing at least two kinds of powders selected from a powder A, a powder B, a powder C, and a powder D. A sintered body of a magnetic material having an NaZn13 crystal structure phase is formed by heating the powder raw material while applying a pressure treatment. The powder A is at least one of elemental powder of element R selected from Y, La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, and Yb. The powder B is at least one of elemental powder of element T selected from Fe, Co, Ni, Mn, and Cr. The powder C is at least one of elemental powder of element M selected from Si, B, C, Ge, Al, Ga, and In. The powder D is a compound powder composed of at least two kinds of elements selected from the element R, the element T, and the element M.

A method for manufacturing an Al-Mg-Si series alloy plate includes the steps of hot-rolling and subsequently cold-rolling an Al-Mg-Si series alloy ingot. The Al-Mg-Si series alloy ingot consists of Si: 0.2 to 0.8 mass %, Mg: 0.3 to 1 mass %, Fe: 0.5 mass % or less, Cu: 0.5 mass % or less, at least one of elements selected from the group consisting of Ti: 0.1 mass % or less and B: 0.1 mass % or less and the balance being Al and inevitable impurities. Heat-treating for holding a rolled ingot at 200 to 400° C. for 1 hour or more is performed after a completion of the hot-rolling but before a completion of the cold-rolling.

A system to detect a plurality of elements is proposed. The system includes one or more X-ray sources for transmitting X-rays towards a sample and also includes plurality of photon detectors. An array of crystals are arranged in a curvature with appropriate geometry for receiving a plurality of photon energies emitted from the sample and focusing the photon energy on the plurality of detectors. The plurality of photon detectors are spatially arranged at Bragg angles corresponding to signature photon energies to detect the plurality of elements simultaneously.